GAMRY 992-00183 Faraday Shield Conductive Glass Window User Manual

June 5, 2024
GAMRY

GAMRY 992-00183 Faraday Shield Conductive Glass Window

Safety Considerations

Your Faraday Shield has been supplied in a safe condition. This chapter of the Operator’s Manual contains some information and warnings that you must follow to insure continued safe operation.
Inspection
When you receive your Faraday Shield, inspect it for evidence of shipping damage. If any damage is noted, please notify Gamry Instruments Inc. and the shipping carrier immediately. Save the shipping container for possible inspection by the carrier. The Faraday Shield has a conductive coating on the outer side of the glass pane in the door. If the glass is cracked, the conductivity could be broken, compromising the Faraday Shield’s ability to function as a Faraday cage.

Warning! The door of the Faraday Shield contains a large pane of glass with a conductive coating on the outside surface. Chips on the corners, while not affecting performance, can have extremely sharp edges that represent a significant safety hazard. Injuries from broken glass can be quite severe.

Grounding in the Faraday Shield
The metal case of the Faraday Shield is not connected to an earth ground. Grounding is best accomplished by connecting the ground lead of the potentiostat to the internal ground lug of the Faraday Shield. Proper grounding is required for the Faraday cage to function.
Most electrochemical cells are isolated from earth ground, in which cases isolation of the Faraday Shield from earth is not required. Connection of the Faraday Shield to an earth ground (when allowed) may lower the noise seen in an electrochemical test.

Sources of earth ground include

  • most metal water pipes
  •  the chassis of most electronic apparatus (which are generally earth grounded)
  • the protective ground terminal of an AC mains power plug

We recommend that you discuss grounding with an electrical or electronics professional prior to making this earth ground connection. This connection of the Faraday Shield to an earth ground is not a “Protective Earth Ground” as defined in IEC 1010. The Faraday Shield is safe in the absence of this connection, for it does not contain any hazardous voltages.

Warning! Do not connect the Faraday Shield’s ground binding post to any voltage other than a potentiostat’s floating or earth ground. An improper connection can create a safety hazard, which could result in personal injury or death.

Temperature and ventilation
Your Faraday Shield was designed for indoor use at ambient temperatures between 0C and 45C. You may need to ventilate or even cool the Faraday Shield with forced air if the temperature rises excessively.

Environmental limits
There are environmental limits on the storage, shipping and operation of this equipment. The Faraday Shield has not been designed for outdoor use.

Storage

Ambient Temperature Relative Humidity            –40C to 75C  Maximum 90% non- condensing

Shipping

Same as storage plus Acceleration                        Maximum 30 G

Operation

Ambient Temperature Relative Humidity              0C to 45C Maximum 90% non- condensing

Caution! The Faraday Shield is not designed for operation in conditions where liquid water may enter the chassis, or water vapor may condense within the chassis.

Use with dangerous materials
Do not use the Faraday Shield with hazardous gases or other poisonous or noxious materials.

Warning! Do not connect the Faraday Shield unit to poisonous, noxious, or explosive materials. Failure to observe this warning could cause injury or property damage. The Faraday Shield is not gas or liquid tight. Use the same precautions as if using an open electrochemical cell on a bench. Operate in a hood (fume cupboard) if dangerous gases are used.

Cleaning
When cleaning the Faraday Shield, disconnect any equipment inside from all power sources prior to cleaning Use a cloth lightly dampened with either clean water or water containing a mild detergent to clean the outside of the enclosure. Alternatively, you can use isopropyl alcohol. Do not use a wet rag or allow fluid to enter the enclosure. Do not immerse the Faraday Shield in any type of cleaning fluid (including water). Do not use any abrasive cleaners.

Caution! Read and understand the Material Safety Data Sheet (MSDS) for any solvent, such as isopropyl alcohol, before use. Always take appropriate precautions when using these materials.

Leakage inside
The Faraday Shield is not sealed to be liquid tight. Avoid spills and promptly clean up any spills that do occur.

RoHS Compliance
The Faraday Shield has been built using lead-free components. This equipment complies with the European RoHS initiative.

Introduction

About this manual
This manual covers the installation, safety, and use of the Gamry Instruments Faraday Shield. Both versions of the Faraday Shield – with and without glass pane are discussed.
About the Faraday Shield
The Faraday Shield is a Faraday cage, designed to be as flexible and convenient as possible for a wide range of electrochemical experiments.
Faraday Shield features include

  1.  Conductive-glass window to allow visual inspection without breaking shielding
  2. Pass-throughs for cables, feed gas, thermostatic control (water)
  3.  Electrical isolation from earth ground
  4.  Adjustable plastic shelf for reducing capacitive effects
  5. Ring stand rod for mounting clamps, various connectors, or adapters to hold glassware, cables, or any other laboratory equipment
  6. Full flexibility with the assembly due to interchangeability of panels

Notational conventions
To make this manual more readable we have adopted some notational conventions. These are used throughout this manual and all other Gamry Instruments manuals:

  • Numbered lists. A numbered list is reserved for step-by-step procedures, with the steps always performed sequentially.
  •  Bulleted list. The items in a bulleted list, such as this one, are grouped together because they represent similar items. The order of items in the list is not critical.

