PCE Instruments PCE-MA 50X Moisture Analyzer User Manual
- June 9, 2024
- PCE Instruments
Table of Contents
PCE-MA 50X Moisture Analyzer
Englis h
User Manual
PCE-MA 50X Moisture Analyzer
User manuals in various languages (français, italiano, español, português,
nederlands, türk, polski,
, ) can be found by using our product search on: www.pce-instruments.com
Last change: 23 October 2018 v1.0
© PCE Instruments
Contents 1 General Safety Precautions ……………………………………………………….. 1
1.1 Warning Symbols and Signals……………………………………………………………………………… 1 1.2
Precautions ………………………………………………………………………………………………………. 1 1.3 Intended
Use…………………………………………………………………………………………………….. 3 1.4 Contact
Conditions…………………………………………………………………………………………… 3 1.5 Precautions
………………………………………………………………………………………………………. 3 1.6 Warranty
………………………………………………………………………………………………………….. 4 1.7 Supervision over Metrological
Parameters …………………………………………………………….. 4 1.8 User Manual
Significance……………………………………………………………………………………. 4 1.9 Staff Competence
……………………………………………………………………………………………… 4 1.10 Protective Clothing
…………………………………………………………………………………………….. 4
2 Transport and Storage ………………………………………………………………. 5
2.1 Delivery Checklist………………………………………………………………………………………………. 5 2.2
Package…………………………………………………………………………………………………………… 5
3 Unpacking and Installation ………………………………………………………… 5
3.1 Place of Use and Assembling………………………………………………………………………………. 5 3.2 Unpacking
………………………………………………………………………………………………………… 5 3.3 Balance Level
Setting…………………………………………………………………………………………. 6 3.4 Standard Delivery Components
List ……………………………………………………………………… 6 3.5 Maintenance
Activities………………………………………………………………………………………… 7 3.6 Powering the Device
………………………………………………………………………………………….. 8 3.7 Temperature Stabilization
Time……………………………………………………………………………. 9 3.8 Connecting Additional Hardware
………………………………………………………………………….. 9
4 Start-Up …………………………………………………………………………………….. 9 5 Keyboard Buttons
functions……………………………………………………. 9 6 Weighing Mode Home Screen
………………………………………………….. 10
6.1 Weighing Window ……………………………………………………………………………………………..10 6.2 Drying Window
………………………………………………………………………………………………….11
7 Balance Menu ………………………………………………………………………….. 12
7.1 Entering Balance Menu ………………………………………………………………………………………12
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7.2 Screen Scrolling ………………………………………………………………………………………………..13 7.3 Soft Keys
List ……………………………………………………………………………………………………13 7.4 Running Software Functions
……………………………………………………………………………….13 7.5 Return to Weighing
Mode……………………………………………………………………………………15 7.6 Buttons, Labels, and Text Field
Configuration ………………………………………………………..15
8 Weighing Operation …………………………………………………………………. 25
8.1 Good Weighing Practice……………………………………………………………………………………..25 8.2 Logging
……………………………………………………………………………………………………………26 8.3
Units………………………………………………………………………………………………………………..27 8.4 Weighing Unit
Selection ……………………………………………………………………………………..27 8.5 Weighing Units
Accessibility………………………………………………………………………………..27 8.6 Start Unit Selection
……………………………………………………………………………………………28 8.7 User defined Unit
………………………………………………………………………………………………28 8.8 Balance Zeroing
………………………………………………………………………………………………..28 8.9 Balance Taring
………………………………………………………………………………………………….29 8.10 Weighing Mode Settings
…………………………………………………………………………………….30 8.11 Proximity Sensors
……………………………………………………………………………………………..32 8.12 AUTOTARE
……………………………………………………………………………………………………..32 8.13 Print
Mode………………………………………………………………………………………………………..33 8.14 Minimum Sample
Weight…………………………………………………………………………………….34 8.15 Cooperation with TITRATORS
…………………………………………………………………………….36
9 Miscellaneous………………………………………………………………………….. 37 10 Adjustment
……………………………………………………………………………… 40
10.1 External Adjustment …………………………………………………………………………………………..40 10.2 User
Adjustment………………………………………………………………………………………………..40 10.3 Report Printout
………………………………………………………………………………………………….41 10.4 Temperature Adjustment
…………………………………………………………………………………….41 10.5 Drying Process Test
…………………………………………………………………………………………..44
11 Determining Printout Content…………………………………………………… 45
11.1 Adjustment Report …………………………………………………………………………………………….45 11.2 Drying
Process Report Printout ……………………………………………………………………………46 11.3 Other Printouts
………………………………………………………………………………………………….48 11.4 Non-standard Printouts
………………………………………………………………………………………51
© PCE Instruments
11.5 Variables ………………………………………………………………………………………………………….54
12 Working Modes General Information ……………………………………… 55
12.1 Working Modes Accessibility ……………………………………………………………………………….55 12.2
Running Working Mode………………………………………………………………………………………56 12.3 Parameters
Related to a Working Mode ………………………………………………………………..56
13 Databases ……………………………………………………………………………….. 56
13.1 Database Connected Operations …………………………………………………………………………57 13.2
Products…………………………………………………………………………………………………………..58 13.3 Users
………………………………………………………………………………………………………………59 13.4 Packaging
………………………………………………………………………………………………………..59 13.5
Customers………………………………………………………………………………………………………..59 13.6 Drying Program
…………………………………………………………………………………………………59 13.7 Drying Process Reports
……………………………………………………………………………………..60 13.8 Ambient Conditions
……………………………………………………………………………………………60 13.9 Weighing
Records……………………………………………………………………………………………..61
14 Sample Preparation for Drying …………………………………………………. 61
14.1 Means of Moisture Content Measurement on a Moisture Analyzer
…………………………….61 14.2 Sampling and Preparation
…………………………………………………………………………………..62
15 Selection of Drying Parameters………………………………………………… 64
15.1 Selecting Optimum Mass for a Sample………………………………………………………………….64 15.2
Influence of Sample Weight on Measurement Result Repeatability ……………………………64
15.3 Drying Temperature …………………………………………………………………………………………..65 15.4 Selecting
Drying Profile ………………………………………………………………………………………65 15.5 Drying
Time………………………………………………………………………………………………………66 15.6 Drying Profile Analysis
……………………………………………………………………………………….67
16 Drying ……………………………………………………………………………………… 67
16.1 Mode Related Settings ……………………………………………………………………………………….68 16.2 Drying
Quick Access Key …………………………………………………………………………………68
17 Drying Process Performed by Means of Quick Menu ………………… 69
17.1 Drying Process Profile and Drying Parameters……………………………………………………….69 17.2
Automatic Finish Mode ……………………………………………………………………………………….71 17.3 Unit of
Displayed and Printed Measurement…………………………………………………………..71
© PCE Instruments
17.4 Printout interval …………………………………………………………………………………………………72
18 Drying Process Performed with Use of Drying Modes Database .. 72 19 Drying
Process ………………………………………………………………………… 73
19.1 End Result Prognosis…………………………………………………………………………………………77
20 Communication ……………………………………………………………………….. 81
20.1 RS-232 Port Settings………………………………………………………………………………………….81 20.2 Ethernet
Port Settings ………………………………………………………………………………………..81 20.3 Wi-Fi Port Settings
…………………………………………………………………………………………….82 20.4 USB Ports
………………………………………………………………………………………………………..85
21 Peripherals………………………………………………………………………………. 88
21.1 Computer …………………………………………………………………………………………………………88 21.2 Printer
……………………………………………………………………………………………………………..90 21.3 USB flash drive
…………………………………………………………………………………………………93 21.4 Barcode reader
…………………………………………………………………………………………………94 21.5 Ambient Conditions
Module…………………………………………………………………………………94
22 Ambient conditions………………………………………………………………….. 95 23 Communication Protocol
…………………………………………………………. 97
23.1 List of commands ………………………………………………………………………………………………97 23.2 Response
format……………………………………………………………………………………………….98 23.3 Manual Printout / Automatic
Printout …………………………………………………………………..112
24 Peripherals…………………………………………………………………………….. 113 25 Error Messages
……………………………………………………………………… 113 26 Use of Moisture Analyzer
……………………………………………………….. 114 27 Maintenance Activities ……………………………………………………………
114
27.1 Cleaning Moisture Analyzer Components…………………………………………………………….115 27.2
Cleaning Temperature Sensor……………………………………………………………………………115 27.3
Troubleshooting ………………………………………………………………………………………………115
28 Additional Equipment …………………………………………………………….. 116 29 Information on
Moister Analyzer …………………………………………….. 116 30
Warranty………………………………………………………………………………… 117 31 Disposal
………………………………………………………………………………… 117
© PCE Instruments
1 General Safety Precautions
1.1 Warning Symbols and Signals
Safety precautions are marked with special descriptions and warning signs.
They inform and warn a user of possible dangers. Ignoring the safety warnings
may cause injuries, damage of the moisture analyzer, its inappropriate
operation and errors of measurements.
1.1.1
Warning Descriptions
WARNING
Medium risk danger that can lead to a serious injury or death.
CAUTION
Low risk danger that can lead to moisture analyzer damage or dysfunction, loss of data or minor or moderate injury.
NOTE
Critical information on the moisture analyzer.
1.1.2 Warning Symbols
Electric shock Acid / Corrosion Potential danger Flammable or explosive substances Toxic substances Hot surface
1.2 Precautions
WARNING! Adherence to safety information and user manual guidelines is
required in order to prevent risk of health damage and even death.
WARNING: Nominal voltage for a moisture analyzer is 230V AC or 115V AC. It
means that safety usage precautions for low voltage devices must be abided by
while operating the device. The moisture analyzer is equipped with a three-
core power supply cable with grounding pin. If necessary, an extension cord
can be used provided that it meets the applicable standards and has a
protective ground conductor. Intended disconnection of the grounding cable is
forbidden.
© PCE Instruments 1
CAUTION: Drying chamber cannot be opened during operation (drying process). It
is due to the fact that a halogen lamp and its glass shield may reach the
temperature of up to 400° C. When setting up the moisture analyzer leave
enough space to prevent heat from building up and to keep your analyzer from
overheating. Leave about 20 cm around the instrument and about 1 m above. Air
vents that are located in the housing cannot be covered, sealed or blocked in
any other way. Do not put any flammable substances on, under or near the
moisture analyzer. Be particularly careful when removing the sample from the
drying chamber: the sample itself, the drying chamber, shields and the pan can
still be extremely hot. In case of any maintenance work (cleaning the inside
of the drying chamber), the moisture analyzer must be switched off. Wait until
all the components have cooled down. Do not perform any modification to the
heating module.
Some types of samples require taking particular safety precautions. They can
pose a danger for people and objects. It is always the user who is liable for
possible damages caused by the use of an inappropriate sample.
CAUTION: Corrosion: substances that release aggressive vapours (e.g. acids)
during the heating process. While drying such substances it is recommended to
work with small samples. Otherwise, vapours can condense on cold housing parts
and cause corrosion.
WARNING: Fire or explosion: flammable or explosive substances, substances
containing solvents or releasing flammable or explosive gases or vapours. When
in doubt as for the sample’s characteristics perform risk analysis before
carrying out the procedure. For the said type of samples, apply as low drying
temperatures as possible, thus preventing flames or explosion. During the
analysis it is necessary to wear protective glasses and gloves. The samples
should be relatively small. Under no circumstances can the instrument be left
unsupervised!
