PCE Instruments PCE-MA 50X Moisture Analyzer User Manual

June 9, 2024
PCE Instruments

PCE-MA 50X Moisture Analyzer

Englis h

User Manual
PCE-MA 50X Moisture Analyzer
User manuals in various languages (français, italiano, español, português, nederlands, türk, polski,
, ) can be found by using our product search on: www.pce-instruments.com
Last change: 23 October 2018 v1.0
© PCE Instruments

Contents 1 General Safety Precautions ……………………………………………………….. 1
1.1 Warning Symbols and Signals……………………………………………………………………………… 1 1.2 Precautions ………………………………………………………………………………………………………. 1 1.3 Intended Use…………………………………………………………………………………………………….. 3 1.4 Contact Conditions…………………………………………………………………………………………… 3 1.5 Precautions ………………………………………………………………………………………………………. 3 1.6 Warranty ………………………………………………………………………………………………………….. 4 1.7 Supervision over Metrological Parameters …………………………………………………………….. 4 1.8 User Manual Significance……………………………………………………………………………………. 4 1.9 Staff Competence ……………………………………………………………………………………………… 4 1.10 Protective Clothing …………………………………………………………………………………………….. 4
2 Transport and Storage ………………………………………………………………. 5
2.1 Delivery Checklist………………………………………………………………………………………………. 5 2.2 Package…………………………………………………………………………………………………………… 5
3 Unpacking and Installation ………………………………………………………… 5
3.1 Place of Use and Assembling………………………………………………………………………………. 5 3.2 Unpacking ………………………………………………………………………………………………………… 5 3.3 Balance Level Setting…………………………………………………………………………………………. 6 3.4 Standard Delivery Components List ……………………………………………………………………… 6 3.5 Maintenance Activities………………………………………………………………………………………… 7 3.6 Powering the Device ………………………………………………………………………………………….. 8 3.7 Temperature Stabilization Time……………………………………………………………………………. 9 3.8 Connecting Additional Hardware ………………………………………………………………………….. 9
4 Start-Up …………………………………………………………………………………….. 9 5 Keyboard ­ Buttons functions……………………………………………………. 9 6 Weighing Mode Home Screen ………………………………………………….. 10
6.1 Weighing Window ……………………………………………………………………………………………..10 6.2 Drying Window ………………………………………………………………………………………………….11
7 Balance Menu ………………………………………………………………………….. 12
7.1 Entering Balance Menu ………………………………………………………………………………………12
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7.2 Screen Scrolling ………………………………………………………………………………………………..13 7.3 Soft Keys List ……………………………………………………………………………………………………13 7.4 Running Software Functions ……………………………………………………………………………….13 7.5 Return to Weighing Mode……………………………………………………………………………………15 7.6 Buttons, Labels, and Text Field Configuration ………………………………………………………..15
8 Weighing Operation …………………………………………………………………. 25
8.1 Good Weighing Practice……………………………………………………………………………………..25 8.2 Logging ……………………………………………………………………………………………………………26 8.3 Units………………………………………………………………………………………………………………..27 8.4 Weighing Unit Selection ……………………………………………………………………………………..27 8.5 Weighing Units Accessibility………………………………………………………………………………..27 8.6 Start Unit Selection ……………………………………………………………………………………………28 8.7 User defined Unit ………………………………………………………………………………………………28 8.8 Balance Zeroing ………………………………………………………………………………………………..28 8.9 Balance Taring ………………………………………………………………………………………………….29 8.10 Weighing Mode Settings …………………………………………………………………………………….30 8.11 Proximity Sensors ……………………………………………………………………………………………..32 8.12 AUTOTARE ……………………………………………………………………………………………………..32 8.13 Print Mode………………………………………………………………………………………………………..33 8.14 Minimum Sample Weight…………………………………………………………………………………….34 8.15 Cooperation with TITRATORS …………………………………………………………………………….36
9 Miscellaneous………………………………………………………………………….. 37 10 Adjustment ……………………………………………………………………………… 40
10.1 External Adjustment …………………………………………………………………………………………..40 10.2 User Adjustment………………………………………………………………………………………………..40 10.3 Report Printout ………………………………………………………………………………………………….41 10.4 Temperature Adjustment …………………………………………………………………………………….41 10.5 Drying Process Test …………………………………………………………………………………………..44
11 Determining Printout Content…………………………………………………… 45
11.1 Adjustment Report …………………………………………………………………………………………….45 11.2 Drying Process Report Printout ……………………………………………………………………………46 11.3 Other Printouts ………………………………………………………………………………………………….48 11.4 Non-standard Printouts ………………………………………………………………………………………51
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11.5 Variables ………………………………………………………………………………………………………….54
12 Working Modes ­ General Information ……………………………………… 55
12.1 Working Modes Accessibility ……………………………………………………………………………….55 12.2 Running Working Mode………………………………………………………………………………………56 12.3 Parameters Related to a Working Mode ………………………………………………………………..56
13 Databases ……………………………………………………………………………….. 56
13.1 Database Connected Operations …………………………………………………………………………57 13.2 Products…………………………………………………………………………………………………………..58 13.3 Users ………………………………………………………………………………………………………………59 13.4 Packaging ………………………………………………………………………………………………………..59 13.5 Customers………………………………………………………………………………………………………..59 13.6 Drying Program …………………………………………………………………………………………………59 13.7 Drying Process Reports ……………………………………………………………………………………..60 13.8 Ambient Conditions ……………………………………………………………………………………………60 13.9 Weighing Records……………………………………………………………………………………………..61
14 Sample Preparation for Drying …………………………………………………. 61
14.1 Means of Moisture Content Measurement on a Moisture Analyzer …………………………….61 14.2 Sampling and Preparation …………………………………………………………………………………..62
15 Selection of Drying Parameters………………………………………………… 64
15.1 Selecting Optimum Mass for a Sample………………………………………………………………….64 15.2 Influence of Sample Weight on Measurement Result Repeatability ……………………………64 15.3 Drying Temperature …………………………………………………………………………………………..65 15.4 Selecting Drying Profile ………………………………………………………………………………………65 15.5 Drying Time………………………………………………………………………………………………………66 15.6 Drying Profile Analysis ……………………………………………………………………………………….67
16 Drying ……………………………………………………………………………………… 67
16.1 Mode Related Settings ……………………………………………………………………………………….68 16.2 Drying ­ Quick Access Key …………………………………………………………………………………68
17 Drying Process Performed by Means of Quick Menu ………………… 69
17.1 Drying Process Profile and Drying Parameters……………………………………………………….69 17.2 Automatic Finish Mode ……………………………………………………………………………………….71 17.3 Unit of Displayed and Printed Measurement…………………………………………………………..71
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17.4 Printout interval …………………………………………………………………………………………………72
18 Drying Process Performed with Use of Drying Modes Database .. 72 19 Drying Process ………………………………………………………………………… 73
19.1 End Result Prognosis…………………………………………………………………………………………77
20 Communication ……………………………………………………………………….. 81
20.1 RS-232 Port Settings………………………………………………………………………………………….81 20.2 Ethernet Port Settings ………………………………………………………………………………………..81 20.3 Wi-Fi Port Settings …………………………………………………………………………………………….82 20.4 USB Ports ………………………………………………………………………………………………………..85
21 Peripherals………………………………………………………………………………. 88
21.1 Computer …………………………………………………………………………………………………………88 21.2 Printer ……………………………………………………………………………………………………………..90 21.3 USB flash drive …………………………………………………………………………………………………93 21.4 Barcode reader …………………………………………………………………………………………………94 21.5 Ambient Conditions Module…………………………………………………………………………………94
22 Ambient conditions………………………………………………………………….. 95 23 Communication Protocol …………………………………………………………. 97
23.1 List of commands ………………………………………………………………………………………………97 23.2 Response format……………………………………………………………………………………………….98 23.3 Manual Printout / Automatic Printout …………………………………………………………………..112
24 Peripherals…………………………………………………………………………….. 113 25 Error Messages ……………………………………………………………………… 113 26 Use of Moisture Analyzer ……………………………………………………….. 114 27 Maintenance Activities …………………………………………………………… 114
27.1 Cleaning Moisture Analyzer Components…………………………………………………………….115 27.2 Cleaning Temperature Sensor……………………………………………………………………………115 27.3 Troubleshooting ………………………………………………………………………………………………115
28 Additional Equipment …………………………………………………………….. 116 29 Information on Moister Analyzer …………………………………………….. 116 30 Warranty………………………………………………………………………………… 117 31 Disposal ………………………………………………………………………………… 117
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1 General Safety Precautions

1.1 Warning Symbols and Signals
Safety precautions are marked with special descriptions and warning signs. They inform and warn a user of possible dangers. Ignoring the safety warnings may cause injuries, damage of the moisture analyzer, its inappropriate operation and errors of measurements.

1.1.1

Warning Descriptions

WARNING

Medium risk danger that can lead to a serious injury or death.

CAUTION

Low risk danger that can lead to moisture analyzer damage or dysfunction, loss of data or minor or moderate injury.

NOTE

Critical information on the moisture analyzer.

1.1.2 Warning Symbols

Electric shock Acid / Corrosion Potential danger Flammable or explosive substances Toxic substances Hot surface

1.2 Precautions
WARNING! Adherence to safety information and user manual guidelines is required in order to prevent risk of health damage and even death.
WARNING: Nominal voltage for a moisture analyzer is 230V AC or 115V AC. It means that safety usage precautions for low voltage devices must be abided by while operating the device. The moisture analyzer is equipped with a three- core power supply cable with grounding pin. If necessary, an extension cord can be used provided that it meets the applicable standards and has a protective ground conductor. Intended disconnection of the grounding cable is forbidden.