Unpacking and Installation

GAMRY-992-00183-Faraday-Shield-Conductive-
Glass-Window-1

Unpacking
When you receive your Faraday Shield, please verify that you have received the following items. Please refer to the parts list of the system you have:
Table 1 – Faraday Shield – Rev 1 (992-00164)

Quantity Part number Description
1 730-00119 4 mm female banana socket, M4 male screw, insulated, black
1 810-00121 Faraday Shield – Bottom Panel
1 820-00161 Shelf, polypropylene
1 820-00163 Ring stand rod, 12 mm OD, 400 mm length, M6
14 835-00042 Thumbscrew, plastic, M4 x 10 mm, black
4 850-00067 Rubber bumper, 1 5mm OD, 15 mm height, M4
1 966-00012 Door Panel Sub-assembly
3 966-00013 Side Panel Sub-assembly
1 966-00014 Top Panel Sub-assembly
1 988-00078 Operator’s Manual

Table 2 – Faraday Shield with Glass Door – Rev 1 (992-00183)

Quantity Part number Description
1 730-00119 4 mm female banana socket, M4 male screw, insulated, black
1 810-00121 Faraday Shield – Bottom Panel
1 820-00161 Shelf, polypropylene
1 820-00163 Ring stand rod, 12 mm OD, 400 mm length, M6
14 835-00042 Thumbscrew, plastic, M4 x 10 mm, black
4 850-00067 Rubber bumper, 1 5mm OD, 15 mm height, M4
3 966-00013 Side Panel Sub-assembly
1 966-00014 Top Panel Sub-assembly
1 966-00037 Door Panel with Glass Window Sub-assembly
1 988-00078 Operator’s Manual

All panel sub-assemblies have their cable entry plates (P/N 810-00123) already pre-mounted. Please refer to Appendix B for a list of replacement parts and other optional parts for your Faraday Shield.
Initial visual inspection
After you remove your Faraday Shield components from its shipping carton, check all parts for any signs of shipping damage. If any damage is noted, please notify Gamry Instruments, Inc. and the shipping carrier immediately. Save the shipping container for possible inspection by the carrier.
Assembly
Use flat and padded surface (e.g. carpet, cardboard, etc.) for assembling to avoid scratches. No tools are required to assemble or disassemble the Faraday Shield.

Connect side panel sub-assemblies

  • each side panel has two pairs of quick-release hinges mounted
  • snap together corresponding hinges of all three side panel sub-assemblies (966-00013)GAMRY-992-00183-Faraday-Shield-Conductive-Glass-Window-2

Insert bottom panel

  •  slide the bottom panel from the lower end inside the side panel assembly
  • standoffs of the bottom panel don’t have to be inserted into clearance holes yetGAMRY-992-00183-Faraday-Shield-Conductive-Glass-Window-3

Connect door panel sub-assembly

  •  connect the front panel sub-assembly to the left side panel using the quick-release hinges
  • open the door (either metal or with glass pane) and slightly lift up the front part of the bottom panel with its standoffs
  •  align the front panel and connect the other side using the quick-release hingesGAMRY-992-00183-Faraday-Shield-Conductive-Glass-Window-4

Mount bottom panel and feet

  •  once the door panel sub-assembly is connected, align all four standoffs of bottom panel with clearance holes and fully insert
  • lift the cage assembly and screw rubber bumper onto threaded studs
  •  verify that the bottom panel if flush mountedGAMRY-992-00183-Faraday-Shield-Conductive-Glass-Window-5

Mount top panel sub-assembly

  •  put top panel sub-assembly on the top side of the cage
  •  use four thumbscrews to attach

Interconnect side panels

use four thumbs screws to connect all side panels

Mount ground connector, ring stand rod, and shelf

  •  a 4 mm ground jack is provided which can be screwed into any open M4 thread on each side panel inside the Faraday cage
  • screw ring stand rod in any of the four M6 threads at the bottom panel
  • the shelf can be mounted on flanges of side panels at two different heights
  •  place the shelf on flanges (upper or lower level) and attach with six thumb screws
  • slightly open thumbscrews and slide shelf to remove itGAMRY-992-00183-Faraday-Shield-Conductive-Glass-Window-8