WARNING: Substances containing toxic and caustic or corrosive components:
substances that release toxic gases or vapours can cause irritations (eyes,
skin or respiratory system), illnesses or even death. Dry such substances only
in fume cupboards.
Under no circumstances should the instrument be used within an explosion
endangered area. The moisture analyzer is designed to be operated outside
hazardous areas exclusively.
© PCE Instruments 2
1.3 Intended Use
Moisture analyzer is designed to verify relative moisture content in small
samples of various substances, dry mass content in small samples and mass of
weighed objects. The device ensures fast and precise process of determination
of water content in a tested sample whereas application of touch screen
display considerably simplifies operation and improves functionality of the
moisture analyzer. The device can be used to determine humidity content of
different materials. At the initial stage of the measurement, the moisture
analyzer precisely determines mass of an object placed on a weighing pan. As
the mass reading is stabilized, the sample is quickly heated by a halogen
lamp, an IR emitter or a metal heater causing humidity evaporation from the
tested sample. While sampling, the moisture analyzer is continuously checking
loss of mass, and on calculation, it displays current moisture content of a
tested sample. Compared to conventional methods of humidity content
determination of various substances, application of moisture analyzer
considerably shortens measurement time and simplifies testing procedure.
Moisture analyzer facilitates setting multiple parameters which influence the
procedure of moisture content determination in a sample (temperature, time,
drying modes, etc.).
1.4 Warranty Conditions
CAUTION!
Do not open the drying chamber during the drying process. The moisture analyzer features a
halogen lamp which is a very powerful heat source. Pay special attention not to touch those
elements of a moisture analyzer that get hot while the drying procedure (i.e.: disposable pan, pan
handle, and inner shields of the drying chamber).
Remember that some tested samples may become dangerous when heated (emission of
poisoning vapours, danger of ignition or explosion).
The moisture analyzer is not intended for dynamic weighing. Even if small amounts of a sample
are added to or taken off the weighing pan, the mass readout should be taken only on stabilization
of the measurement result (appearance of stability pictogram
on the display).
Do not place any magnetic materials on the weighing pan, as this can cause damage of the
measuring system of the instrument.
Be sure to avoid impact shock and overloading of the moisture analyzer in excess of the
prescribed maximum measuring range (max capacity), minus any possible tare weight that has
been applied).
Never use the moisture analyzer in an environment endangered by an explosion!
This moisture analyzer is not adjusted for operation in explosive areas. Remember that it is
forbidden to make any modification to the moisture analyzer.
1.5 Precautions
PCE moisture analyzer adheres to all binding safety regulations. Nevertheless
there are exceptional circumstances that may cause danger. Do not open the
instrument’s housing. Inside there are no parts that would require
maintenance, repair or replacement carried out by a user. In case of any
problems, contact PCE service or a distributor. Remember to use the device in
accordance with this user manual, especially to follow instructions on
installation and configuration of a new device. Since use of the moisture
analyzer conversely to safety precautions and user manual guidelines may be
hazardous to operator’s health and life, it is obligatory to read them
carefully:
© PCE Instruments 3
– Use the moisture analyzer to determine humidity content in samples and to
determine mass of a tested sample; any other use of the moisture analyzer may
be dangerous both to the device and the user,
– Before commissioning the moisture analyzer, make sure that the nominal power
of the device specified on its data plate is compatible with the supply in the
mains to which the moisture analyzer is to be plugged in,
– Halogen lamps can only be changed by an authorized service employee, –
Protect moisture analyzer against contacts with liquids, it might lead to
electrocution,
fire, emission of substances containing toxic or caustic vapour, emission of
explosive substances.
1.6 Warranty Warranty does not cover the following cases:
– not observing the user manual regulations, – using the moisture analyzer
conversely to its intended use, – any modifications of a moisture analyzer or
cases when its housing has been opened
(damaged protective stickers), – mechanical defects and defects caused by
media, liquids, water and natural wearing
off, – inappropriate working environment or electrical installations defects,
– and overloading of measuring mechanism.
1.7 Supervision over Metrological Parameters Metrological parameters of a
moisture analyzer need to be checked by a user in determined time intervals.
Inspection frequency is conditioned by ambient conditions in which a moisture
analyzer is used, kind of carried out processes and adopted quality management
system.
1.8 User Manual Significance It is very important to read the user manual
carefully before switching on and starting up moisture analyzer operation,
even if you are experienced and have worked with this type of balance before.
1.9 Staff Competence The moisture analyzer should be utilized and supervised
only by users who are trained and experienced in such type of instruments. In
order to use the moisture analyzer, first read the user manual. Keep these
instructions for the future reference. Do not make any design modifications.
Additional equipment compatible with the moisture analyzer and spare parts
should be supplied by PCE or an authorized distributor.
1.10 Protective Clothing While working with the instrument use protective
clothing, this is to take safety precautions against potential hazards source
of which might be tested samples and ingredients. Use the following while
carrying out tests:
– protective apron, – protective glasses, – protective gloves (while working
with hazardous chemical substances).
© PCE Instruments 4
Before the use of the above-mentioned protective clothing, make sure that it
has been designed to be used with specific samples and that it is not damaged.
2 Transport and Storage
2.1 Delivery Checklist Upon delivery it is necessary to check the package,
make sure that your package bears no signs of damage.
2.2 Package Keep all package elements should your device be transported in the
future. Remember that only original packaging can be used for shipping
purposes. Prior packing uncouple any cables, remove any separable components
(weighing pan, shields, inserts). The device components shall be packed into
an original packaging, thus being protected against potential damage during
transportation.
3 Unpacking and Installation
3.1 Place of Use and Assembling – Store and use your moisture analyzer in
locations free of vibrations and shakes, and free of air movement and dust,
make sure that it is located at the max altitude of 2000 above sea level. –
Make sure that the moisture analyzer’s workplace ensures good air circulation
around the instrument (approximately 20 cm free space around the moisture
analyzer and 1 m free space over it). – Pay attention to the ambient air
temperature in the weighing room, it should not be out of the specified range,
i.e. +10 °C – +40 °C. – Make sure that the moisture analyzer is placed away
from heat sources on a stable wall console desk or on a stable table which is
not affected by vibrations. – Since part of the balance is a strong magnet
take special safety measures when weighing magnetic objects.
3.2 Unpacking Carefully take the device out of the packaging, remove the
transport lock and gently place the moisture analyzer at its workplace.
Install the weighing pan and accessories following the diagram below:
© PCE Instruments 5
Accessories installation:
Install: – Drying chamber base insert (1), – Anti-draft chamber (2), – Pan
handle (3), – Cross-shaped holder (4), – Disposable pan (5).
Positioning the bracket:
When installing the cross-shaped holder (pan supporter) pay special attention
to the correct positioning of its mandrel. The mandrel features a cut
providing unique positioning of the holder against the pan handle, thus
preventing their contact and friction.
Setting the cross-shaped holder: – assemble the holder onto the mandrel and
turn it slightly so that the mandrel cuts are located in their unique and
correct position, – CAUTION: turn the mandrel gently so as not to damage
moisture analyzer’s measuring system.
3.3 Balance Level Setting It is necessary to level the balance prior
connecting it to the mains. To level the balance turn its feet until an air
bubble takes central position.
3.4 Standard Delivery Components List – Moisture analyzer, – Drying chamber
base insert, – Drying pan shield,
© PCE Instruments 6
– Drying pan handle, – Cross-shaped holder, – Disposable pan, – Power cord, –
User manual CD version.
3.5 Maintenance Activities Disassembly a weighing pan and other detachable
components (the components differ depending on a balance type see Unpacking
and Installation section). Be careful while detaching the components so as not
to cause any damages to the balance mechanism. In order to ease cleaning of
glass anti-draft chamber panes, it is permissible to remove them following the
below instruction.
CAUTION! Cleaning anti-draft chamber while still installed may cause damage of
the measuring system. Cleaning ABS components:
To clean dry surfaces and avoid smutching use clean non-coloring cloths made
of cellulose or cotton. You can use a solution of water and detergent (soap,
dishwashing detergent, glass cleaner). Gently rub the cleaned surface and let
it dry. Repeat cleaning process if needed.
In the case when contamination is hard to remove, e.g. adhesive, rubber,
resin, polyurethane foam residues etc., you can use a special cleaning agents
based on a mixture of aliphatic hydrocarbons that do not dissolve plastics.
Before using the cleanser for all surfaces we recommend carrying out tests. Do
not use products containing abrasive substances.
Cleaning anti-draft chamber panes:
Select dissolvent depending on a dirt. Never soak the glass panes in alkaline
solutions since they interact with glass and may cause damage. Do not use
abrasive substances.
For organic dirt use acetone first, next use water or detergent. For other
than organic dirt use diluted acid solutions (soluble salts of hydrochloric or
nitric acid) or base solutions (ammonium or sodium base).
To remove ACIDS use protofilic solvent (sodium carbonate), to remove BASE use
protogenic solvent (mineral acid of various concentration).
In case of heavy contamination use brush or detergent nevertheless avoid
detergents containing large and hard molecules which could potentially scratch
glass panes.
Use soft brush with wooden or plastic handle exclusively to avoid risk of
scratches. Do not use wire brush.
At the end of the cleaning process rinse the pane using running water first,
distilled next.
Rinsing is a necessary cleaning process stage allowing to remove remaining
soap, detergents and other cleansers from the panes prior their
reinstallation.
Avoid drying the panes either using paper towel or forced air circulation
since some fibres, grains or contamination of other type could permeate into
the panes thus causing weighing errors.
© PCE Instruments 7
One shall not use driers when drying measuring glass tools.
It is a frequent treatment to leave glass components on a rack to dry.
Cleaning stainless steel components:
Avoid using cleansers containing any corrosive chemicals, e.g. bleach
(containing chlorine). Do not use abrasive substances. Always remove the dirt
using microfiber cloth to avoid damage of protective coating.
In case of a daily maintenance: 1. Remove the dirt using cloth dipped in warm
water. 2. For best results, add a little dishwashing detergent.
Cleaning powder-coated components:
For preliminary cleaning stage you need running water or wet sponge featuring
large holes, this will help you to remove loose, heavy dirt.
Do not use cleansers containing abrasive substances.
Next using cloth and cleanser-water solution (soap, dishwashing liquid) gently
rub the cleaned surface.
Avoid using cleanser without water since it may result with damage of the
cleaned surface, please mind that large amount of water mixed with cleanser is
a must.
Cleaning aluminium components:
While cleaning aluminium components use products acid by nature, e.g. spirit
vinegar, lemon. Do not use abrasive substances. Avoid using hard brush, this
may cause scratches. It is recommended to use microfiber cloth.
Use circular movements while polishing the surface. Use only clean and dry
cloth.
3.6 Powering the Device
A moisture analyzer can be plugged to the mains only by means of an original
power cord, which comes standard with the moisture analyzer. Rated voltage
(specified on the device’s data plate) must be compatible with the mains rated
voltage.
The power cord can be connected only to a socket with a ground contact. Plug the power cord to
the moisture analyzer. The moisture analyzer’s power plug is located at the
back of its housing. Moisture analyzer display shows name and program number
first, next an indication 0.000 g
(balances with readability of 1 mg) or 0.0000 g (balances with readability of
0,1 mg). If the
indication does not equal zero, press
button.
© PCE Instruments 8
3.7 Temperature Stabilization Time Before start of measuring processes, it is
necessary to wait until the moisture analyzer reaches thermal stabilisation.