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CAUTION: Drying chamber cannot be opened during operation (drying process). It is due to the fact that a halogen lamp and its glass shield may reach the temperature of up to 400° C. When setting up the moisture analyzer leave enough space to prevent heat from building up and to keep your analyzer from overheating. Leave about 20 cm around the instrument and about 1 m above. Air vents that are located in the housing cannot be covered, sealed or blocked in any other way. Do not put any flammable substances on, under or near the moisture analyzer. Be particularly careful when removing the sample from the drying chamber: the sample itself, the drying chamber, shields and the pan can still be extremely hot. In case of any maintenance work (cleaning the inside of the drying chamber), the moisture analyzer must be switched off. Wait until all the components have cooled down. Do not perform any modification to the heating module.
Some types of samples require taking particular safety precautions. They can pose a danger for people and objects. It is always the user who is liable for possible damages caused by the use of an inappropriate sample.
CAUTION: Corrosion: substances that release aggressive vapours (e.g. acids) during the heating process. While drying such substances it is recommended to work with small samples. Otherwise, vapours can condense on cold housing parts and cause corrosion.
WARNING: Fire or explosion: flammable or explosive substances, substances containing solvents or releasing flammable or explosive gases or vapours. When in doubt as for the sample’s characteristics perform risk analysis before carrying out the procedure. For the said type of samples, apply as low drying temperatures as possible, thus preventing flames or explosion. During the analysis it is necessary to wear protective glasses and gloves. The samples should be relatively small. Under no circumstances can the instrument be left unsupervised!
WARNING: Substances containing toxic and caustic or corrosive components: substances that release toxic gases or vapours can cause irritations (eyes, skin or respiratory system), illnesses or even death. Dry such substances only in fume cupboards.
Under no circumstances should the instrument be used within an explosion endangered area. The moisture analyzer is designed to be operated outside hazardous areas exclusively.
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1.3 Intended Use
Moisture analyzer is designed to verify relative moisture content in small samples of various substances, dry mass content in small samples and mass of weighed objects. The device ensures fast and precise process of determination of water content in a tested sample whereas application of touch screen display considerably simplifies operation and improves functionality of the moisture analyzer. The device can be used to determine humidity content of different materials. At the initial stage of the measurement, the moisture analyzer precisely determines mass of an object placed on a weighing pan. As the mass reading is stabilized, the sample is quickly heated by a halogen lamp, an IR emitter or a metal heater causing humidity evaporation from the tested sample. While sampling, the moisture analyzer is continuously checking loss of mass, and on calculation, it displays current moisture content of a tested sample. Compared to conventional methods of humidity content determination of various substances, application of moisture analyzer considerably shortens measurement time and simplifies testing procedure. Moisture analyzer facilitates setting multiple parameters which influence the procedure of moisture content determination in a sample (temperature, time, drying modes, etc.).

1.4 Warranty Conditions

CAUTION!

Do not open the drying chamber during the drying process. The moisture analyzer features a

halogen lamp which is a very powerful heat source. Pay special attention not to touch those

elements of a moisture analyzer that get hot while the drying procedure (i.e.: disposable pan, pan

handle, and inner shields of the drying chamber).

Remember that some tested samples may become dangerous when heated (emission of

poisoning vapours, danger of ignition or explosion).

The moisture analyzer is not intended for dynamic weighing. Even if small amounts of a sample

are added to or taken off the weighing pan, the mass readout should be taken only on stabilization

of the measurement result (appearance of stability pictogram

on the display).

Do not place any magnetic materials on the weighing pan, as this can cause damage of the

measuring system of the instrument.

Be sure to avoid impact shock and overloading of the moisture analyzer in excess of the

prescribed maximum measuring range (max capacity), minus any possible tare weight that has

been applied).

Never use the moisture analyzer in an environment endangered by an explosion!

This moisture analyzer is not adjusted for operation in explosive areas. Remember that it is

forbidden to make any modification to the moisture analyzer.

1.5 Precautions
PCE moisture analyzer adheres to all binding safety regulations. Nevertheless there are exceptional circumstances that may cause danger. Do not open the instrument’s housing. Inside there are no parts that would require maintenance, repair or replacement carried out by a user. In case of any problems, contact PCE service or a distributor. Remember to use the device in accordance with this user manual, especially to follow instructions on installation and configuration of a new device. Since use of the moisture analyzer conversely to safety precautions and user manual guidelines may be hazardous to operator’s health and life, it is obligatory to read them carefully:

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– Use the moisture analyzer to determine humidity content in samples and to determine mass of a tested sample; any other use of the moisture analyzer may be dangerous both to the device and the user,
– Before commissioning the moisture analyzer, make sure that the nominal power of the device specified on its data plate is compatible with the supply in the mains to which the moisture analyzer is to be plugged in,
– Halogen lamps can only be changed by an authorized service employee, – Protect moisture analyzer against contacts with liquids, it might lead to electrocution,
fire, emission of substances containing toxic or caustic vapour, emission of explosive substances.
1.6 Warranty Warranty does not cover the following cases:
– not observing the user manual regulations, – using the moisture analyzer conversely to its intended use, – any modifications of a moisture analyzer or cases when its housing has been opened
(damaged protective stickers), – mechanical defects and defects caused by media, liquids, water and natural wearing
off, – inappropriate working environment or electrical installations defects, – and overloading of measuring mechanism.
1.7 Supervision over Metrological Parameters Metrological parameters of a moisture analyzer need to be checked by a user in determined time intervals. Inspection frequency is conditioned by ambient conditions in which a moisture analyzer is used, kind of carried out processes and adopted quality management system.
1.8 User Manual Significance It is very important to read the user manual carefully before switching on and starting up moisture analyzer operation, even if you are experienced and have worked with this type of balance before.
1.9 Staff Competence The moisture analyzer should be utilized and supervised only by users who are trained and experienced in such type of instruments. In order to use the moisture analyzer, first read the user manual. Keep these instructions for the future reference. Do not make any design modifications. Additional equipment compatible with the moisture analyzer and spare parts should be supplied by PCE or an authorized distributor.
1.10 Protective Clothing While working with the instrument use protective clothing, this is to take safety precautions against potential hazards source of which might be tested samples and ingredients. Use the following while carrying out tests:
– protective apron, – protective glasses, – protective gloves (while working with hazardous chemical substances).
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Before the use of the above-mentioned protective clothing, make sure that it has been designed to be used with specific samples and that it is not damaged.
2 Transport and Storage
2.1 Delivery Checklist Upon delivery it is necessary to check the package, make sure that your package bears no signs of damage.
2.2 Package Keep all package elements should your device be transported in the future. Remember that only original packaging can be used for shipping purposes. Prior packing uncouple any cables, remove any separable components (weighing pan, shields, inserts). The device components shall be packed into an original packaging, thus being protected against potential damage during transportation.
3 Unpacking and Installation
3.1 Place of Use and Assembling – Store and use your moisture analyzer in locations free of vibrations and shakes, and free of air movement and dust, make sure that it is located at the max altitude of 2000 above sea level. – Make sure that the moisture analyzer’s workplace ensures good air circulation around the instrument (approximately 20 cm free space around the moisture analyzer and 1 m free space over it). – Pay attention to the ambient air temperature in the weighing room, it should not be out of the specified range, i.e. +10 °C – +40 °C. – Make sure that the moisture analyzer is placed away from heat sources on a stable wall console desk or on a stable table which is not affected by vibrations. – Since part of the balance is a strong magnet take special safety measures when weighing magnetic objects.
3.2 Unpacking Carefully take the device out of the packaging, remove the transport lock and gently place the moisture analyzer at its workplace. Install the weighing pan and accessories following the diagram below:
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Accessories installation:
Install: – Drying chamber base insert (1), – Anti-draft chamber (2), – Pan handle (3), – Cross-shaped holder (4), – Disposable pan (5).

Positioning the bracket:

When installing the cross-shaped holder (pan supporter) pay special attention to the correct positioning of its mandrel. The mandrel features a cut providing unique positioning of the holder against the pan handle, thus preventing their contact and friction.
Setting the cross-shaped holder: – assemble the holder onto the mandrel and turn it slightly so that the mandrel cuts are located in their unique and correct position, – CAUTION: turn the mandrel gently so as not to damage moisture analyzer’s measuring system.