Adjust cable entry plates for cables

  • all cable entry plates are pre-mounted; two are located at the top and three on each side panel
  •  slightly unscrew thumb screws of cable entry plate and guide cable through the opening
  •  tighten thumbs screws again to hold both cable entry plate and cables in positionGAMRY-992-00183-Faraday-Shield-Conductive-Glass-Window-9

Physical location
Normally place your Faraday Shield on a flat workbench surface. You need access to the top, rear, left, or right side of the Faraday Shield for cable connections. There are handles on both sides and the rear panel to carry the Faraday Shield. If you place your Faraday Shield within an enclosed space, make sure that the internal temperature within that space does not exceed the 45C ambient temperature limit of the Faraday Shield. Be particularly careful if a computer or other heat-dissipating equipment is mounted in the same enclosure.

Caution! If the Faraday Shield is taken from a cold location (for example: outdoors in winter conditions) to a warm, humid location, water vapor could condense on the cold surfaces inside the Faraday Shield. Allow at least one hour for the Faraday Shield to warm to room temperature.

Faraday Shield fully assembled – 992-00164 (top) and 992-00183 (bottom)GAMRY-992-00183-Faraday-Shield-Conductive-Glass-
Window-10

Specifications

All specifications are subject to change without notice.

Description Dimensions
Exterior dimensions (max.) width: 38 cm (15 inch)

length: 38 cm (15 inch)

height: 45.5 cm (18 inch)

Interior dimensions (max.)| width: 35 cm (13.7 inch)

length: 35 cm (13.7 inch)

height: 41.7 cm (16.4 inch)

Door opening (max.)| width: 28.8 cm (11.3 inch)

height: 40.5 cm (16 inch)

Top opening (max.)| width: 30.2 cm (11.8 inch)

length: 30.2 cm (11.8 inch)

Cable opening (max.)| width: 21 cm (8.2 inch)

height: 2.5 cm (1 inch)

Ring stand rod| length: 40 cm (15.8 inch)

diameter: 12 mm (0.5 inch)

Shelf (max.)| width: 34 cm (13.4 inch)

length: 27.5 cm (10.8 inch) thickness: 6 mm (1/4 inch)

Glass pane| width: 21.5 cm (0.85 inch)

length: 36 cm (1.4 inch) thickness: 4.76 mm (3/16 inch)

conductive coating: about 15 ohms/sq. (on one side only)

Weight (approx.)| Faraday Shield: 7 kg (15.4 lbs)

shelf: 0.5 kg (1.1 lbs)

ring stand rod: 0.12 kg (0.26 lbs) glass pane: 0.9 kg (2 lbs)

Description| Dimensions
Exterior dimensions (max.)| width: 38 cm (15 inch)

length: 38 cm (15 inch)

height: 45.5 cm (18 inch)

Interior dimensions (max.)| width: 35 cm (13.7 inch)

length: 35 cm (13.7 inch)

height: 41.7 cm (16.4 inch)

Door opening (max.)| width: 28.8 cm (11.3 inch)

height: 40.5 cm (16 inch)

Top opening (max.)| width: 30.2 cm (11.8 inch)

length: 30.2 cm (11.8 inch)

Cable opening (max.)| width: 21 cm (8.2 inch)

height: 2.5 cm (1 inch)

Ring stand rod| length: 40 cm (15.8 inch)

diameter: 12 mm (0.5 inch)

Shelf (max.)| width: 34 cm (13.4 inch)

length: 27.5 cm (10.8 inch) thickness: 6 mm (1/4 inch)

Glass pane| width: 21.5 cm (0.85 inch)

length: 36 cm (1.4 inch) thickness: 4.76 mm (3/16 inch)

conductive coating: about 15 ohms/sq. (on one side only)

Weight (approx.)| Faraday Shield: 7 kg (15.4 lbs)

shelf: 0.5 kg (1.1 lbs)

ring stand rod: 0.12 kg (0.26 lbs) glass pane: 0.9 kg (2 lbs)

Appendix B: Replacement parts
In the event of losing or breaking any parts of the Faraday Shield, replacement parts can be individually ordered. The list also includes both door variants and door panel assemblies which are mutually interchangeable for more flexibility.

Part number Description
730-00119 4 mm female banana socket, M4 male screw, insulated, black
810-00123 Cable entry plate
820-00161 Shelf, polypropylene
820-00163 Ring stand rod, 12 mm OD, 400 mm length, M6
835-00042 Thumbscrew, plastic, M4 x 10 mm, black
850-00067 Rubber bumper, 1 5mm OD, 15 mm height, M4

810-00119

966-00036

| Door

Door with Glass Window

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