For moisture analyzers that were stored in much lower temperatures before
plugging to mains (e.g. during winter period), thermal stabilisation period
shall take at least 4 hours. During the thermal stabilization, the indications
on a display panel can change. It is recommended that ambient temperature
changes at place of use were insignificant (slow to change).
3.8 Connecting Additional Hardware Use only accessories and peripheral
equipment recommended by the manufacturer. The moisture analyzer must be
disconnected from the mains before connecting or disconnecting any peripherals
(printer, PC computer, USB type computer keyboard or additional display). On
connecting the peripherals, plug the balance to the mains.
4 Start-Up
– Plug the power adapter to a socket, next connect the connector to port
located at the back of the housing.
– Press button located in the top right hand corner of the terminal. – Wait
until start-up procedure is completed, the home screen of balance software is
displayed automatically. – The balance runs with no user logged in. In order
to start operation it is necessary to
carry out the logging procedure (for detailed logging procedure read later
sections of this user manual).
5 Keyboard Buttons functions
Button Overview:
© PCE Instruments 9
Press to switch the balance ON/OFF Press to Zero the balance Press to Tare the balance Press to send measurement to a printer or a computer Function key
– Section comprising supplementary information on currently performed
operations, and function buttons:
CAUTION! Data and buttons contained in the workspace are freely configurable.
For detailed information on data and buttons configuration refer to section
7of this user manual. 6.2 Drying Window
The main window of balance software can be divided into 3 sections: – Top
section displaying data on active working mode (pictogram and name),
metrologically important data and button enabling selection of functions
available for a particular working mode:
– Section presenting the weighing result: © PCE Instruments 11
– Section comprising supplementary information on currently performed
operations, and function buttons:
CAUTION! Data and buttons contained in the workspace are freely configurable.
For detailed information on data and buttons configuration refer to section 7
of this user manual.
7 Balance Menu
Operation of balance software menu is intuitive and uncomplicated. The touch
panel makes the software operation easy. Pressing a function key, a soft key
or an area on the display initiates an assigned function or process. 7.1
Entering Balance Menu
In order to enter balance menu, press
comprised within information section, or clicking any button with particular parameter name,
results with change of color. This is for signalling purposes. If a given area has any function or
© PCE Instruments 12
action assigned, then it is performed automatically upon clicking (e.g.
adjustment procedure), respectively a particular window with parameters or
list of appropriate settings is displayed.
7.2 Screen Scrolling
There are two methods for scrolling the screen of parameters window. The first
one requires pressing, holding down and scrolling up or down the scrollbar
located on the left. The second one requires pressing, holding down and
scrolling up or down any point of the displayed window.
7.3 Soft Keys List
Press to enter the main menu.
Press to scroll the menu ,,up”, or ,,down”.
Press to confirm changes.
Press to resign form introducing function modifications.
Press to add a new record to a database.
Press to print out a particular record from a database.
Press to clear the editing field.
Press to enable / disable an onscreen keyboard.
Press to export databases (key active upon plugging a pen drive). Press to
import databases (key active upon plugging a pen drive).
Press to select variables, out of the list, for a printout.
Press to delete database’s content.
7.4 Running Software Functions Quick access key
© PCE Instruments 13
Label:
Press to enter parameters setup. Press to enter tare value.
Text field with function assigned:
Press to develop an internal adjustment operation (internal adjustment function is assigned to the text field).
Functions selections pictogram:
CAUTION! For instruction on configuration of buttons, labels and text fields
refer to section 7.6 of this user manual.
© PCE Instruments 14
7.5 Return to Weighing Mode Introduced modifications are automatically saved in menu on return to the weighing mode.
Press
soft key repeatedly, keep Press soft key located on the balance
pressing the key until the balance home overlay for immediate display of a home
screen is displayed.
screen.
7.6 Buttons, Labels, and Text Field Configuration
Area beneath weight indication section can be freely programmed. It is divided
into active fields taking form of a table: 3 rows, 10 columns.
The division lines presented above are not visible on the balance screen, they
serve only for informative purposes.
This section is designed to comprise user-selected widgets: buttons, labels,
text fields, bar graphs:
– button pictogram to which a particular function is assigned, the function
is triggered upon pressing the pictogram;
– label field for information, its content is stable. The content depends on
displayed option, wherein the options change in course of balance operation.
The label may be active or passive. Active label, when pressed, triggers
function that is assigned to it, e.g. selecting product out of products
database. Passive label provides you with information on current state, no
function is assigned to it;
– text field – field for information, both content (text and variables of line
1 and 2) and function assigned to text field are programmable. The field may
be active or passive. Its operation is likewise as for label, the only
difference is that for the text field it is the user who specifies which
function is to be assigned to it. The function does not have to
© PCE Instruments 15
refer to displayed information, e.g. the text field displaying date and time
may trigger balance calibration upon being pressed; – bar graph option
available for Checkweighing and Dosing modes, field providing information on
Min and Max threshold – Checkweighing mode, and target weight Dosing mode, the
given information is presented in a graphic form, bar graph color informs
whether weight stays within the specified tolerance or is out of it. The
section may be set up freely in a way matching your needs. Each of the modes
may be configured independently. Set up rules: Widgets dimensions (width x
height) – button 1×1 – label 2×1; 3×1; 4×1; 5×1 – text field 2×1; 3×1;
4×1; 5×1; 6×1; 7×1; 8×1; 9×1; 10×1 – bargraph 5×1; 10×1 To quickly restore
the default widgets layout press the widget and hold it until a window with
available options displays. Select
– Always click extreme left side of a particular field that is to hold a
selected
– A new widget can only take such area that holds no other widgets yet. The
software automatically detects which widgets can be applied for a particular
area, this is conditioned by widget dimensions.
© PCE Instruments 16
– It is possible to change functions assigned to an already applied widget.
The applied widget, if not needed, can be removed.
– In order to rearrange widgets layout, it is necessary to delete already
applied widgets first, and define new arrangement of buttons, labels and text
fields next.
7.6.1 Quick Access Keys
You can define quick access underneath weight indication provides direct
access to the functions, it is selected from a
keys, the keys are displayed section. Quick access key most frequently operated list of available keys.
© PCE Instruments 17
1. Press and hold for a while the spot
where a given key is to be placed.
2. Select option: key 1×1
3. Enter particular key setup.
4. Select the key.
© PCE Instruments 18
5. The selected key is displayed
automatically on a home screen.
Quick access keys list:
Key
Function
Accept/Print
Print header
Print footer Zero Tare Set Tare Change Unit Select Unit Parameters Databases
User
Product Customer Packaging Adjustment Variable 1
Modes featuring the key All modes
Weighing mode exclusively Weighing mode exclusively All modes All modes All
modes Weighing mode exclusively Weighing mode exclusively All modes All modes
All modes
All modes All modes All modes All modes All modes
© PCE Instruments 19
Variable 2 Variable3 Working mode parameters Hide/show last digit Drying mode Drying profile Finish mode Printout interval and unit Open/close cover Start
All modes All modes All modes Weighing mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively
7.6.2 Labels You can select label size and type of information to be displayed
for a particular label. In order to select a particular label, use a list of
available labels. Upon label selection, specify type of information to be
displayed for the label. The selected label is displayed automatically on a
specified home screen spot.
Procedure:
Press and hold for a while the spot where a given label is to be placed.
Select a label and its size.
© PCE Instruments 20
Label settings window opens, click INFORMATION field in order to see a list of
information type available for the selected label.
Select data to be displayed.
The selected label is displayed automatically on a home screen.
Label information types: Label information type Date Time Date and Time Net Weight Tare Gross weight User Product Packaging Customer Variable 1 Variable 2 Variable 3 MSW value MSW status Drying mode Drying profile Finish mode Printout interval Temperature/drying time
Modes featuring the information All modes All modes All modes All modes All
modes All modes All modes All modes All modes All modes All modes All modes
Weighing mode exclusively Weighing mode exclusively Weighing mode exclusively
Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying
mode exclusively Drying mode exclusively
© PCE Instruments 21
Drying chamber status
Drying mode exclusively
The above presented information type has been designed for particular working modes. Detailed description for a given information type is provided within section overviewing a respective mode.
7.6.3 Text Fields You can select text field size and type of information to be
displayed in the first and the second line of the field, plus you can decide
on a function that is to be assigned to a particular text field. Upon
completed setup operation, the selected text field is displayed automatically
on a specified home screen spot.
Procedure:
Press and hold for a while the spot where a given key is to be placed.
Select text field and its size.
Text field settings window opens. Define particular text field parameters:
© PCE Instruments 22
Line 1: e.g. text
Line 2: e.g. variable {3}, variable for current time displaying (other
variables refer to point for non-standard printouts defining),
Function: e.g. adjustment.
When all text field parameters have been defined, the window displays
respective values.
The defined text field is displayed automatically on a home screen.
© PCE Instruments 23
7.6.4 Bargraphs Bargraph function is accessible for all weighing modes. The
bargraph presents in a graphic form how much of balance capacity is in use.
Additionally it shows Min and Max thresholds positions for Checkweighing mode,
and for Dosing mode it shows target weight value along with permissible
tolerance. You can select bargraph size and turn on/off
Press and hold for a while the spot where bargraph is to be placed.
Select bargraph and its size.
The selected bargraph is displayed automatically on a home screen.
© PCE Instruments 24
8 Weighing Operation
Load a weighed object on a balance weighing pan. On stabilization of weighing result, indicated
by stability marker
visible on the left side of balance display, read the measurement result.
Record / printout of the measurement result is available on pressing
– for verified balances only stable measurement result can be saved or printed (stability
marker
visible on balance’s display),
– for non-verified balances stable or unstable measurement result can be saved or
printed (regardless of stability marker
absence). If unstable measurement result
is printed then it is accompanied by question mark <?> in front of printed mass value.
8.1 Good Weighing Practice In order to ensure long lasting use of a moisture
analyzer plus correct and reliable measurement of weighed loads, follow below
procedures:
– Start the balance with no load on the weighing pan (permissible value of
load on the weighing pan on balance start is ±10% of its maximum capacity).
– Load the weighing pan steadily avoiding shocks:
– Place weighed loads centrally on the weighing pan: – Avoid side loading, in particular side shocks:
© PCE Instruments 25
8.2 Logging Full access to user parameters and to editing databases requires
logging as an operator with
First Log In operation – procedure:
Run home screen and press < > button, operator’s database window opens with
list of available users,
Select
Press button to confirm, home screen of the software is displayed again
automatically, When logged, add users and set the permissions levels (for the
procedure of assigning permissions levels go further down this user manual).
On future Logging In, select a user from the list and enter the password, the
software initiates operation with permissions level set for the selected user.
Log out operation procedure:
Run home screen and press < > button, operators database window opens, Press
Permissions levels
Balance software comprises three permissions levels: administrator, advanced operator, user.
Permissions level dependent access to edition of user parameters, databases and software functions:
Permissions levels User
Advanced User
Administrator
Enabled operations
Free editing of parameters of <Readout/Filter> submenu. Modification of
settings for <Misc.> parameter group, except for settings for
© PCE Instruments 26
8.3 Units
UNITS parameter group enables you to change availability of mass units (the
change can be performed in-course of balance operation), and to define two
custom units, thus positively effecting comfort and speed of operation. It is
possible to change unit to other than unit [g] during weighing process or
during operation of other modes.
8.4 Weighing Unit Selection Change of weighing unit is carried out by pressing the weighing unit icon visible next to the value
of measurement result, or by clicking
key (if displayed in an information section). Clicking
the unit triggers its replacement, the clicked unit is replaced with the unit that is next on the list of
available units.