3.3 Balance Level Setting It is necessary to level the balance prior connecting it to the mains. To level the balance turn its feet until an air bubble takes central position.
3.4 Standard Delivery Components List – Moisture analyzer, – Drying chamber base insert, – Drying pan shield,
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– Drying pan handle, – Cross-shaped holder, – Disposable pan, – Power cord, – User manual ­ CD version.
3.5 Maintenance Activities Disassembly a weighing pan and other detachable components (the components differ depending on a balance type ­ see Unpacking and Installation section). Be careful while detaching the components so as not to cause any damages to the balance mechanism. In order to ease cleaning of glass anti-draft chamber panes, it is permissible to remove them following the below instruction.
CAUTION! Cleaning anti-draft chamber while still installed may cause damage of the measuring system. Cleaning ABS components:
To clean dry surfaces and avoid smutching use clean non-coloring cloths made of cellulose or cotton. You can use a solution of water and detergent (soap, dishwashing detergent, glass cleaner). Gently rub the cleaned surface and let it dry. Repeat cleaning process if needed.
In the case when contamination is hard to remove, e.g. adhesive, rubber, resin, polyurethane foam residues etc., you can use a special cleaning agents based on a mixture of aliphatic hydrocarbons that do not dissolve plastics. Before using the cleanser for all surfaces we recommend carrying out tests. Do not use products containing abrasive substances.
Cleaning anti-draft chamber panes:
Select dissolvent depending on a dirt. Never soak the glass panes in alkaline solutions since they interact with glass and may cause damage. Do not use abrasive substances.
For organic dirt use acetone first, next use water or detergent. For other than organic dirt use diluted acid solutions (soluble salts of hydrochloric or nitric acid) or base solutions (ammonium or sodium base).
To remove ACIDS use protofilic solvent (sodium carbonate), to remove BASE use protogenic solvent (mineral acid of various concentration).
In case of heavy contamination use brush or detergent nevertheless avoid detergents containing large and hard molecules which could potentially scratch glass panes.
Use soft brush with wooden or plastic handle exclusively to avoid risk of scratches. Do not use wire brush.
At the end of the cleaning process rinse the pane using running water first, distilled next.
Rinsing is a necessary cleaning process stage allowing to remove remaining soap, detergents and other cleansers from the panes prior their reinstallation.
Avoid drying the panes either using paper towel or forced air circulation since some fibres, grains or contamination of other type could permeate into the panes thus causing weighing errors.
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One shall not use driers when drying measuring glass tools.
It is a frequent treatment to leave glass components on a rack to dry.
Cleaning stainless steel components:
Avoid using cleansers containing any corrosive chemicals, e.g. bleach (containing chlorine). Do not use abrasive substances. Always remove the dirt using microfiber cloth to avoid damage of protective coating.
In case of a daily maintenance: 1. Remove the dirt using cloth dipped in warm water. 2. For best results, add a little dishwashing detergent.

Cleaning powder-coated components:
For preliminary cleaning stage you need running water or wet sponge featuring large holes, this will help you to remove loose, heavy dirt.
Do not use cleansers containing abrasive substances.
Next using cloth and cleanser-water solution (soap, dishwashing liquid) gently rub the cleaned surface.
Avoid using cleanser without water since it may result with damage of the cleaned surface, please mind that large amount of water mixed with cleanser is a must.
Cleaning aluminium components:
While cleaning aluminium components use products acid by nature, e.g. spirit vinegar, lemon. Do not use abrasive substances. Avoid using hard brush, this may cause scratches. It is recommended to use microfiber cloth.
Use circular movements while polishing the surface. Use only clean and dry cloth.

3.6 Powering the Device
A moisture analyzer can be plugged to the mains only by means of an original power cord, which comes standard with the moisture analyzer. Rated voltage (specified on the device’s data plate) must be compatible with the mains rated voltage.

The power cord can be connected only to a socket with a ground contact. Plug the power cord to

the moisture analyzer. The moisture analyzer’s power plug is located at the back of its housing. Moisture analyzer display shows name and program number first, next an indication 0.000 g
(balances with readability of 1 mg) or 0.0000 g (balances with readability of 0,1 mg). If the

indication does not equal zero, press

button.

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3.7 Temperature Stabilization Time Before start of measuring processes, it is necessary to wait until the moisture analyzer reaches thermal stabilisation. For moisture analyzers that were stored in much lower temperatures before plugging to mains (e.g. during winter period), thermal stabilisation period shall take at least 4 hours. During the thermal stabilization, the indications on a display panel can change. It is recommended that ambient temperature changes at place of use were insignificant (slow to change).
3.8 Connecting Additional Hardware Use only accessories and peripheral equipment recommended by the manufacturer. The moisture analyzer must be disconnected from the mains before connecting or disconnecting any peripherals (printer, PC computer, USB type computer keyboard or additional display). On connecting the peripherals, plug the balance to the mains.
4 Start-Up
– Plug the power adapter to a socket, next connect the connector to port located at the back of the housing.
– Press button located in the top right hand corner of the terminal. – Wait until start-up procedure is completed, the home screen of balance software is
displayed automatically. – The balance runs with no user logged in. In order to start operation it is necessary to
carry out the logging procedure (for detailed logging procedure read later sections of this user manual).
5 Keyboard ­ Buttons functions

Button Overview:

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Press to switch the balance ON/OFF Press to Zero the balance Press to Tare the balance Press to send measurement to a printer or a computer Function key

, press to abandon parameter changes or exit to previous menu level Function key , press to exit to home screen Programmable proximity sensors, press to enable operation of freely selected functions 6 Weighing Mode Home Screen 6.1 Weighing Window The main window of balance software can be divided into 3 sections: – Top section displaying data on active working mode (pictogram and name), metrologically important data and button enabling selection of functions available for a particular working mode: – Section presenting the weighing result: © PCE Instruments 10

– Section comprising supplementary information on currently performed operations, and function buttons:
CAUTION! Data and buttons contained in the workspace are freely configurable. For detailed information on data and buttons configuration refer to section 7of this user manual. 6.2 Drying Window
The main window of balance software can be divided into 3 sections: – Top section displaying data on active working mode (pictogram and name), metrologically important data and button enabling selection of functions available for a particular working mode:
– Section presenting the weighing result: © PCE Instruments 11

– Section comprising supplementary information on currently performed operations, and function buttons:
CAUTION! Data and buttons contained in the workspace are freely configurable. For detailed information on data and buttons configuration refer to section 7 of this user manual.
7 Balance Menu
Operation of balance software menu is intuitive and uncomplicated. The touch panel makes the software operation easy. Pressing a function key, a soft key or an area on the display initiates an assigned function or process. 7.1 Entering Balance Menu

In order to enter balance menu, press

button. Clicking any button

comprised within information section, or clicking any button with particular parameter name,

results with change of color. This is for signalling purposes. If a given area has any function or

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action assigned, then it is performed automatically upon clicking (e.g. adjustment procedure), respectively a particular window with parameters or list of appropriate settings is displayed.
7.2 Screen Scrolling

There are two methods for scrolling the screen of parameters window. The first one requires pressing, holding down and scrolling up or down the scrollbar located on the left. The second one requires pressing, holding down and scrolling up or down any point of the displayed window.
7.3 Soft Keys List

Press to enter the main menu.
Press to scroll the menu ,,up”, or ,,down”.
Press to confirm changes.
Press to resign form introducing function modifications.
Press to add a new record to a database.
Press to print out a particular record from a database.

Press to clear the editing field.
Press to enable / disable an onscreen keyboard.
Press to export databases (key active upon plugging a pen drive). Press to import databases (key active upon plugging a pen drive).
Press to select variables, out of the list, for a printout.
Press to delete database’s content.

7.4 Running Software Functions Quick access key
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Label:

Press to enter parameters setup. Press to enter tare value.

Text field with function assigned:

Press to develop an internal adjustment operation (internal adjustment function is assigned to the text field).

Functions selections pictogram:

CAUTION! For instruction on configuration of buttons, labels and text fields refer to section 7.6 of this user manual.
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7.5 Return to Weighing Mode Introduced modifications are automatically saved in menu on return to the weighing mode.

Press

soft key repeatedly, keep Press soft key located on the balance

pressing the key until the balance home overlay for immediate display of a home

screen is displayed.

screen.

7.6 Buttons, Labels, and Text Field Configuration
Area beneath weight indication section can be freely programmed. It is divided into active fields taking form of a table: 3 rows, 10 columns.

The division lines presented above are not visible on the balance screen, they serve only for informative purposes.
This section is designed to comprise user-selected widgets: buttons, labels, text fields, bar graphs:
– button ­ pictogram to which a particular function is assigned, the function is triggered upon pressing the pictogram;
– label ­ field for information, its content is stable. The content depends on displayed option, wherein the options change in course of balance operation. The label may be active or passive. Active label, when pressed, triggers function that is assigned to it, e.g. selecting product out of products database. Passive label provides you with information on current state, no function is assigned to it;
– text field – field for information, both content (text and variables of line 1 and 2) and function assigned to text field are programmable. The field may be active or passive. Its operation is likewise as for label, the only difference is that for the text field it is the user who specifies which function is to be assigned to it. The function does not have to
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refer to displayed information, e.g. the text field displaying date and time may trigger balance calibration upon being pressed; – bar graph ­ option available for Checkweighing and Dosing modes, field providing information on Min and Max threshold – Checkweighing mode, and target weight Dosing mode, the given information is presented in a graphic form, bar graph color informs whether weight stays within the specified tolerance or is out of it. The section may be set up freely in a way matching your needs. Each of the modes may be configured independently. Set up rules: Widgets dimensions (width x height) – button ­ 1×1 – label ­ 2×1; 3×1; 4×1; 5×1 – text field ­ 2×1; 3×1; 4×1; 5×1; 6×1; 7×1; 8×1; 9×1; 10×1 – bargraph ­ 5×1; 10×1 To quickly restore the default widgets layout press the widget and hold it until a window with available options displays. Select and confirm. Exemplary arrangement of widgets:
– Always click extreme left side of a particular field that is to hold a selected .
– A new widget can only take such area that holds no other widgets yet. The software automatically detects which widgets can be applied for a particular area, this is conditioned by widget dimensions.
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– It is possible to change functions assigned to an already applied widget. The applied widget, if not needed, can be removed.
– In order to rearrange widgets layout, it is necessary to delete already applied widgets first, and define new arrangement of buttons, labels and text fields next.

7.6.1 Quick Access Keys
You can define quick access underneath weight indication provides direct access to the functions, it is selected from a

keys, the keys are displayed section. Quick access key most frequently operated list of available keys.

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1. Press and hold for a while the spot
where a given key is to be placed.
2. Select option: key 1×1
3. Enter particular key setup.
4. Select the key.
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5. The selected key is displayed
automatically on a home screen.

Quick access keys list:

Key

Function

Accept/Print

Print header
Print footer Zero Tare Set Tare Change Unit Select Unit Parameters Databases
User

Product Customer Packaging Adjustment Variable 1

Modes featuring the key All modes
Weighing mode exclusively Weighing mode exclusively All modes All modes All modes Weighing mode exclusively Weighing mode exclusively All modes All modes All modes
All modes All modes All modes All modes All modes

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Variable 2 Variable3 Working mode parameters Hide/show last digit Drying mode Drying profile Finish mode Printout interval and unit Open/close cover Start

All modes All modes All modes Weighing mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively

7.6.2 Labels You can select label size and type of information to be displayed for a particular label. In order to select a particular label, use a list of available labels. Upon label selection, specify type of information to be displayed for the label. The selected label is displayed automatically on a specified home screen spot.
Procedure:
Press and hold for a while the spot where a given label is to be placed.

Select a label and its size.

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Label settings window opens, click INFORMATION field in order to see a list of information type available for the selected label.
Select data to be displayed.

The selected label is displayed automatically on a home screen.

Label information types: Label information type Date Time Date and Time Net Weight Tare Gross weight User Product Packaging Customer Variable 1 Variable 2 Variable 3 MSW value MSW status Drying mode Drying profile Finish mode Printout interval Temperature/drying time

Modes featuring the information All modes All modes All modes All modes All modes All modes All modes All modes All modes All modes All modes All modes Weighing mode exclusively Weighing mode exclusively Weighing mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively Drying mode exclusively
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Drying chamber status

Drying mode exclusively

The above presented information type has been designed for particular working modes. Detailed description for a given information type is provided within section overviewing a respective mode.

7.6.3 Text Fields You can select text field size and type of information to be displayed in the first and the second line of the field, plus you can decide on a function that is to be assigned to a particular text field. Upon completed setup operation, the selected text field is displayed automatically on a specified home screen spot.
Procedure:
Press and hold for a while the spot where a given key is to be placed.

Select text field and its size.

Text field settings window opens. Define particular text field parameters:

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Line 1: e.g. text ,
Line 2: e.g. variable {3}, variable for current time displaying (other variables refer to point for non-standard printouts defining),
Function: e.g. adjustment.
When all text field parameters have been defined, the window displays respective values.
The defined text field is displayed automatically on a home screen.
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7.6.4 Bargraphs Bargraph function is accessible for all weighing modes. The bargraph presents in a graphic form how much of balance capacity is in use. Additionally it shows Min and Max thresholds positions for Checkweighing mode, and for Dosing mode it shows target weight value along with permissible tolerance. You can select bargraph size and turn on/off function. This function rescales bargraph in order to improve visualization of indication. Procedure:
Press and hold for a while the spot where bargraph is to be placed.
Select bargraph and its size.
The selected bargraph is displayed automatically on a home screen.
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8 Weighing Operation

Load a weighed object on a balance weighing pan. On stabilization of weighing result, indicated

by stability marker

visible on the left side of balance display, read the measurement result.

Record / printout of the measurement result is available on pressing key:

– for verified balances ­ only stable measurement result can be saved or printed (stability

marker

visible on balance’s display),

– for non-verified balances ­ stable or unstable measurement result can be saved or

printed (regardless of stability marker

absence). If unstable measurement result

is printed then it is accompanied by question mark <?> in front of printed mass value.

8.1 Good Weighing Practice In order to ensure long lasting use of a moisture analyzer plus correct and reliable measurement of weighed loads, follow below procedures:
– Start the balance with no load on the weighing pan (permissible value of load on the weighing pan on balance start is ±10% of its maximum capacity).
– Load the weighing pan steadily avoiding shocks:

– Place weighed loads centrally on the weighing pan: – Avoid side loading, in particular side shocks:

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8.2 Logging Full access to user parameters and to editing databases requires logging as an operator with permissions level. The logging procedure should be carried out on each switching on of the balance.
First Log In operation – procedure:

Run home screen and press < > button, operator’s database window opens with list of available users,
Select option, the software activates an on-screen keyboard, use it to enter operator’s password: ,,1111″,

Press button to confirm, home screen of the software is displayed again automatically, When logged, add users and set the permissions levels (for the procedure of assigning permissions levels go further down this user manual).
On future Logging In, select a user from the list and enter the password, the software initiates operation with permissions level set for the selected user.
Log out operation ­ procedure:

Run home screen and press < > button, operators database window opens, Press

soft key (located as position no. 1 in the list of operators), Home screen of the software is displayed again automatically.

Permissions levels

Balance software comprises three permissions levels: administrator, advanced operator, user.

Permissions level dependent access to edition of user parameters, databases and software functions:

Permissions levels User
Advanced User
Administrator

Enabled operations
Free editing of parameters of <Readout/Filter> submenu. Modification of settings for <Misc.> parameter group, except for settings for ,

and . The operator can start and carry out all weighing processes. The operator can preview information recorded in , (s)he can define universal variables. Free editing of parameters of the following submenus: ; ; ; ; . Access to , and submenus denied. The advanced operator can start and carry out all weighing processes. Access to all user parameters and functions, editing databases enabled.

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8.3 Units
UNITS parameter group enables you to change availability of mass units (the change can be performed in-course of balance operation), and to define two custom units, thus positively effecting comfort and speed of operation. It is possible to change unit to other than unit [g] during weighing process or during operation of other modes.

8.4 Weighing Unit Selection Change of weighing unit is carried out by pressing the weighing unit icon visible next to the value

of measurement result, or by clicking

key (if displayed in an information section). Clicking

the unit triggers its replacement, the clicked unit is replaced with the unit that is next on the list of

available units.

Another option for unit replacement is selecting a particular unit out of the units list, to view the

list click

key (if displayed in an information section).

Unit

Denotation Verified Unit

balance

gram

[g]

Yes*

Taele Taiwan

milligram

[mg]

Yes*

Taele China

kilogram

[kg]

Yes*

Momme

carat

[ct]

Yes*

Grain

pound

[lb]

No

Newton

ounce

[oz]

No

Tical

ounce Troy

[ozt]

No

baht

pennyweight

[dwt]

No

tola

Taele Hongkong [tlh]

No

mesghal

Taele Singapuore [tls]

No

  • – Accessibility of measuring units is conditioned by balance type.

Denotation
[tlt] [tlc] [mom] [gr] [N] [ti] [baht] [tola] [msg]

Verified balance No No No No No No No No No

8.5 Weighing Units Accessibility You may declare which units shall be accessible while selecting a temporary unit by means of
key. Units with parameter value set to option are available for selection in particular working modes, i.e. modes facilitating units change.

Units with parameter value set to option will not be accessible while operating the balance.

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8.6 Start Unit Selection Upon selection of start unit, the balance activates with the specified start unit for these modes where change of the unit is possible. Ability of selecting a given unit depends on the balance status, i.e. if the balance is verified or not.
8.7 User defined Unit You may declare two units. Displayed value of a user- defined unit is a multiplication of measured mass value and a coefficient specified for the particular user-defined unit. The units can be freely named with use of 3 characters maximum. By default the names are displayed as [u1] ­ user unit 1, and [u2] ­ user unit 2.

8.8 Balance Zeroing

In order to zero mass indication, press

button. Mass indication of zero value shall be

displayed together with precise zero

and stability

markers.

Zeroing process is an equivalent for determining new zero point, recognized by the balance as

precise zero. Zeroing is possible only for stable status of display indication.

CAUTION! Zeroing the display indication is possible only within ±2% range of instrument’s maximum capacity. If the zeroed value is above ±2% of the maximum capacity, then the software indicates
a respective error message.

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8.9 Balance Taring

In order to determine net weight of the object, place object’s container (packaging) on the

weighing pan, and on stabilization of measurement result press

key. The display indicates

mass equal zero and symbols: Net and

. On taking off the weighed load and its packaging

from the weighing pan, the display indicates sum of total tared mass with minus sign.

The software enables assigning tare value to a database-stored product. Using this option, the

software automatically uploads data on tare value for a particular product upon its selection from

the database.

CAUTION! Taring negative values is impossible. On taring negative values the balance responds with an error message. In such case, zero balance indication and repeat taring procedure.

Manual Tare Determination Procedure:

– While in optional mode press

quick access key,

An on-screen numeric keyboard is displayed,

Enter tare value and press key, The balance returns to the weighing mode, and the display indicates entered tare value with minus ­ sign.

Deleting Tare The tare value indicated on balance display can be deleted by pressing overlay, or by using programmable function key .

key on balance

Procedure 1 – on taking the tared load off the weighing pan:

– Press

key.

The NET marker is deleted, and new zero point of the balance is determined.

Procedure 2 – with tared load on the weighing pan:

– Press

key.

The NET marker is deleted, and new zero point of the balance is determined.

When tare value exceeds 2% of the maximum capacity, respective message is

displayed in order to inform a user about the fact.

Selecting tare value out of PACKAGINGS DATABASE Procedure:

– While in optional mode, press display.

button located in a top left hand corner of the mass

Wait for a respective window to open, next select . Window with a list of tare values recorded into tare database opens. Select the packaging that is to be used. The balance returns to the weighing mode, and the display indicates selected tare value with a minus ­ sign. or

© PCE Instruments 29

– While in optional mode, press button (if displayed on the screen), Window with a list of tare values recorded into tare database opens. Select the packaging that is to be used. The balance returns to the weighing mode, and the display indicates selected tare value with a minus ­ sign.

AUTOTARE function Autotare function provides automatic taring of the packaging during the weighing process when packaging mass for each of the product is different. For description of this function go further down this manual.