Another option for unit replacement is selecting a particular unit out of the units list, to view the
list click
key (if displayed in an information section).
Unit
Denotation Verified Unit
balance
gram
[g]
Yes*
Taele Taiwan
milligram
[mg]
Yes*
Taele China
kilogram
[kg]
Yes*
Momme
carat
[ct]
Yes*
Grain
pound
[lb]
No
Newton
ounce
[oz]
No
Tical
ounce Troy
[ozt]
No
baht
pennyweight
[dwt]
No
tola
Taele Hongkong [tlh]
No
mesghal
Taele Singapuore [tls]
No
- – Accessibility of measuring units is conditioned by balance type.
Denotation
[tlt] [tlc] [mom] [gr] [N] [ti] [baht] [tola] [msg]
Verified balance No No No No No No No No No
8.5 Weighing Units Accessibility You may declare which units shall be
accessible while selecting a temporary unit by means of
key. Units with parameter value set to
Units with parameter value set to
© PCE Instruments 27
8.6 Start Unit Selection Upon selection of start unit, the balance activates
with the specified start unit for these modes where change of the unit is
possible. Ability of selecting a given unit depends on the balance status,
i.e. if the balance is verified or not.
8.7 User defined Unit You may declare two units. Displayed value of a user-
defined unit is a multiplication of measured mass value and a coefficient
specified for the particular user-defined unit. The units can be freely named
with use of 3 characters maximum. By default the names are displayed as [u1]
user unit 1, and [u2] user unit 2.
8.8 Balance Zeroing
In order to zero mass indication, press
button. Mass indication of zero value shall be
displayed together with precise zero
and stability
markers.
Zeroing process is an equivalent for determining new zero point, recognized by the balance as
precise zero. Zeroing is possible only for stable status of display indication.
CAUTION! Zeroing the display indication is possible only within ±2% range of
instrument’s maximum capacity. If the zeroed value is above ±2% of the maximum
capacity, then the software indicates
a respective error message.
© PCE Instruments 28
8.9 Balance Taring
In order to determine net weight of the object, place object’s container (packaging) on the
weighing pan, and on stabilization of measurement result press
key. The display indicates
mass equal zero and symbols: Net and
. On taking off the weighed load and its packaging
from the weighing pan, the display indicates sum of total tared mass with minus sign.
The software enables assigning tare value to a database-stored product. Using this option, the
software automatically uploads data on tare value for a particular product upon its selection from
the database.
CAUTION! Taring negative values is impossible. On taring negative values the balance responds with an error message. In such case, zero balance indication and repeat taring procedure.
Manual Tare Determination Procedure:
– While in optional mode press
quick access key,
An on-screen numeric keyboard is displayed,
Enter tare value and press key, The balance returns to the weighing mode, and
the display indicates entered tare value with minus
sign.
Deleting Tare The tare value indicated on balance display can be deleted by
pressing overlay, or by using programmable function key
key on balance
Procedure 1 – on taking the tared load off the weighing pan:
– Press
key.
The NET marker is deleted, and new zero point of the balance is determined.
Procedure 2 – with tared load on the weighing pan:
– Press
key.
The NET marker is deleted, and new zero point of the balance is determined.
When tare value exceeds 2% of the maximum capacity, respective message is
displayed in order to inform a user about the fact.
Selecting tare value out of PACKAGINGS DATABASE Procedure:
– While in optional mode, press display.
button located in a top left hand corner of the mass
Wait for a respective window to open, next select
sign. or
© PCE Instruments 29
– While in optional mode, press button (if displayed on the screen), Window
with a list of tare values recorded into tare database opens. Select the
packaging that is to be used. The balance returns to the weighing mode, and
the display indicates selected tare value with a minus
sign.
AUTOTARE function Autotare function provides automatic taring of the packaging during the weighing process when packaging mass for each of the product is different. For description of this function go further down this manual.
Deleting tare Entered tare value can be deleted by pressing value of 0.000g (see description above).
button on the overlay or by entering tare
8.10 Weighing Mode Settings
The software allows setup of operating parameters (filters, value release and
autozero function, deleting the last digit and other settings) separately for
each working mode. It enables customizing the instrument and utilizing its
properties depending on your needs and expectations, or on specific
requirements for selected working mode (e.g. DOSING); as a result the device
operation is quick and easy.
© PCE Instruments 30
Filter level setting Filter settings adjustment depends on the working
environment. For the best possible conditions the filter can work in a very
fast mode (V.FAST value for Filter parameter); however, if the conditions are
poor (shakes, drafts), the filter should be set to slow or very slow option
(SLOW or V. SLOW value for Filter parameter). The effectiveness of the filter
is different throughout the weighing range. The filter works slower when
“approaching” the weighed mass, it works more intensively for weighed mass
within the set range of the filter (parameter for setting filter range is
accessible only from the service menu the user does not have any access to
it). Depending on the filter, the weighing time is shorter (V.FAST and FAST)
or longer (SLOW and V. SLOW).
CAUTION! The higher filter level, the longer weighing time.
Value release Since ambient conditions at a workplace vary, it is necessary to
determine the value release parameter in the most preferable way enabling
balance adaptation, parameter options are: FAST.+REL., FAST or RELIABLE.
Depending on the selected option, weighing time is either shorter or longer.
Autozero function The software features an autozero function (Auto) ensuring
precise mass indication. This function automatically controls and corrects
zero indication. When Autozero is enabled, it compares balance indications at
declared time interval e.g. 1s, provided that weighing pan is unloaded and
display indication is close to zero. If results vary less than declared
AUTOZERO range e.g. one division, balance zeroes automatically, marker of
stable measurement result , and precise zero marker are displayed. If
AUTOZERO function is enabled, then each weighing process starts from precise
zero point. There are, however, some cases when this function can be a
disturbing factor for the measuring process; e.g. very slow placing of a load
on the weighing pan (load adding). Here, zero indication correction can also
correct actual indication of loaded mass.
Last digit display Function enables displaying the last digit of decimal place
for a weighing result. There are three available options:
– Always: all digits visible, – Never: last digit is not displayed, – When
stable: last digit is displayed only for a stable weighing result.
Balance ambient conditions Parameter relating to ambient and environmental
conditions in which the balance operates. There are two options:
8.11 Proximity Sensors The balance features two proximity sensors enabling
touch-free balance control. The software detects two motions performed around
the sensors:
– Hand in a close vicinity to the left sensor
Each motion can trigger optional balance function. For available functions
list go to section 7.6.1. Upon completed configuration procedure, the software
runs function assigned to a particular proximity sensor having detected motion
around it. To provide correct operation, it is necessary to set the right
proximity sensors sensitivity (for more information go to section 9).
8.12 AUTOTARE Autotare is used for quick determination of net weight for loads
with different tare values, wherein they are measured one after another. When
the function is active (
– Make sure that the weighing pan is empty and press button responsible for
zeroing, Put product packaging on a weighing pan (packaging weight value must
be greater than set AUTO THRESH value), After measurement stabilization,
automatic taring of the packaging mass proceeds (Net marker appears in the
upper part of the display), Put product that is to be packed into the
packaging; The display shows net weight of the product; Take off the product
together with the packaging;
The balance cancels tare value (packaging weight recorded in balance storage
during the first step of the operating process) after the gross mass value
(set in
For correct operation of the balance with AUTOTARE function it is necessary to
adjust the threshold value.
8.13 Print Mode
Function designed to enable print mode setting, it activates key. Print mode
options:
–
parameter
the result is not stable (no
marker on a display), the balance software sends the
measurement result to the port after reaching stability for the measurement.
–
CAUTION! Each result is printed and recorded (stable and unstable for a non- verified balance, stable for a verified balance). Automatic operation with interval starts at the moment of switching the function on and it lasts until it is switched off. The first stable weighing result of value greater than AUTO THRES value is printed as a first measuremnt. The following measurements are printed with frequency set in INTERVAL parameter. Automatic operation with interval stops when the option is off. On switching the function of auto print with interval, PRINT button becomes inoperative (no indication is printed when pressed).
Automatic operation procedure:
– Press
button to zero the balance (marker of stable measurement
and zero
marker
are shown on a display),
Deposit load, the balance sends the first stable measurement to the printer port,
Remove the load from the pan,
Next measurement is possible when the indication is lower than the set value
of
For automatic operation adjust the threshold value. The measurement will not
be send from the computer to the printer as long as the mass measurement stays
within the set value range
© PCE Instruments 33
8.14 Minimum Sample Weight
Weighing mode comprises
CAUTION! This function is valid for weighing mode exclusively.
Options: – MODE None minimum sample weight function off Block select to
make the balance display respective pictograms informing on mass (whether it
is out-of-tolerance low or out-of-tolerance high); with this option on, the
software disables confirmation of the measurement that is out-of-tolerance low
Warn select to make the balance display respective pictograms informing on
mass (whether it is out-of-tolerance low or out-of-tolerance high); with this
option on, the software enables confirmation of the measurement that is out-
of-tolerance low – Tare maximum tare value for which minimum sample weight
value is obligatory (read examples below) – Minimum mass minimum sample
weight determined for particular balance on site using respective method.
Example 1 for balance with d=0.0001 g:
No. Tara value 2 10.0000 g
Minimum Sample Weight 1.0000 g
Operation
Minimum sample weight refers to all net weights subjected to weighing in a
tare container of mass 0,0001g 9,9999g inclusive (
Example no. 2 for balance with d=0.0001 g:
© PCE Instruments 34
No. Tara value 1 220.0000 g
Minimum Sample Weight 0.5000 g
Operation
Minimum sample weight refers to all net weights subjected to weighing in a
tare container of mass covered by full weighing range (
Example no. 3 for balance with d=0.0001 g:
No. Tara value Minimum Operation
Sample
Weight
1 0.0000 g
0.2500 g Minimum sample weight refers to all net weights subjected
to weighing where no tare container is used (
not used). The program identifies setting specifying that
minimum sample weight is valid exclusively for samples not
weighed in a tare container. If taring function is used, then
pictogram informing on use of minimum sample weight goes
blank.
As a user you can preview entered data, but you are not allowed to edit it.
Weighing with use of
Procedure (Administrator exclusively): 1. Enter weighing mode settings, 2.
Press
Block select to make the balance display respective pictograms informing on
mass (whether it is out-of-tolerance low or out-of-tolerance high); with this
option on, the software disables confirmation of the measurement that is out-
of-tolerance low, Warn select to make the balance display respective
pictograms informing on mass (whether it is out-of-tolerance low or out-of-
tolerance high); with this option on, the software enables confirmation of the
measurement that is out-of-tolerance low. 5. Select respective option and
return to the home screen, 6. Section presenting the weighing result comprises
additional pictogram providing supplementary information. The pictogram
changes in course of weighing operation informing you on the weighed sample
mass with reference to declared minimum sample weight value
© PCE Instruments 35
Weight value lower than minimum sample Weight value higher than minimum sample
weight specified for a particular tare range. weight specified for a
particular tare range. Pictograms for minimum sample weight:
Weight value lower than specified minimum sample weight. Weight value higher
than or equal to specified minimum sample weight.
CAUTION! If more than one reference tare value has been programmed (along with
min load values assigned to them) then indicated value automatically turns to
range respective for tare container weight. Requested minimum load changes
simultaneously. 8.15 Cooperation with TITRATORS In order to provide correct
cooperation with Titrators, go to settings of standard printout content and
set
With
© PCE Instruments 36
9 Miscellaneous
A user can set up parameters which influence balance operation. These
parameters are to be found in parameters group MISC. Settings modification for
particular parameters of this parameter group proceeds likewise as described
in section 7 of this user manual.