Deleting tare Entered tare value can be deleted by pressing value of 0.000g (see description above).

button on the overlay or by entering tare

8.10 Weighing Mode Settings
The software allows setup of operating parameters (filters, value release and autozero function, deleting the last digit and other settings) separately for each working mode. It enables customizing the instrument and utilizing its properties depending on your needs and expectations, or on specific requirements for selected working mode (e.g. DOSING); as a result the device operation is quick and easy.

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Filter level setting Filter settings adjustment depends on the working environment. For the best possible conditions the filter can work in a very fast mode (V.FAST value for Filter parameter); however, if the conditions are poor (shakes, drafts), the filter should be set to slow or very slow option (SLOW or V. SLOW value for Filter parameter). The effectiveness of the filter is different throughout the weighing range. The filter works slower when “approaching” the weighed mass, it works more intensively for weighed mass within the set range of the filter (parameter for setting filter range is accessible only from the service menu ­ the user does not have any access to it). Depending on the filter, the weighing time is shorter (V.FAST and FAST) or longer (SLOW and V. SLOW).
CAUTION! The higher filter level, the longer weighing time.
Value release Since ambient conditions at a workplace vary, it is necessary to determine the value release parameter in the most preferable way enabling balance adaptation, parameter options are: FAST.+REL., FAST or RELIABLE. Depending on the selected option, weighing time is either shorter or longer.
Autozero function The software features an autozero function (Auto) ensuring precise mass indication. This function automatically controls and corrects zero indication. When Autozero is enabled, it compares balance indications at declared time interval e.g. 1s, provided that weighing pan is unloaded and display indication is close to zero. If results vary less than declared AUTOZERO range e.g. one division, balance zeroes automatically, marker of stable measurement result ­ , and precise zero marker ­ are displayed. If AUTOZERO function is enabled, then each weighing process starts from precise zero point. There are, however, some cases when this function can be a disturbing factor for the measuring process; e.g. very slow placing of a load on the weighing pan (load adding). Here, zero indication correction can also correct actual indication of loaded mass.
Last digit display Function enables displaying the last digit of decimal place for a weighing result. There are three available options:
– Always: all digits visible, – Never: last digit is not displayed, – When stable: last digit is displayed only for a stable weighing result.
Balance ambient conditions Parameter relating to ambient and environmental conditions in which the balance operates. There are two options: and

. Selecting mode makes the balance work much faster, i.e. weighing takes much less time than for mode. If the ambient conditions are unstable it is recommended to use mode. By default, the parameter is set to option. © PCE Instruments 31

8.11 Proximity Sensors The balance features two proximity sensors enabling touch-free balance control. The software detects two motions performed around the sensors:
– Hand in a close vicinity to the left sensor , Hand in a close vicinity to the right sensor .
Each motion can trigger optional balance function. For available functions list go to section 7.6.1. Upon completed configuration procedure, the software runs function assigned to a particular proximity sensor having detected motion around it. To provide correct operation, it is necessary to set the right proximity sensors sensitivity (for more information go to section 9).
8.12 AUTOTARE Autotare is used for quick determination of net weight for loads with different tare values, wherein they are measured one after another. When the function is active ( parameter set to option), the operating process takes the following steps:
– Make sure that the weighing pan is empty and press button responsible for zeroing, Put product packaging on a weighing pan (packaging weight value must be greater than set AUTO THRESH value), After measurement stabilization, automatic taring of the packaging mass proceeds (Net marker appears in the upper part of the display), Put product that is to be packed into the packaging; The display shows net weight of the product; Take off the product together with the packaging;
The balance cancels tare value (packaging weight recorded in balance storage during the first step of the operating process) after the gross mass value (set in parameter) has been exceeded; the entered tare value is cancelled automatically (Net marker disappears from the top section of the display), net weight is displayed; Put packaging of the next product on a weighing pan, automatic taring of the packaging weight proceeds after measurement stabilization (Net marker appears in the top section of the display); Put a next product that is to be packed.
For correct operation of the balance with AUTOTARE function it is necessary to adjust the threshold value.

parameter is connected with the following functions: – automatic tare, – automatic operation, No automatic taring takes place as long as the gross weight value stays within the range set in parameter. © PCE Instruments 32

8.13 Print Mode
Function designed to enable print mode setting, it activates key. Print mode options:

, for this option stable measurement result, along with the settings for

parameter , is sent to the printer port. On pressing key, when

the result is not stable (no

marker on a display), the balance software sends the

measurement result to the port after reaching stability for the measurement.

, for this option every single pressing of button results with sending the measurement indication to the printer port along with the settings for

parameter. Every single indication is sent (stable and unstable). For unstable indication character appears at the beginning of the printing frame. This function applies to non-verified balances exclusively. – – select this option to enable automatic printing of measurements. If this option has been selected, remember to set parameter to suit your needs. – select this option to start automatic printout and record of indications in Weighings database and Alibi database, carried out in a cyclic manner in a specified time interval. The interval is set in minutes, in parameter. Interval range is 1-9999 min.

CAUTION! Each result is printed and recorded (stable and unstable for a non- verified balance, stable for a verified balance). Automatic operation with interval starts at the moment of switching the function on and it lasts until it is switched off. The first stable weighing result of value greater than AUTO THRES value is printed as a first measuremnt. The following measurements are printed with frequency set in INTERVAL parameter. Automatic operation with interval stops when the option is off. On switching the function of auto print with interval, PRINT button becomes inoperative (no indication is printed when pressed).

Automatic operation procedure:

– Press

button to zero the balance (marker of stable measurement

and zero

marker

are shown on a display),

Deposit load, the balance sends the first stable measurement to the printer port,

Remove the load from the pan,

Next measurement is possible when the indication is lower than the set value of parameter (next measurement does not require zero value).
For automatic operation adjust the threshold value. The measurement will not be send from the computer to the printer as long as the mass measurement stays within the set value range .

parameter is connected with the following functions: – automatic tare, – automatic operation, – auto with interval.

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8.14 Minimum Sample Weight
Weighing mode comprises function. In order to use this function it is necessary to enter minimum sample weight (MSW) value and tare values for which the MSW value is to be obligatory. For standard X2 series models the values equal zero. Only authorized PCE employee or operator with Administrator permissions level, providing that balance factory settings enable this, can carry out procedure aiming to determine minimum sample weight and next enter the respective data. If you want to use this function, and your balance menu contains no minimum sample weight data, ask the nearest PCE office for help. Authorized PCE employee determines minimum sample weight for specified tare containers. The determination is carried out using mass standards on site, requirements of applied quality system are adhered to. Obtained value is entered into software, . Balance software enables defining tare value with assigned minimum sample weight value. function guarantees that results of weighing operation are comprised within set tolerance, accordant to applied quality management system of particular company.
CAUTION! This function is valid for weighing mode exclusively.
Options: – MODE None ­ minimum sample weight function off Block ­ select to make the balance display respective pictograms informing on mass (whether it is out-of-tolerance low or out-of-tolerance high); with this option on, the software disables confirmation of the measurement that is out-of-tolerance low Warn ­ select to make the balance display respective pictograms informing on mass (whether it is out-of-tolerance low or out-of-tolerance high); with this option on, the software enables confirmation of the measurement that is out- of-tolerance low – Tare ­ maximum tare value for which minimum sample weight value is obligatory (read examples below) – Minimum mass ­ minimum sample weight determined for particular balance on site using respective method.

Example 1 for balance with d=0.0001 g:

No. Tara value 2 10.0000 g

Minimum Sample Weight 1.0000 g

Operation
Minimum sample weight refers to all net weights subjected to weighing in a tare container of mass 0,0001g ­ 9,9999g inclusive ( button used). The program identifies setting specifying that minimum sample weight is valid exclusively for samples weighed in a tare container of weight covered by the above specified range. If taring function is not used or tare container weight is covered by range 10,0000g ­ Max, then pictogram informing on use of minimum sample weight goes blank.

Example no. 2 for balance with d=0.0001 g:
© PCE Instruments 34

No. Tara value 1 220.0000 g

Minimum Sample Weight 0.5000 g

Operation
Minimum sample weight refers to all net weights subjected to weighing in a tare container of mass covered by full weighing range ( button used). The program identifies setting specifying that minimum sample weight is valid exclusively for samples weighed in a tare container. If taring function is not used, then pictogram informing on use of minimum sample weight goes blank.

Example no. 3 for balance with d=0.0001 g:

No. Tara value Minimum Operation

Sample

Weight

1 0.0000 g

0.2500 g Minimum sample weight refers to all net weights subjected

to weighing where no tare container is used ( button

not used). The program identifies setting specifying that

minimum sample weight is valid exclusively for samples not

weighed in a tare container. If taring function is used, then

pictogram informing on use of minimum sample weight goes

blank.

As a user you can preview entered data, but you are not allowed to edit it.