Menu language Language parameter enables selecting the language of the balance
menu descriptions for unlogged user. Available languages: POLISH, ENGLISH,
RUSSIAN, UKRAINIAN, HUNGARIAN, SPANISH, FRENCH, GERMAN, ITALIAN, CZECH,
CHINESE, ARABIC, TURKISH, KOREAN. In order to change menu default language for
unlogged user select new language (Setup/Misc./Language) and restart the
balance.
Permissions Permissions parameter enables choosing access level for a
particular user, one that is not logged in. Available access levels: ADMIN. /
USER. / ADV. Depending on selected permissions level, you can enter balance
parameters and modify the settings, as far as possible for a particular level.
Logging in operation is not required (for permissions overview go to section 9
of this user manual).
,,Beep” sound reaction to operation of pressing a key Sound parameter
enables switching on/off a `beep’ sound responsible for informing a user about
pressing any key of balance overlay or display, or about proximity sensors
response.
Procedure:
© PCE Instruments 37
Backlight and adjusting display brightness Display brightness parameter
enables setting the brightness of the backlight or switching off the display
brightness completely.
Proximity sensors sensitivity adjustment Proximity sensors sensitivity
parameter specifies distance within which the sensors can be operated, its
scale is expressed in percent and it ranges from 0% to 100%. For lower percent
value the proximity sensors operate at a shorter distance. Procedure:
Date Date parameter enables setting the current date. Procedure:
© PCE Instruments 38
Time Time parameter enables setting the current time. Procedures for change of
time settings and date settings are likewise. letter is displayed next to
presented time value, where: A stands for hours before noon; P stands for
hours after noon. AM and PM will be printed near to the time. 10 Adjustment In order to ensure the highest weighing accuracy, it is recommended to
periodically introduce a corrective factor of indications to balance memory,
the said factor must be referred to a mass standard. In other words, balance
adjustment shall be performed from time to time. Adjustment should be carried out: – Before the beginning of weighing
procedure, – If long breaks between following measuring series occur, – If
temperature inside the balance changes more than: 2°C. Adjustment type: Adjustment with an external weight of declared mass which
cannot be modified or of any mass, but not lower than 30% of maximum range. CAUTION! Remember to carry out the adjustment process when there is no load on
the pan! When the weighing pan is loaded, command be aborted if necessary by pressing button at any time during the process. 10.1 External Adjustment © PCE Instruments 40 10.3 Report Printout Adjustment report is generated automatically at the end
of each adjustment process or adjustment test and next it is sent to
communication port assigned for PERIPHERAL DEVICES/PRINTER (by default it is
COM1). Report content is declared in PRINTOUTS/ADJUSTMENT REPORT menu.
Instruction on how to declare settings for this option is to be found further
down this manual, read sections referring to printouts. The report can be
printed using balance-connected printer or sent to a computer and saved for
archiving purposes as a file. Step 2. Assemble in the drying pan the components of temperature adjustment
kit: Press key to confirm, the second step of adjustment starts. The moisture
analyzer halogen lamp starts to operate and the drying chamber is heated as
long as necessary to provide specified temperature, which is next maintained
for 8 minutes. After 8 minutes a numeric keyboard is displayed. Enter the
moisture analyzer temperature that is displayed on the control thermometer. 10.5 Drying Process Test In order to test the drying chamber and the drying
process you need to use a special adjustment set (thermometer and the
thermometer holder). The set is an optional accessory of a moisture analyzer
(the same that is used for temperature adjustment of the drying chamber). For
information on how to assemble the set go to Temperature adjustment section. Upon confirmation of serial number START message is displayed. Press key to confirm. The drying process starts and continues until specified temperature is reached. Time and sensor temperature information is displayed. The temperature is maintained for 8 minutes (like for temperature adjustment
procedure). After 8 minutes you shall see a window for entering temperature
read from the installed adjustment set. Press The result of the test may be printed on a printer connected to the balance.
Look left to see an example of a report. © PCE Instruments 44 11 Determining Printout Content 11.1 Adjustment Report Variable PROJECT Overview Option enables naming the project (name associated with a particular
type of weighing). The name may consist of maximum 31 characters. Option
enables printing out the type of the adjustment being carried out. Option
enables printing out the name of a logged-in user. Option enables printing out
the name of the project (see parameter Project). Option enables printing out
the date of the carried out adjustment. Option enables printing out the time
of the carried out adjustment. Option enables printing out the balance ID
number. Option enables printing out the difference between mass of an
adjustment weight measured during the last adjustment and the current measured
mass of this weight. Option enables printing out dashes that separate the date
of a printout from a signature. Option enables providing an area for the
signature of a user performing the adjustment. Procedure for naming the project: An exemplary report: For the parameters described above, one of these values
must be selected: NO – do not print YES – print 11.2 Drying Process Report Printout Group of parameters enabling user to
declare data that is to be printed on a Drying Process Report printout. The
Drying Process Report is divided into three individually customized sections:
the header, the measurement, the footer. The settings are valid for Drying
Process mode exclusively. Printout variables list: Variable DATE Overview Option enables printing out the date of drying process start Option
enables printing out the time of drying process start Option enables printing
out the balance type. Option enables printing out the balance ID number.
Option enables printing out the name of a logged-in user. Option enables
printing out the name of a currently selected product. Option enables printing
out the name of a currently selected drying mode. Option enables printing out
the drying parameters with accordance to which the sample is to be dried.
Option enables printing out the value of VARIABLE 1. Option enables printing
out the value of VARIABLE 2. Option enables printing out the value of VARIABLE
3. Option enables printing out net weight value in a basic unit (calibration
unit). Option enables printing out an empty separating line. Active for: Header Header Header Header Header Header Header Header Header
Header Header Header Header Footer GLP printout GLP printout GLP printout GLP
printout GLP printout GLP printout GLP printout © PCE Instruments 47 INDICATION SIGNATURE NSTR.PRNT. Option enables printing out the final indication of the drying process. Option
enables providing an area for the signature of a user performing the
measurement. Option enables printing out one of 100 non-standard printouts on
the footer printout. You can choose one of the following options: NONE / non-
standard printout name. The way of entering non-standard printouts is
described further down this user manual. Footer For the parameters described above, one of these values must be selected: NO – do not print YES print CAUTION! For exemplary printout of a report go to section 19 of this user
manual. 11.3 Other Printouts GLP PRINTOUT Group of parameters enabling to declare data that is to be
printed on a measurement result printout. FOOTER Group of parameters enabling to declare data that is to be printed on a
footer printout. © PCE Instruments 48 Printout variables list: Variable WORKING MODE BALANCE TYPE BALANCE ID USER Overview Option enables printing out the name of a working mode. Active for Header Footer Header Footer Header Footer Header GLP printout
Footer Header GLP printout Footer Header GLP printout Footer GLP printout © PCE Instruments 49 DASHES EMPTY LINE SIGNATURE NSTD.PRNT. adjustment report printout (for more information go to section 10.1 of this
user manual. Option enables printing out separating dashes. Footer For the parameters described above, one of these values must be selected: NO – do not print YES – print Exemplary printouts: HEADER GLP Printout FOOTER © PCE Instruments 50 11.4 Non-standard Printouts The balance software enables entering 100 non-
standard printouts. Each of them can consist of approximately 1900 characters. 11.4.1 Inserting Texts Variables list: Symbol {0} 1) {1} 1) {2} {3} {4} {5} {6} {7} {8} {9} Description Standard printout in a calibration unit Standard printout in a
current unit Date Time Date and time Working mode Net weight in a current unit
Net weight in a calibration unit Gross weight in a calibration unit Tare in a
calibration unit {10} Current unit {11} Calibration unit {12} Min threshold {13} Max threshold {32} Factory no. {45} Target value {46} Tolerance {50} Product: Name {51} Product: Code {52} Product: EAN code {53} Product: Mass {54} Product: Tare {56} Product: Minimum {57} Product: Maximum {66} Product: Tolerance {70} Variable 1 {70} Variable 2 {72} Variable 3 © PCE Instruments 51 {75} User: Name {76} User: Code {77} User: Access level {80} Packaging: Name {81} Packaging: Code {82} Packaging: Mass {85} Customer: Name {86} Customer: Code {87} Customer: VAT no. {88} Customer: Address {89} Customer: Postal code {90} Customer: City {146} {147} Gross weight in current unit Tare weight in current unit {150} {151} Form feed for PCL printers Paper crop for EPSON printers {155} Cooperation with CONECT PC software {275} {276} {277} {278} {280} {281} {284} Ambient conditions readout date and time THB: Temperature THB: Humidity
Internal sensor: Temperature 1 THB: Pressure Air density THB: Temperature from
an additional sensor {380} {381} Drying mode: Name Drying mode: Code {385} Drying profile {386} Drying profile parameters {387} Finish mode {388} Finish mode parameters {389} Report from drying process: Unit {390} Report from drying process: Printout interval {395} Moisture analyzer: Set temperature {396} Moisture analyzer: Current temperature {397} Moisture analyzer: Drying time {398} Moisture analyzer: Status {399} Moisture analyzer: Drying time and result {400} Moisture analyzer: Humidity content {401} Moisture analyzer: Dry mass content {402} Moisture analyzer: Humid/Dry CAUTION! © PCE Instruments 52 Every single printout can contain max 1900 characters (letters, numerals, non-
standard characters, spaces). A user can apply non-standard characters
depending on type of data that is to be printed out. An example: “PCE” DATE: Exemplary settings: 12 Working Modes General Information 12.2 Running Working Mode To run working mode other than currently operated
one: – wait for the available working modes list to be displayed, – select the
working mode you need to operate. 13 Databases Balance software features the following databases < : – Products (5 000 products) – Users (100 users) – Packaging (100 packaging types) – Customers (1 000 customers) – Drying modes (200 drying modes) – Drying reports (5000 reports) – Ambient Conditions (10 000 records) – Weighings (50 000 records) CAUTION! It is not possible to edit some of the databases for a balance
cooperating with E2R software. Shall you introduce any modifications on
databases, use the PC software. © PCE Instruments 56 13.1 Database Connected Operations ADD NEW RECORD EXPORT – Insert USB flash drive. Open the database that is to be exported. The program automatically saves exported data to a pendrive file, respective
prompts are displayed for confirmation of successfully completed operation.
The name of a file depends on the database. Database Operators database Products database Packaging database Customers
database Drying modes database Non-standard printouts File name and extension users.x2 products.x2 packaging.x2 customers.x2
programs.x2 non_standard_printouts.x2 IMPORT – Save the file with database content that is to be imported to a flash drive.
Only files exported from other balance that had proper names and extensions
can be imported see table above. Insert USB flash drive. Enter database that
is to be imported. DELETE A RECORD – Press the record and hold it. A message: Press < to confirm, the record is deleted from the list. © PCE Instruments 57 DELETE A DATABASE – Enter selected database and press (Delete everything) pictogram located in
the top bar. A message: Press < to confirm, the database is deleted. DRYING REPORTS and WEIGHING REPORTS cannot be imported. DRYING REPORTS
database cannot be deleted. AMBIENT CONDITIONS database serves informative purposes only. Using records
preview option you can check ambient conditions and observe how they changed
over time. The data 13.2 Products Product database stores names of all products that can be
weighed, counted, controlled. List of parameters defined for a product: 1. Name [product name] 2. Code [product code] 3. EAN [EAN code for a product] 4. Mass [nominal mass/single product mass] 5. Tare [tare value, set automatically when the product is selected out of the database] 6. Min [low limit for product weighing in CHECKWEIGHING mode] 7. Max [high limit for product weighing in CHECKWEIGHING mode] 8. Tolerance [% value calculated in relation to mass, the parameter
determines measuring area for which the measurement is recognized as correct for DOSING mode.] CAUTION! Remember to assign product to particular mode, as some of data values
are adopted to the particular mode functions, e.g. mass in © PCE Instruments 58 13.3 Users User’s database features list of operators permissioned to operate
the balance. 13.7 Drying Process Reports Reports on drying process database stores
information on carried out drying processes. Each report can be previewed and
printed. Procedure: 13.9 Weighing Records Each measurement result sent from a balance to a printer
or a computer is saved in the database of weighing records. Balance user can
preview data from each weighing record. Optimum temperature and drying time depend on sample type and size, and
anticipated measuring accuracy. Selection of drying parameters can only be
carried out on basis of test measurements. Liquid substances It refers to liquid substances, which by creation of drops
on their surface, caused by surface tension, may render difficulties in drying
process. In such cases, it is proved to use a glass fibre filter to shorten
measurement time. The filter causes separating tested liquid around the
fibres, and increasing active evaporating surface. Initial filter drying is
necessary only in case of measurements which require very high accuracy. 15 Selection of Drying Parameters 15.2 Influence of Sample Weight on Measurement Result Repeatability Sample weight ~2g ~10 g Repeatability ±0.05% ±0.01% The above data refers to a model, uniform sample, containing no moisture due
to the evaporation process and showing no signs of decomposition (e.g. wet
high-silica sand). The results uncertainty cannot be avoided, this is due to sample nature and
moisture analyzer repeatability. In practice, it means that obtained
measurement result may exceed repeatability values provided above. 15.3 Drying Temperature Drying temperature has the largest impact on drying
time. Temperature value depends on type of dried substance. Too low drying
temperature causes too low moisture content evaporation (underdried sample),
and consequently unnecessary extending of measurement time. Too high drying
temperature causes burning of dried sample (sample overheating, chemical
decomposition). Drying temperature of traditional method (using a furnace) is
specified in applicable industry or company standards. Unless standards apply,
then temperature should be adjusted by tests. FAST profile Fast profile is recommended to drying samples that moisture
content varies from 5%, and 15%. In the initial stage of Fast profile, heating
takes place at full power of the filaments, causing heating the drying chamber
to increased temperature (maximum temperature value is higher by 30% from set
drying temperature). Overheating compensates heat loss during evaporation of
large moisture content in the test’s initial stage. Defined finish mode – user defined criterion. The operator determines the
limit value for loss of mass and time in which the loss of mass must not
exceed a pre-set value. As the moisture analyzer reaches the set criterion it
automatically finishes the measurement (drying process). – User defined 1 (m
change of mass and t change of time must be given, the former in mg, the
later amounts to 120 s. maximally) – User defined 2 (set moisture content
change ratio %M over time 60s) Info field provides the following information: – Product – Drying program –
Drying profile and drying temperature value – Finish mode – Printout
parameters – Info field displaying (in the course of drying) time and drying
temperature values – Info field displaying chamber status – Buttons:
parameters, user, drying program, open/close cover, drying mode settings,
start, databases 17 Drying Process Performed by Means of Quick Menu Drying process mode parameter takes the following values: 17.2 Automatic Finish Mode %R – humid / dry ratio obtained as a result of drying process, expressed in
percent, measurement result is part of mass that evaporated from the dried
sample during drying process 17.4 Printout interval 19 Drying Process Drying process settings are displayed in the information field above the
buttons. © PCE Instruments 73 Place the disposable weighing pan in a pan handle and deposit it on a bracket.
The display shows disposable pan weight. It is recommended to close the drying
chamber in order to provide stable ambient conditions while taring, to do it
press pictogram (to be found at the bottom of the screen). On sample preparation and result stabilization press key to confirm sample preparation completion. Drying chamber’s lid gets closed automatically, the drying process starts. You can close the drying chamber by pressing pictogram (to be found at the bottom of the screen), this also triggers the drying process start. Information on the drying process is displayed, moisture analyzer proceeds to carrying it out accordingly to set parameters. Required mass measurements and calculations of tested sample moisture content are performed, wherein the calculations are a result of mass change. On process start, printout header is sent to a selected interface (accordingly to set printout options parameter group DRYING PROCESS REPORT/HEADER). In course of a drying process current weight results and information on the process is displayed (test duration, drying chamber temperature, etc.). In course of a drying process (accordingly to set printout options parameter group DRYING PROCESS REPORT/MEASUREMENT) measurements are sent to a selected communication port in a preset time intervals (INTERVAL). © PCE Instruments 75 key allows you to swap between displayed result type during the process. Drying process may be aborted at any time. In order to abort the process,
press key and confirm completion by pressing key. Manual auto switch-off mode is an
exception to the rule for moisture analyzer working in this mode, the drying process ends upon pressing key, there is no need to confirm completion by pressing key. Report on drying is printed again by pressing key located in the bottom bar of
the display. Report is also automatically saved in moisture analyzer’s memory
in the drying reports database. In order to return to the main screen of drying process settings press key located in the bottom bar of the display. Moisture analyzer returns to its initial state,
completed process summary is blanked. The moisture analyzer is ready to perform another test. An example of drying report: © PCE Instruments 76 19.1 End Result Prognosis This option enables estimating end result before
drying process is completed. Based on characteristics of current drying curve,
created online, moisture analyzer estimates the end result of drying process.
It is an approximate result characterized with small error (about +/- 10% of
the end result for most of the products and +/- 20% for products that require
drying process to be longer such as: plastics, gels and materials containing
more than 30% of water). This option is useful for users who need faster
estimation of the drying process end result. The time of the prognosis process
ranges between 15% and 40% of the standard drying time. 1. Enable prognosis option in accordance with the following instructions: the display. On pressing this button, a window with prognosis is displayed. In
the initial stage of the drying process there is no result of prognosis yet
and the 6. If the result of prognosis meets your expectations, you can abort the
drying process before its completion. To do that, return to home screen and press button. © PCE Instruments 79 7. On drying process completion a footer of drying report containing status,
end result and estimated result are printed. The estimated result is a result
that would be achieved on reaching the criteria set by the user for a given
process. An exemplary report from drying process containing prognosis result: 20 Communication 20.1 RS-232 Port Settings Procedure: 20.2 Ethernet Port Settings Procedure: Select < – Ethernet> communication port, next set appropriate values: DHCP – Yes No IP
Address – 192.168.0.2 Subnet mask – 255.255.255.0 Default gate – 192.168.0.1 CAUTION! The above presented settings serve information purposes only.
Transmission parameters should be selected in accordance with the settings of
customer’s local network. Return to weighing mode and restart the device. © PCE Instruments 81 20.3 Wi-Fi Port Settings Pictogram for Wi-Fi network connection status: No. Pictogram Overview Balance connected, very strong signal Balance connected, strong signal Balance connected, poor signal Balance connected, very poor signal No connection (too poor signal or inaccessible selected network or invalid connection parameters password, IP, etc.) Exemplary settings for Wi-Fi port: CAUTION! The above presented settings serve information purposes only. Make
sure that your transmission parameters are accordant for your local network
settings. Procedure: – Select Select network of your choice. Password window is displayed, enter the
password using an on-screen keyboard. Press button to go one level up, informing on the fact that the balance tries to connect the network, For successfully established connection status, respective pictogram is displayed (see pictogram overview above) If it takes too long to establish connection it may be concluded that
connection parameters are Read User Manual Online (PDF format) >>
Date format Date form. parameter enables altering the date format on the
printout [YYYY.MM.DD / YYYY.DD.MM / DD.MM.YYYY / MM.DD.YYYY], where: YYYY
year; MM month; DD day.
Time format Time form. parameter enables specifying time format for a printout
[12h / 24h]. For [12h] option selected, or
Backlight turn-off time
Auto switch-off
© PCE Instruments 39
External adjustment is carried out by means of an external mass standard of
specified accuracy class and weight. The process takes semi-automatic form,
successive stages are signalled with prompts.
Procedure: Enter
Take the weight off the weighing pan and press button. Whereas balance
determines start mass, “Adjustment; Please wait…” prompt is displayed, Upon
completed start mass determination procedure <Put weight …> prompt is
displayed along with particular mass standard value.
Put the required weigh on a pan and press button, Upon completed procedure
“Remove weight” prompt is displayed. Take the weight off the weighing pan,
wait for
10.2 User Adjustment
User adjustment is carried out with an optional standard of mass ranging
between 0,3 Max and Max. User adjustment and external adjustment procedures
are likewise with one exception, before user adjustment start, a message box
for entering mass of a standard used for user adjustment is opened. In order
to start user adjustment, enter
10.4 Temperature Adjustment Temperature adjustment is carried out with a
dedicated kit, which is an optional equipment of the moisture analyzer MA_X.
1. Thermometer 2. Thermometer holder and drying chamber shield
Adjustment of the drying chamber temperature is a process carried out for the
purpose of adjusting the temperature sensor assembled inside the drying
chamber of a moisture analyzer. Before starting temperature adjustment
process, place the temperature calibration kit inside the drying chamber,
following below diagrams:
Step 1. Remove from the drying chamber the following:
– disposable pan – drying pan handle – cross-shaped holder – drying chamber
insert
© PCE Instruments 41
– drying chamber shield – thermometer holder and – the thermometer
Step 3. After assembling the kit start temperature adjustment process.
CAUTION! All the activities must be carried out with great caution not to
damage the measuring mechanism of the moisture analyzer. Go to menu
Press key to confirm, the third step of adjustment starts. The moisture
analyzer halogen lamp starts to operate and the drying chamber is heated as
long as necessary to provide specified temperature, which is next maintained
for 8 minutes. After 8 minutes a numeric keyboard is displayed. Enter the
moisture analyzer temperature that is displayed on the control thermometer.
Press key to confirm. Temperature adjustment process is completed and moisture
analyzer displays
© PCE Instruments 43
Procedure: – Set test parameters in accordance with instruction below and the
displayed prompts. – Enter ADJUSTMENT menu and start
Enter: – testing temperature – permissible error – serial number of the
temperature
adjustment set
to confirm.
ADJUSTMENT REPORT is a group of parameters enabling to declare data that is to
be printed on an adjustment printout.
CALIB TYPE USER PROJECT DATE TIME BALANCE ID CAL. DIFFER
DASHES
SIGNATURE
© PCE Instruments 45
HEADER Group of parameters enabling to declare data that is to be printed on a
header printout.
MEASUREMENT Group of parameters enabling to declare data that is to be printed
on a drying process result printout.
FOOTER Group of parameters enabling to declare data that is to be printed on a
footer printout.
© PCE Instruments 46
TIME
BALANCE TYPE BALANCE ID USER
PRODUCT
PROGRAM
DRY.PARAM.
VARIABLE 1 VARIABLE 2 VARIABLE 3 START MASS
EMPTY LINE
TIME
INDICATION
DRYING TIME AND INDICATION NET
TARE
GROSS
SET TEMPERATURE
CURRENT TEMPERATURE
STATUS
END DATE
END TIME
DRYING TIME
END MASS
Option enables printing out the drying time with preset interval during drying
process. Option enables printing out the drying process indication with preset
interval during drying process. Option enables printing out time and
indication with preset interval during drying process. Option enables printing
out net weight value with preset interval during drying process. Option
enables printing out tare value with preset interval during drying process.