Weighing with use of function If in course of weighing you want to obtain information stating whether particular measurement is out- of-tolerance high, specified for minimum sample weight, then <Minimum sample weight> function shall be on, to turn the function on go to Weighing mode settings.
Procedure (Administrator exclusively): 1. Enter weighing mode settings, 2. Press field, 3. Press field, 4. Settings window is displayed with the following options:
Block ­ select to make the balance display respective pictograms informing on mass (whether it is out-of-tolerance low or out-of-tolerance high); with this option on, the software disables confirmation of the measurement that is out- of-tolerance low, Warn ­ select to make the balance display respective pictograms informing on mass (whether it is out-of-tolerance low or out-of- tolerance high); with this option on, the software enables confirmation of the measurement that is out-of-tolerance low. 5. Select respective option and return to the home screen, 6. Section presenting the weighing result comprises additional pictogram providing supplementary information. The pictogram changes in course of weighing operation informing you on the weighed sample mass with reference to declared minimum sample weight value

© PCE Instruments 35

Weight value lower than minimum sample Weight value higher than minimum sample weight specified for a particular tare range. weight specified for a particular tare range. Pictograms for minimum sample weight:
Weight value lower than specified minimum sample weight. Weight value higher than or equal to specified minimum sample weight.
CAUTION! If more than one reference tare value has been programmed (along with min load values assigned to them) then indicated value automatically turns to range respective for tare container weight. Requested minimum load changes simultaneously. 8.15 Cooperation with TITRATORS In order to provide correct cooperation with Titrators, go to settings of standard printout content and set parameter to value. With this, other variables for the printout are turned off.
With value on, a respective pictogram is displayed in the top bar of a home screen. The pictogram informs on special format of mass printout, tolerable by TITRATORS.
© PCE Instruments 36

9 Miscellaneous
A user can set up parameters which influence balance operation. These parameters are to be found in parameters group MISC. Settings modification for particular parameters of this parameter group proceeds likewise as described in section 7 of this user manual.
Menu language Language parameter enables selecting the language of the balance menu descriptions for unlogged user. Available languages: POLISH, ENGLISH, RUSSIAN, UKRAINIAN, HUNGARIAN, SPANISH, FRENCH, GERMAN, ITALIAN, CZECH, CHINESE, ARABIC, TURKISH, KOREAN. In order to change menu default language for unlogged user select new language (Setup/Misc./Language) and restart the balance.
Permissions Permissions parameter enables choosing access level for a particular user, one that is not logged in. Available access levels: ADMIN. / USER. / ADV. Depending on selected permissions level, you can enter balance parameters and modify the settings, as far as possible for a particular level. Logging in operation is not required (for permissions overview go to section 9 of this user manual).
,,Beep” sound ­ reaction to operation of pressing a key Sound parameter enables switching on/off a `beep’ sound responsible for informing a user about pressing any key of balance overlay or display, or about proximity sensors response.
Procedure:
© PCE Instruments 37

Backlight and adjusting display brightness Display brightness parameter enables setting the brightness of the backlight or switching off the display brightness completely.
Proximity sensors sensitivity adjustment Proximity sensors sensitivity parameter specifies distance within which the sensors can be operated, its scale is expressed in percent and it ranges from 0% to 100%. For lower percent value the proximity sensors operate at a shorter distance. Procedure:
Date Date parameter enables setting the current date. Procedure:
© PCE Instruments 38

Time Time parameter enables setting the current time. Procedures for change of time settings and date settings are likewise.
Date format Date form. parameter enables altering the date format on the printout [YYYY.MM.DD / YYYY.DD.MM / DD.MM.YYYY / MM.DD.YYYY], where: YYYY ­ year; MM ­ month; DD ­ day.
Time format Time form. parameter enables specifying time format for a printout [12h / 24h]. For [12h] option selected, or

letter is displayed next to presented time value, where: A stands for hours before noon; P stands for hours after noon. AM and PM will be printed near to the time.
Backlight turn-off time parameter enables activation of display stand-by mode, the stand-by mode is activated when no weighing process is carried out (stable indication is a necessary condition for activation of the stand-by mode). NONE ­ backlit turn-off time not activated. 0.5; 1; 2; 3; 5 ­ time given in minutes. If the software registers stable indication for a specified time interval, set in parameter , than the display goes out immediately. The backlight activates upon change of indication (no stability pictogram on the display) or pressing any key on the balance keypad. The display remains blank also when balance menu is entered.
Auto switch-off parameter enables automatic display deactivation (the parameter functioning is likewise to button functioning). Upon display deactivation the other subassemblies are powered and the balance turns to stand-by mode. NONE ­ auto switch-off not activated. 0.5; 1; 2; 3; 5 ­ time given in minutes. If the software registers stable indication for a specified time interval, set in parameter , than the display is turned-off immediately. To start-up the balance, it is necessary to press button located on the balance keypad. The balance automatically returns to weighing operation. Balance cannot be turned off if any process is started or if balance menu is entered.
© PCE Instruments 39

10 Adjustment

In order to ensure the highest weighing accuracy, it is recommended to periodically introduce a corrective factor of indications to balance memory, the said factor must be referred to a mass standard. In other words, balance adjustment shall be performed from time to time.

Adjustment should be carried out: – Before the beginning of weighing procedure, – If long breaks between following measuring series occur, – If temperature inside the balance changes more than: 2°C.

Adjustment type: Adjustment with an external weight of declared mass which cannot be modified or of any mass, but not lower than 30% of maximum range.

CAUTION! Remember to carry out the adjustment process when there is no load on the pan! When the weighing pan is loaded, command is displayed. In such a case remove the load and restart the the adjustment process. Adjustment process can

be aborted if necessary by pressing button

at any time during the process.

10.1 External Adjustment
External adjustment is carried out by means of an external mass standard of specified accuracy class and weight. The process takes semi-automatic form, successive stages are signalled with prompts.
Procedure: Enter submenu, next select option, “Remove weight” prompt is displayed.
Take the weight off the weighing pan and press button. Whereas balance determines start mass, “Adjustment; Please wait…” prompt is displayed, Upon completed start mass determination procedure <Put weight …> prompt is displayed along with particular mass standard value.
Put the required weigh on a pan and press button, Upon completed procedure “Remove weight” prompt is displayed. Take the weight off the weighing pan, wait for window to be displayed again.
10.2 User Adjustment
User adjustment is carried out with an optional standard of mass ranging between 0,3 Max and Max. User adjustment and external adjustment procedures are likewise with one exception, before user adjustment start, a message box for entering mass of a standard used for user adjustment is opened. In order to start user adjustment, enter submenu and select <User adjustment> parameter. Then follow the commands displayed on a screen.

© PCE Instruments 40

10.3 Report Printout Adjustment report is generated automatically at the end of each adjustment process or adjustment test and next it is sent to communication port assigned for PERIPHERAL DEVICES/PRINTER (by default it is COM1). Report content is declared in PRINTOUTS/ADJUSTMENT REPORT menu. Instruction on how to declare settings for this option is to be found further down this manual, read sections referring to printouts. The report can be printed using balance-connected printer or sent to a computer and saved for archiving purposes as a file.
10.4 Temperature Adjustment Temperature adjustment is carried out with a dedicated kit, which is an optional equipment of the moisture analyzer MA_X.
1. Thermometer 2. Thermometer holder and drying chamber shield
Adjustment of the drying chamber temperature is a process carried out for the purpose of adjusting the temperature sensor assembled inside the drying chamber of a moisture analyzer. Before starting temperature adjustment process, place the temperature calibration kit inside the drying chamber, following below diagrams:
Step 1. Remove from the drying chamber the following:
– disposable pan – drying pan handle – cross-shaped holder – drying chamber insert
© PCE Instruments 41

Step 2. Assemble in the drying pan the components of temperature adjustment kit:
– drying chamber shield – thermometer holder and – the thermometer
Step 3. After assembling the kit start temperature adjustment process.
CAUTION! All the activities must be carried out with great caution not to damage the measuring mechanism of the moisture analyzer. Go to menu

a message shall be displayed, upon its confirmation temperature sensor adjustment starts. Follow the displayed prompts. After 8 minutes a numeric keyboard is displayed. Enter the moisture analyzer temperature that is displayed on the control thermometer. © PCE Instruments 42

Press key to confirm, the second step of adjustment starts. The moisture analyzer halogen lamp starts to operate and the drying chamber is heated as long as necessary to provide specified temperature, which is next maintained for 8 minutes. After 8 minutes a numeric keyboard is displayed. Enter the moisture analyzer temperature that is displayed on the control thermometer.
Press key to confirm, the third step of adjustment starts. The moisture analyzer halogen lamp starts to operate and the drying chamber is heated as long as necessary to provide specified temperature, which is next maintained for 8 minutes. After 8 minutes a numeric keyboard is displayed. Enter the moisture analyzer temperature that is displayed on the control thermometer.
Press key to confirm. Temperature adjustment process is completed and moisture analyzer displays window. For moisture analyzers with maximum heating temperature of 250 °C, the temperature adjustment process is likewise, only the temperature values are higher for each part of the process.
© PCE Instruments 43

10.5 Drying Process Test In order to test the drying chamber and the drying process you need to use a special adjustment set (thermometer and the thermometer holder). The set is an optional accessory of a moisture analyzer (the same that is used for temperature adjustment of the drying chamber). For information on how to assemble the set go to Temperature adjustment section.
Procedure: – Set test parameters in accordance with instruction below and the displayed prompts. – Enter ADJUSTMENT menu and start procedure.
Enter: – testing temperature – permissible error – serial number of the temperature
adjustment set

Upon confirmation of serial number START message is

displayed. Press

key to

confirm. The drying process starts

and continues until specified

temperature is reached. Time and

sensor temperature information is

displayed.

The temperature is maintained for 8 minutes (like for temperature adjustment procedure). After 8 minutes you shall see a window for entering temperature read from the installed adjustment set. Press
to confirm.

The result of the test may be printed on a printer connected to the balance. Look left to see an example of a report.

© PCE Instruments 44

11 Determining Printout Content

11.1 Adjustment Report
ADJUSTMENT REPORT is a group of parameters enabling to declare data that is to be printed on an adjustment printout.

Variable PROJECT
CALIB TYPE USER PROJECT DATE TIME BALANCE ID CAL. DIFFER
DASHES
SIGNATURE

Overview Option enables naming the project (name associated with a particular type of weighing). The name may consist of maximum 31 characters. Option enables printing out the type of the adjustment being carried out. Option enables printing out the name of a logged-in user. Option enables printing out the name of the project (see parameter Project). Option enables printing out the date of the carried out adjustment. Option enables printing out the time of the carried out adjustment. Option enables printing out the balance ID number. Option enables printing out the difference between mass of an adjustment weight measured during the last adjustment and the current measured mass of this weight. Option enables printing out dashes that separate the date of a printout from a signature. Option enables providing an area for the signature of a user performing the adjustment.