Option enables printing out gross weight value with preset interval during
drying process. Option enables printing out temperature set in a particular
stage of the drying process with preset interval during the process. Option
enables printing out current temperature read from the sensor with preset
interval during drying process. Option enables printing out the status of
drying process summary (Completed/Aborted). Option enables printing out the
end date of the drying process. Option enables printing out the end time of
the drying process. Option enables printing out the total time of the drying
process. Option enables printing out the end mass of the tested sample.
GLP printout
Footer Footer Footer Footer Footer
Footer
Header Footer
HEADER Group of parameters enabling to declare data that is to be printed on a
header printout.
PRODUCT
CUSTOMER
PACKAGING DATE
TIME
VARIABLE 1
VARIABLE 2
VARIABLE 3
NET
TARE GROSS CURR.RES. MSW WEIGHT MSW TARE MASS FOR TRITATOR ADJUSTMENT REPORT
Option enables printing out the balance type.
Option enables printing out the balance ID number.
Option enables printing out the name of a logged-in user.
Option enables printing out the name of a currently selected product.
Option enables printing out the name of a currently selected customer.
Option enables printing out the name of a currently selected packaging. Option
enables printing out the date of the carried out adjustment.
Option enables printing out the time of the printout.
Option enables printing out the value of VARIABLE 1.
Option enables printing out the value of VARIABLE 2.
Option enables printing out the value of VARIABLE 3.
Option enables printing out net weight value in a basic unit (calibration
unit).
Option enables printing out the tare value in the current unit. Option enables
printing out the gross mass value in the current unit. Option enables printing
out the current measurement result (NET weight) in a current unit. Option
enables printing out the minimum sample weight value declared for a balance.
Option enables printing out the tare value for minimum sample weight. Option
enables printing out the net mass set for correct cooperation with titrators.
Option enables printing out the report of the last adjustment in accordance
with the settings declared for
Header GLP printout Footer Header GLP printout Footer Header GLP printout
Footer Header GLP printout Footer Header GLP printout Footer Header GLP
printout Footer GLP printout
GLP printout
GLP printout
GLP printout
GLP printout
GLP printout
Header GLP printout
Option enables printing out an empty separating line.
Option enables providing an area for the signature of a user performing the
adjustment. Option enables printing out one of 100 non-standard printouts on
the footer printout. You can choose one of the following options: NONE / non-
standard printout name. The way of entering non-standard printouts is
described further down this user manual.
Header Footer Header Footer Footer
Header GLP printout Footer
Non-standard printout may include: – variables dependent on the working mode
and other needs (mass, date etc.) – permanent text from the user menu.
Non-standard printout can have approximately 1900 characters.
Means for inserting texts – by an on-screen keyboard – by a computer keyboard
of USB type
A computer keyboard of USB type can be connected to a balance, this enables
easier and quicker editing of the printouts. Willing to insert any text, it is
necessary to select a respective menu option and, using the keyboard, type the
text. 11.5 Variables Variable is defined as alphanumeric data which can be
linked to printouts, products or other information related to weighing. Every
variable is characterized by its content, the content must be given. Variables
are used for entering various data during the weighing process, e.g. serial
number or batch number. The program allows to enter 3 variables. Each can
consist of max 31 characters. In order to insert a variable content, you need
to enter variable settings (VARIABLE 1, VARIABLE 2, VARIABLE 3) and enter the
respective values using direction keys (arrows) on the balance keypad or a
computer keyboard. Procedure for entering texts is the same as for non-
standard printouts.
© PCE Instruments 54
Standard version of MA_X balance feature the following working modes: Weighing
Means of operation: weight of a load is determined through an indirect
measurement. A balance measures gravitational force which attracts the load.
An obtained result is processed to a digital format and displayed in a form of
measurement result. Drying Means of operation: determining moisture content in
a sample, obtained by vaporization of all moisture components from a sample
placed inside a drying chamber of a moisture analyzer. A measurement result is
automatically calculated by the software and visualized on an ongoing basis on
moisture analyzer’s display by comparing mass of a sample on measurement
start, in progress, and at the end of drying process.
Particular working modes settings feature specific functions. The functions
enable adapting mode operation to your individual needs. The special settings
are activated on selecting a respective profile. A detailed description of
specific functions is provided within description of working modes.
12.1 Working Modes Accessibility Group of parameters enabling you to declare
which functions are to be accessible. You can deactivate functions that are
not used in course of balance operation, to do it, value
© PCE Instruments 55
– press pictogram of currently used working mode, the pictogram is located in
the top left hand corner,
12.3 Parameters Related to a Working Mode Each working mode has programmable
parameters determining its functioning. Read point 9 of this user manual for
description of possible settings for WEIGHING working mode. Settings for
DRYING working mode are specified within its description.
The program enables the user with appropriate access level to carry out the
following operations: adding new record, exporting data from databases,
importing data to databases, deleting one record from the database, deleting
all records from database, printing data saved in a record.
– Enter a database and press (Add) button located in the top bar. Define
fields for the new record (data content depends on the database). On returning
to the databases window a new record is displayed on the list.
Press icon located in the top bar.
Press icon located in the top bar. The program automatically reads the file
and the data is imported to the balance. Respective prompts are displayed for
confirmation of successfully completed operation.
saved to records can be printed by pressing pictogram located in the top bar.
Records’ names contain date and time of saving the record’s data to balance
memory.
List of parameters defined for a user: 1. Name 2. Code 3. Password 4.
Permissions level 5. Language
13.4 Packaging List of used packaging with parameters such as name, code and
weight value specified. When carrying out weighing process, upon selection of
particular packaging, a respective tare value is operated automatically. The
tare value is displayed with minus sign.
List of parameters defined for packaging: 1. Name 2. Code [internal code
providing packaging identification] 3. Tare [packaging weight] 13.5 Customers
Customer’s database features a list of names of customers for whom the
measurements are carried out.
List of parameters defined for a customer: 1. Name 2. Code [internal code
providing customer identification] 3. NIP 4. Address 5. Postal code 6. City
13.6 Drying Program Database of drying programs contains saved data on drying
parameters which are activated to dry a product.
List of parameters defined for drying mode: 1. Name 2. Code 3. Drying profile
4. Finish mode 5. Printouts 6. Sample mass control
© PCE Instruments 59
– Enter < Databases> submenu, press
Information provided by the Drying Process Report: 1. User 2. Drying mode 3.
Start date 4. End date 5. Drying time 6. Status 7. End mass 8. Drying status
9. Indication
13.8 Ambient Conditions Ambient Conditions database comprises ambient
conditions related information. Depending on the setup, the ambient conditions
record may comprise data such as temperature, humidity, atmospheric pressure.
When the THB module is connected to the balance then its indications are
recorded to the database too. Procedure:
– Enter < Databases> submenu, press
CAUTION! The software saves ambient conditions record in a so called loop,
i.e. when the measurement 10 001 is saved, the measurement 1 is automatically
deleted from the balance’s memory. Records saved to balance memory cannot be
deleted.
© PCE Instruments 60
Procedure:
– Enter < Databases> submenu. Enter
Information defined for a weighing record: 1. Measurement date 2. Measurement
time 3. Measurement result 4. Weight 5. Tare value 6. User 7. Product name 8.
Customer, Customer name 9. Packaging, tare name applied during product
measurement 10. Working mode name 11. Variable 1 12. Variable 2 13. Variable 3
14 Sample Preparation for Drying
This section of the MA_X user manual contains data on setting optimum test
results during drying processes. There are hints for selection of appropriate
drying parameters for various materials and substances.
14.1 Means of Moisture Content Measurement on a Moisture Analyzer Measurement
of moisture content in a tested sample is carried out by determining loss of
mass in a sample by its heating (humidity evaporation). PCE moisture analyzer
MA_X comprises two components: a precision balance and a drying chamber.
Compared to standard moisture content determining methods, the measurements
with application of PCE moisture analyzer is much quicker and does not require
additional mathematical calculations (a result of moisture content is
previewed on an ongoing basis during product testing process). Independently
on moisture content determining method, the measurement accuracy is highly
influenced by means of sample preparation and selection of testing parameters,
such as:
– Sample size – Sample type – Drying temperature – Drying time
In practice, the measurement accuracy is not as important as the speed of
obtaining measurement result (control over technological process). Thus,
heating a sample (with application of a halogen filament) carried out by a
moisture analyzer, makes the measurement process very time efficient and
short. Measurement speed can be additionally increased by appropriate
adjusting moisture analyzer’s parameters depending on tested substances.
© PCE Instruments 61
14.2 Sampling and Preparation Sample features, its preparation and size are
very important factors influencing the speed and accuracy of measurement
process. Means of sampling and preparation are extremely important for
repeatability of measurement results, as a sample should be a representative
part of tested substance.
Final measurement result is vastly conditioned by precise and considered
sample preparation. A sample used for analysis has to represent the total
structure of tested material. Sampling process should determine: sampling
means, sample disintegrating, particle size after disintegration, sample
uniformity and other. The sampling process should be carried out as quickly as
possible, so that a sample does not lose or absorb humidity from surrounding
area. Applied sampling standards should match individual user needs and
requirements of tested material, its consistence and sample size.
Number of samples Increasing number of tested samples also increases statistic
measurement certainty. Number of samples depends on uniformity of tested
material, its purity, accuracy of applied measuring method and anticipated
accuracy of obtained results.
Material mechanical disintegrating for measurements Applied disintegrating
method should be selected appropriately to tested material. Substances that
are hard and brittle (crisp) can be disintegrated by cutting. Grinding such
substances may cause their heating and thus humidity vaporization, resulting
in unreliable measurement results. Unless a substance can be prepared for
measurement otherwise than grinding, any possible moisture content loss should
be calculated.
Use of high-silica sand Ensuring optimum substance drying requires that a
sample has the largest possible surface for moisture content evaporation. Test
results of moisture content for substance with surface in a form of a shell
(e.g. glucose syrup) or doughy (e.g. butter), can be much more reliable if a
sample is mixed with a dried high-silica sand (improvement of measurement
accuracy and repeatability). While using mixture, disposable weighing pan with
extended brim must be applied (greater volume of a sample).
Grease in a form of paste or melting substances Such substance requires
testing with use of a filter made of glass fibre, which considerably increases
active evaporation surface by separating the substance between the fibre.
Initial filter drying is necessary only in case of measurements which require
very high accuracy.
© PCE Instruments 62
Substances with structure of leather or temperature sensitive In case of such
substances it is proved to use a glass fibre filter. While testing, a
substance is placed on a drying pan, and sample surface is covered with a
filter, which protects the sample from direct heat radiation. In such case,
the sample is heated by convection (which is milder than radiation).
Substances containing sugar The surface of such substances often may
caramelize during testing procedure. Therefore, it is recommended to use thin
layer of a sample, and moderate drying temperature.
Sample distribution on a pan:
Loose materials Dried in their natural state, i.e. in their natural form or
disintegrated. Sample disintegration causes smaller dispersion between the
following measurements. Sample mass should not be too high, and the sample
should be evenly spread on whole surface of the drying pan.
Liquid substances Semi-fluid substances are dried in their natural form. Large
amount of grease (fat) occurring in some of substances makes moisture content
determination difficult. In such case it is recommended to use additional
components, which increase sample’s active surface and aid moisture content
releasing process from a sample. Such components are high silica sand,
blotting paper or filter. Before drying a tested substance, initially dry the
additional component, so that its humidity is close to zero.
Solid objects Depending on solid object’s structure (dense or loose), moisture
content determining process may take short or long time. The size of solid’s
surface determines the speed of drying process, and measurement reliability.
Thus, the surface of a solid object should be as large as possible. Since
solid objects release moisture through their outer surface, sample thickness
is another important factor.
© PCE Instruments 63
15.1 Selecting Optimum Mass for a Sample Sample mass influences the accuracy
of measurement result and measurement time. Higher mass of a sample, causes
higher amount of water (moisture content) which needs to evaporate, and
therefore measurement time is also longer. Obtaining short measurement time is
feasible in case of small sample mass, but sample mass cannot be too small, as
it may negatively influence required measurement accuracy.
Sample mass considerably influences repeatability of measurement results
obtained on a moisture analyzer. Relation between sample mass and
repeatability is presented in a table below.
© PCE Instruments 64
On selecting drying temperature value, proceed as follows: – Determine
moisture content in a sample – Determine temperature of substance chemical
decomposition by tests – Compare result obtained on a moisture analyzer with
the one of traditional method
When drying a sample with high moisture content, it is possible to shorten
measurement time by selecting quick or step drying mode. In such case, the
majority of moisture content is released drying temperature higher than set.
Only after some time, the temperature is lowered to the set value, and
maintained until completing drying process.
15.4 Selecting Drying Profile The software of moisture analyzer enables
selecting one of four drying profiles:
– Standard – Quick – Mild – Step
STANDARD profile Standard profile is the most frequently used of all drying
profiles. It enables accurate determining of moisture content in a dried
sample.
MILD profile Mild profile is used in case of drying substances that are
sensitive to rapid heat emitted by filaments operating at full power in the
initial stage of drying process. This profile prevents from decomposing of
substances sensitive to heat by mild temperature increase in set amount of
time (time interval has to be selected by tests). Mild profile is recommended
to drying samples of leather structure.
© PCE Instruments 65
STEP profile Enables determining up to three steps with random drying
temperature. Step profile is recommended for drying substances with moisture
content over 15%. Temperature and heating time in each step have to be
adjusted by tests.
15.5 Drying Time Drying time is set by selecting one of available finish mode
criteria. This means that a moisture analyzer must meet pre-set criterion (one
of the requirements: mass over time, time) to automatically finish the drying
process. Finish of drying process can be triggered by amount of time,
independently on loss in mass. This criterion is used for substances that may
decompose during drying process, and their mass does not reach constant value.
The second criterion is loss in mass (less than 1 mg) in defined amount of
time.
Automatic finish mode (Auto switch off mode) The operator can choose between
various types of finish modes:
– Automatic 1 (change 1mg/10s) – Automatic 2 (change 1mg/25s) – Automatic 3
(change 1mg/60s) – Automatic 4 (change 1mg/90s) – Automatic 5 (change
1mg/120s)
Time-defined finish mode – drying process finish takes place on elapsing a set
amount of time, independently on measurement result (maximum drying time 99
hours 59 minutes).
Manual finish mode – the operator ends drying process manually by pressing
START/STOP soft key on moisture analyzer’s display.
© PCE Instruments 66
15.6 Drying Profile Analysis For the first case, the drying profile is an
asymptote. Moisture content value remains constant even after long drying
time. Using this drying profile makes determination of humidity easy. The
measurement result is always referred to constant value of asymptote. The
result corresponds easily and it is not difficult to select a proper criterion
of finish mode. For the second case the drying process is quick at the
beginning, next it stabilizes. Moisture content value is never constant.
Drying process profile may proceed as follows: The sample undergoes thermal
decomposition, wherein evaporation takes place and as a result the product
weigh decreases. Evaporation of grease, oil, plastic or other volatile
materials may take much more time than in case of water. Difficult to
evaporate materials drop weight. Result obtained using this mode may be
optimistic:
– Lower temperature may slower material reaction. – Selection of appropriate
criterion may let the user recognize end of analysis, within
described drying step. – Constant drying often assures good drying results. –
Maintaining start sample weight permanently (+10%….+20%).
16 Drying
DRYING mode has been designed to enable determination of moisture content of a
given sample. The moisture content value is obtained via evaporation of
moisture from sample placed inside of the drying chamber. The result is
calculated automatically (and displayed) in real time, the calculation is made
on the basis of sample mass at the beginning, in the course, and at the end of
the process.
Procedure for activation of Drying mode: – Select
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16.1 Mode Related Settings The supplementary settings enable you to adjust the
working mode to your needs and requirements. Drying profile Parameter enabling
you to select respective drying profile and set drying temperature. Finish
mode Parameter enabling you to select respective finish mode and set its
parameters. Printout parameters Parameter enabling you to set the drying
process unit for both the display and the printout, and measurement result
printout interval during drying.
Prognosis Parameter enabling to turn on/off result prognosis function.
Close the cover and turn the moisture analyzer off Parameter enabling you to
activate/deactivate auto opening/closing of the drying chamber’s lid upon
switching the moisture analyzer off by pressing button.
For means of operation of the remaining functions read point 8.11 WEIGHING
Mode Settings.
16.2 Drying Quick Access Key Each working mode features automatically
displayed set of default keys. The set can be modified by assigning out-of-
list quick access keys to the on-screen buttons. Such operation requires
particular permissions level. List of quick access keys it to be found in
section 7.6 of this user manual.
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Default display configuration in drying mode. Current drying parameters are
displayed in a form of pictograms in the middle of the information field.
Willing to perform the procedure in accordance with other parameters, enter
the settings and modify the respective parameters values. Enter drying process
menu, set the following parameters:
– Drying process mode and drying process parameters, – Drying process finish
mode and finish mode parameters – Unit for a displayed and printed result –
Interval for measurement printout, wherein the measurements are printed during
the
drying process 17.1 Drying Process Profile and Drying Parameters
Enter drying parameters settings and select mode type. Upon selection fields
enabling setting profile parameters are displayed. Parameters depend on
selected mode.
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– STANDARD drying profile For standard profile set drying temperature in which
a sample is to be tested.
– FAST drying profile For quick profile, set both, heating time in a
temperature higher than the preset one and temperature for which a sample is
to be tested.
Specific feature of this drying profile is fast increase of drying temperature
in short period of time. When compared to the preset temperature, the drying
temperature rises 30% within 180 seconds and it is maintained at this level
for a specified amount of time, next it drops to temperature value preset in
drying profile parameters.
CAUTION! For Fast profile set the drying temperature and heating time 30%
higher than set temperature. Heating time is measured since reaching the set
temperature.
– MILD drying profile For mild profile, set length of time within which
moisture analyzer is to reach specified temperature and temperature for which
a sample is to be tested.
– STEP drying profile For step profile, set heating time in temperature number
one, first step temperature, heating time in temperature number two, second
step temperature and temperature in which a sample is to be tested.
CAUTION! For Step profile, set step temperature ,,1″ and ,,2″ and temperature
of drying, set also time heating time in particular indirect temperatures (1
and 2). Time for heating in particular steps is counted from the moment of
reaching a preset temperature for a particular step.
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Automatic finish mode (Auto switch off mode) takes the following values:
Automatic 1 – auto switch-off (mass change of 1mg / within time length of 10s)
Automatic 2 – auto switch-off (mass change of 1mg / within time length of 25s)
Automatic 3 – auto switch-off (mass change of 1mg / within time length of 60s)
Automatic 4 – auto switch-off (mass change of 1mg / within time length of 90s)
Automatic 5 – auto switch-off (mass change of 1mg / within time length of
120s) Manual Manual switch-off (on pressing Start/Stop button, maximum drying
time is 99 hours and 59 minutes, when drying takes this long or longer the
drying process is finished automatically) Time-defined time-defined switch-off
(maximum drying time is 99 hours 59 minutes) Defined 1 defined switch-off
(change of mass comprised within the balance range, set with moisture analyzer
readability, time interval ranging from 1 to 120s) Defined 2 defined switch-
off (change in humidity set with moisture analyzer readability, time interval
ranging from 1 to 60s).
17.3 Unit of Displayed and Printed Measurement
g – mass change, measurement result is mass change recorded during drying
process, %M – percent loss of weight, displays weight change recorded during
drying process expressed in percent, %D – part of dry mass obtained during
drying process, expressed in percent, measurement result is part of mass that
is remaining on a drying pan after humidity content evaporation,
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The time interval between printouts in seconds ranging from 0 to 120.
18 Drying Process Performed with Use of Drying Modes Database
Moisture analyzer can record up to 200 drying modes that may be freely
configured, recorded and used. Procedure selecting a mode:
– Insert the mode to moisture analyzer’s memory (read section 13 Databases) –
Select inserted mode prior drying process. Drying parameters update to
parameters
saved in selected drying mode.
Or: Insert data related to product/sample that is to be dried. Set the
inserted mode as drying mode (read section 13 Databases). Select inserted
product as a current one prior drying process. Drying parameters update to
parameters saved in the drying mode that is assigned to a selected product.
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Press Start button in order to run the drying process. If the drying chamber’s
lid is closed, it gets opened automatically Prompts and messages are displayed
making moisture analyzer operation easier. Follow the prompts to correctly
prepare the sample and to perform the process of humidity content
determination for a tested sample.
Program prompts you to prepare a weighing pan. A respective pictogram on
drying chamber status is displayed.
Press key to zero the weighing pan weight.
Indication equals ZERO, drying chamber’s lid gets opened automatically,
subsequent prompt is displayed and the pictogram on drying chamber status
changes.
Deposit sample on a weighing pan. Sample weight shall be selected on the basis
of prior experience and tested material characteristics.
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Upon drying process completion, summary of the test is displayed, final
moisture content result is held, drying chamber’s lid gets opened
automatically. Printout footer is sent to a selected interface (accordingly to
set printout options parameter group DRYING PROCESS REPORT/FOOTER).
CAUTION: Do not open the weighing chamber during drying process while using
prognosis option. It may distract the process and the calculations would be
incorrect. Prognosis is finished when the drying chamber is opened and a
suitable message is displayed.
Prior drying process using prognosis option, set the following parameters.
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2. In accordance with description in point 8.6.2., place the label with
displayed prognosis on the home screen.
3. If the prognosis is to be printed with the measurement, enable its
printing in the following settings: PRINTOUTS/REPORT FROM DRYING
PROCESS/MEASUREMENT/PROGNOSIS.
4. On setting the above parameters you can start drying process by following
the above description. On starting the drying process an additional button is
displayed in the bottom part of
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5. When the intersection of the drying curve is found, the end result can be
estimated. When calculated, it is displayed in the prognosis label.
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COMMUNICATION menu is comprised within Parameters menu. It is accessed by
pressing key. The balance can communicate with a peripheral device, wherein
the communication is established via the following ports:
– COM 1 (RS232), – USB 1 type A, – USB 2 type B, – Ethernet, – Wi-Fi.
The ports can be configured using
press key, next press “Communication” key.
– Select communication port
The RS 232 ports enable the following setting of transmission parameters: –
Baud rate – 2400, 4800, 9600, 19200, 38400, 57600, 115200 bit/s – Parity –
None, Even, Odd
CAUTION! 1. Make sure that transmission parameters are accordant for your
local network settings, 2. For correct communication via Wi-Fi, set port
parameter for computer to
Balance equipped with Wi-Fi module features a respective pictogram at the home
screen in the top right-hand corner:
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Enter
With DHCP set to NO value, enter manually:
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