Procedure for naming the project:

An exemplary report: For the parameters described above, one of these values must be selected: NO – do not print YES – print
© PCE Instruments 45

11.2 Drying Process Report Printout Group of parameters enabling user to declare data that is to be printed on a Drying Process Report printout. The Drying Process Report is divided into three individually customized sections: the header, the measurement, the footer. The settings are valid for Drying Process mode exclusively.
HEADER Group of parameters enabling to declare data that is to be printed on a header printout.
MEASUREMENT Group of parameters enabling to declare data that is to be printed on a drying process result printout.
FOOTER Group of parameters enabling to declare data that is to be printed on a footer printout.
© PCE Instruments 46

Printout variables list:

Variable DATE
TIME
BALANCE TYPE BALANCE ID USER
PRODUCT
PROGRAM
DRY.PARAM.
VARIABLE 1 VARIABLE 2 VARIABLE 3 START MASS
EMPTY LINE
TIME
INDICATION
DRYING TIME AND INDICATION NET
TARE
GROSS
SET TEMPERATURE
CURRENT TEMPERATURE
STATUS
END DATE
END TIME
DRYING TIME
END MASS

Overview Option enables printing out the date of drying process start Option enables printing out the time of drying process start Option enables printing out the balance type. Option enables printing out the balance ID number. Option enables printing out the name of a logged-in user. Option enables printing out the name of a currently selected product. Option enables printing out the name of a currently selected drying mode. Option enables printing out the drying parameters with accordance to which the sample is to be dried. Option enables printing out the value of VARIABLE 1. Option enables printing out the value of VARIABLE 2. Option enables printing out the value of VARIABLE 3. Option enables printing out net weight value in a basic unit (calibration unit). Option enables printing out an empty separating line.
Option enables printing out the drying time with preset interval during drying process. Option enables printing out the drying process indication with preset interval during drying process. Option enables printing out time and indication with preset interval during drying process. Option enables printing out net weight value with preset interval during drying process. Option enables printing out tare value with preset interval during drying process. Option enables printing out gross weight value with preset interval during drying process. Option enables printing out temperature set in a particular stage of the drying process with preset interval during the process. Option enables printing out current temperature read from the sensor with preset interval during drying process. Option enables printing out the status of drying process summary (Completed/Aborted). Option enables printing out the end date of the drying process. Option enables printing out the end time of the drying process. Option enables printing out the total time of the drying process. Option enables printing out the end mass of the tested sample.

Active for: Header Header Header Header Header Header Header Header Header Header Header Header Header Footer GLP printout GLP printout GLP printout GLP printout GLP printout GLP printout GLP printout
GLP printout
Footer Footer Footer Footer Footer

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INDICATION SIGNATURE NSTR.PRNT.

Option enables printing out the final indication of the drying process. Option enables providing an area for the signature of a user performing the measurement. Option enables printing out one of 100 non-standard printouts on the footer printout. You can choose one of the following options: NONE / non- standard printout name. The way of entering non-standard printouts is described further down this user manual.

Footer
Footer
Header Footer

For the parameters described above, one of these values must be selected:

NO – do not print YES ­ print

CAUTION! For exemplary printout of a report go to section 19 of this user manual.

11.3 Other Printouts
HEADER Group of parameters enabling to declare data that is to be printed on a header printout.

GLP PRINTOUT Group of parameters enabling to declare data that is to be printed on a measurement result printout.

FOOTER Group of parameters enabling to declare data that is to be printed on a footer printout.

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Printout variables list:

Variable WORKING MODE BALANCE TYPE BALANCE ID USER
PRODUCT
CUSTOMER
PACKAGING DATE
TIME
VARIABLE 1
VARIABLE 2
VARIABLE 3
NET
TARE GROSS CURR.RES. MSW WEIGHT MSW TARE MASS FOR TRITATOR ADJUSTMENT REPORT

Overview Option enables printing out the name of a working mode.
Option enables printing out the balance type.
Option enables printing out the balance ID number.
Option enables printing out the name of a logged-in user.
Option enables printing out the name of a currently selected product.
Option enables printing out the name of a currently selected customer.
Option enables printing out the name of a currently selected packaging. Option enables printing out the date of the carried out adjustment.
Option enables printing out the time of the printout.
Option enables printing out the value of VARIABLE 1.
Option enables printing out the value of VARIABLE 2.
Option enables printing out the value of VARIABLE 3.
Option enables printing out net weight value in a basic unit (calibration unit).
Option enables printing out the tare value in the current unit. Option enables printing out the gross mass value in the current unit. Option enables printing out the current measurement result (NET weight) in a current unit. Option enables printing out the minimum sample weight value declared for a balance. Option enables printing out the tare value for minimum sample weight. Option enables printing out the net mass set for correct cooperation with titrators. Option enables printing out the report of the last adjustment in accordance with the settings declared for

Active for Header Footer Header Footer Header Footer Header GLP printout Footer Header GLP printout Footer Header GLP printout Footer GLP printout
Header GLP printout Footer Header GLP printout Footer Header GLP printout Footer Header GLP printout Footer Header GLP printout Footer Header GLP printout Footer GLP printout
GLP printout
GLP printout
GLP printout
GLP printout
GLP printout
Header GLP printout

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DASHES EMPTY LINE SIGNATURE NSTD.PRNT.

adjustment report printout (for more information go to section 10.1 of this user manual. Option enables printing out separating dashes.
Option enables printing out an empty separating line.
Option enables providing an area for the signature of a user performing the adjustment. Option enables printing out one of 100 non-standard printouts on the footer printout. You can choose one of the following options: NONE / non- standard printout name. The way of entering non-standard printouts is described further down this user manual.

Footer
Header Footer Header Footer Footer
Header GLP printout Footer

For the parameters described above, one of these values must be selected:

NO – do not print YES – print

Exemplary printouts:

HEADER

GLP Printout FOOTER

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11.4 Non-standard Printouts The balance software enables entering 100 non- standard printouts. Each of them can consist of approximately 1900 characters.
Non-standard printout may include: – variables dependent on the working mode and other needs (mass, date etc.) – permanent text from the user menu.
Non-standard printout can have approximately 1900 characters.

11.4.1 Inserting Texts Variables list:

Symbol {0} 1) {1} 1) {2} {3} {4} {5} {6} {7} {8} {9}

Description Standard printout in a calibration unit Standard printout in a current unit Date Time Date and time Working mode Net weight in a current unit Net weight in a calibration unit Gross weight in a calibration unit Tare in a calibration unit

{10}

Current unit

{11}

Calibration unit

{12}

Min threshold

{13}

Max threshold

{32}

Factory no.

{45}

Target value

{46}

Tolerance

{50}

Product: Name

{51}

Product: Code

{52}

Product: EAN code

{53}

Product: Mass

{54}

Product: Tare

{56}

Product: Minimum

{57}

Product: Maximum

{66}

Product: Tolerance

{70}

Variable 1

{70}

Variable 2

{72}

Variable 3

© PCE Instruments 51

{75}

User: Name

{76}

User: Code

{77}

User: Access level

{80}

Packaging: Name

{81}

Packaging: Code

{82}

Packaging: Mass

{85}

Customer: Name

{86}

Customer: Code

{87}

Customer: VAT no.

{88}

Customer: Address

{89}

Customer: Postal code

{90}

Customer: City

{146} {147}

Gross weight in current unit Tare weight in current unit

{150} {151}

Form feed for PCL printers Paper crop for EPSON printers

{155}

Cooperation with CONECT PC software

{275} {276} {277} {278} {280} {281} {284}

Ambient conditions readout date and time THB: Temperature THB: Humidity Internal sensor: Temperature 1 THB: Pressure Air density THB: Temperature from an additional sensor

{380} {381}

Drying mode: Name Drying mode: Code

{385}

Drying profile

{386}

Drying profile parameters

{387}

Finish mode

{388}

Finish mode parameters

{389}

Report from drying process: Unit

{390}

Report from drying process: Printout interval

{395}

Moisture analyzer: Set temperature

{396}

Moisture analyzer: Current temperature

{397}

Moisture analyzer: Drying time

{398}

Moisture analyzer: Status

{399}

Moisture analyzer: Drying time and result

{400}

Moisture analyzer: Humidity content

{401}

Moisture analyzer: Dry mass content

{402}

Moisture analyzer: Humid/Dry

CAUTION!

  1. {0} and {1} variables format terminates with CR LF characters, with this the newline occurs by default.

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Every single printout can contain max 1900 characters (letters, numerals, non- standard characters, spaces). A user can apply non-standard characters depending on type of data that is to be printed out. An example: “PCE” DATE:

TIME: PRODUCT MASS: *****SIGNATURE:……… Enter printout content settings and design the printout using respective data variables and characters for text format. If you want to carry out HEADER or GLP or FOOTER printout using EPSON printer (equipped with autocutter blade) and crop the paper beneath the respective printout, then you have to select an option of non-standard printout comprising {151} variable, and set this option in header, GLP printout or footer settings, respectively (means for entering control codes are described in section 21 of this user manual). In such case command should stay empty. Paper must be cropped underneath the FOOTER. © PCE Instruments 53

Exemplary settings:
Means for inserting texts – by an on-screen keyboard – by a computer keyboard of USB type
A computer keyboard of USB type can be connected to a balance, this enables easier and quicker editing of the printouts. Willing to insert any text, it is necessary to select a respective menu option and, using the keyboard, type the text. 11.5 Variables Variable is defined as alphanumeric data which can be linked to printouts, products or other information related to weighing. Every variable is characterized by its content, the content must be given. Variables are used for entering various data during the weighing process, e.g. serial number or batch number. The program allows to enter 3 variables. Each can consist of max 31 characters. In order to insert a variable content, you need to enter variable settings (VARIABLE 1, VARIABLE 2, VARIABLE 3) and enter the respective values using direction keys (arrows) on the balance keypad or a computer keyboard. Procedure for entering texts is the same as for non- standard printouts.
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12 Working Modes ­ General Information
Standard version of MA_X balance feature the following working modes: Weighing Means of operation: weight of a load is determined through an indirect measurement. A balance measures gravitational force which attracts the load. An obtained result is processed to a digital format and displayed in a form of measurement result. Drying Means of operation: determining moisture content in a sample, obtained by vaporization of all moisture components from a sample placed inside a drying chamber of a moisture analyzer. A measurement result is automatically calculated by the software and visualized on an ongoing basis on moisture analyzer’s display by comparing mass of a sample on measurement start, in progress, and at the end of drying process.
Particular working modes settings feature specific functions. The functions enable adapting mode operation to your individual needs. The special settings are activated on selecting a respective profile. A detailed description of specific functions is provided within description of working modes.
12.1 Working Modes Accessibility Group of parameters enabling you to declare which functions are to be accessible. You can deactivate functions that are not used in course of balance operation, to do it, value has to be selected for a particular parameter. Procedure:
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12.2 Running Working Mode To run working mode other than currently operated one:
– press pictogram of currently used working mode, the pictogram is located in the top left hand corner,

– wait for the available working modes list to be displayed, – select the working mode you need to operate.
12.3 Parameters Related to a Working Mode Each working mode has programmable parameters determining its functioning. Read point 9 of this user manual for description of possible settings for WEIGHING working mode. Settings for DRYING working mode are specified within its description.

13 Databases

Balance software features the following databases <

:

– Products (5 000 products)

– Users (100 users)

– Packaging (100 packaging types)

– Customers (1 000 customers)

– Drying modes (200 drying modes)

– Drying reports (5000 reports)

– Ambient Conditions (10 000 records)

– Weighings (50 000 records)

CAUTION! It is not possible to edit some of the databases for a balance cooperating with E2R software. Shall you introduce any modifications on databases, use the PC software.

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13.1 Database Connected Operations
The program enables the user with appropriate access level to carry out the following operations: adding new record, exporting data from databases, importing data to databases, deleting one record from the database, deleting all records from database, printing data saved in a record.

ADD NEW RECORD
– Enter a database and press (Add) button located in the top bar. Define fields for the new record (data content depends on the database). On returning to the databases window a new record is displayed on the list.

EXPORT

– Insert USB flash drive. Open the database that is to be exported.
Press icon located in the top bar.

The program automatically saves exported data to a pendrive file, respective prompts are displayed for confirmation of successfully completed operation. The name of a file depends on the database.

Database Operators database Products database Packaging database Customers database Drying modes database Non-standard printouts

File name and extension users.x2 products.x2 packaging.x2 customers.x2 programs.x2 non_standard_printouts.x2

IMPORT

– Save the file with database content that is to be imported to a flash drive. Only files exported from other balance that had proper names and extensions can be imported ­ see table above. Insert USB flash drive. Enter database that is to be imported.
Press icon located in the top bar. The program automatically reads the file and the data is imported to the balance. Respective prompts are displayed for confirmation of successfully completed operation.

DELETE A RECORD

– Press the record and hold it. A message: is displayed.

Press <

to confirm, the record is deleted from the list.

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DELETE A DATABASE

– Enter selected database and press (Delete everything) pictogram located in the top bar. A message: is displayed.

Press <

to confirm, the database is deleted.

DRYING REPORTS and WEIGHING REPORTS cannot be imported. DRYING REPORTS database cannot be deleted.

AMBIENT CONDITIONS database serves informative purposes only. Using records preview option you can check ambient conditions and observe how they changed over time. The data
saved to records can be printed by pressing pictogram located in the top bar. Records’ names contain date and time of saving the record’s data to balance memory.

13.2 Products Product database stores names of all products that can be weighed, counted, controlled.

List of parameters defined for a product:

1. Name

[product name]

2. Code

[product code]

3. EAN

[EAN code for a product]

4. Mass

[nominal mass/single product mass]

5. Tare

[tare value, set automatically when the product is selected out of the

database]

6. Min

[low limit for product weighing in CHECKWEIGHING mode]

7. Max

[high limit for product weighing in CHECKWEIGHING mode]

8. Tolerance [% value calculated in relation to mass, the parameter determines

measuring area for which the measurement is recognized as correct for

DOSING mode.]

CAUTION! Remember to assign product to particular mode, as some of data values are adopted to the particular mode functions, e.g. mass in mode is accepted as reference mass, whereas mass in mode is accepted as single part mass. When a particular product is used for different modes then its weight, taken from product data, is associated with different data for these modes.

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13.3 Users User’s database features list of operators permissioned to operate the balance.
List of parameters defined for a user: 1. Name 2. Code 3. Password 4. Permissions level 5. Language
13.4 Packaging List of used packaging with parameters such as name, code and weight value specified. When carrying out weighing process, upon selection of particular packaging, a respective tare value is operated automatically. The tare value is displayed with minus sign.
List of parameters defined for packaging: 1. Name 2. Code [internal code providing packaging identification] 3. Tare [packaging weight] 13.5 Customers Customer’s database features a list of names of customers for whom the measurements are carried out.
List of parameters defined for a customer: 1. Name 2. Code [internal code providing customer identification] 3. NIP 4. Address 5. Postal code 6. City
13.6 Drying Program Database of drying programs contains saved data on drying parameters which are activated to dry a product.
List of parameters defined for drying mode: 1. Name 2. Code 3. Drying profile 4. Finish mode 5. Printouts 6. Sample mass control
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13.7 Drying Process Reports Reports on drying process database stores information on carried out drying processes. Each report can be previewed and printed. Procedure:
– Enter < Databases> submenu, press key, Select particular report button out of the list, use scroll buttons to find the report you need, Report’s name consists of date and time of its creation, e.g.: 2011.10.12 15:12:15.
Information provided by the Drying Process Report: 1. User 2. Drying mode 3. Start date 4. End date 5. Drying time 6. Status 7. End mass 8. Drying status 9. Indication
13.8 Ambient Conditions Ambient Conditions database comprises ambient conditions related information. Depending on the setup, the ambient conditions record may comprise data such as temperature, humidity, atmospheric pressure. When the THB module is connected to the balance then its indications are recorded to the database too. Procedure:
– Enter < Databases> submenu, press key. Press the required record, if not visible scroll the records list down. Record name comprises date and time.
CAUTION! The software saves ambient conditions record in a so called loop, i.e. when the measurement 10 001 is saved, the measurement 1 is automatically deleted from the balance’s memory. Records saved to balance memory cannot be deleted.
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13.9 Weighing Records Each measurement result sent from a balance to a printer or a computer is saved in the database of weighing records. Balance user can preview data from each weighing record.
Procedure:
– Enter < Databases> submenu. Enter database and press selected record.
Information defined for a weighing record: 1. Measurement date 2. Measurement time 3. Measurement result 4. Weight 5. Tare value 6. User 7. Product name 8. Customer, Customer name 9. Packaging, tare name applied during product measurement 10. Working mode name 11. Variable 1 12. Variable 2 13. Variable 3
14 Sample Preparation for Drying
This section of the MA_X user manual contains data on setting optimum test results during drying processes. There are hints for selection of appropriate drying parameters for various materials and substances.
14.1 Means of Moisture Content Measurement on a Moisture Analyzer Measurement of moisture content in a tested sample is carried out by determining loss of mass in a sample by its heating (humidity evaporation). PCE moisture analyzer MA_X comprises two components: a precision balance and a drying chamber. Compared to standard moisture content determining methods, the measurements with application of PCE moisture analyzer is much quicker and does not require additional mathematical calculations (a result of moisture content is previewed on an ongoing basis during product testing process). Independently on moisture content determining method, the measurement accuracy is highly influenced by means of sample preparation and selection of testing parameters, such as:
– Sample size – Sample type – Drying temperature – Drying time
In practice, the measurement accuracy is not as important as the speed of obtaining measurement result (control over technological process). Thus, heating a sample (with application of a halogen filament) carried out by a moisture analyzer, makes the measurement process very time efficient and short. Measurement speed can be additionally increased by appropriate adjusting moisture analyzer’s parameters depending on tested substances.
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Optimum temperature and drying time depend on sample type and size, and anticipated measuring accuracy. Selection of drying parameters can only be carried out on basis of test measurements.
14.2 Sampling and Preparation Sample features, its preparation and size are very important factors influencing the speed and accuracy of measurement process. Means of sampling and preparation are extremely important for repeatability of measurement results, as a sample should be a representative part of tested substance.
Final measurement result is vastly conditioned by precise and considered sample preparation. A sample used for analysis has to represent the total structure of tested material. Sampling process should determine: sampling means, sample disintegrating, particle size after disintegration, sample uniformity and other. The sampling process should be carried out as quickly as possible, so that a sample does not lose or absorb humidity from surrounding area. Applied sampling standards should match individual user needs and requirements of tested material, its consistence and sample size.
Number of samples Increasing number of tested samples also increases statistic measurement certainty. Number of samples depends on uniformity of tested material, its purity, accuracy of applied measuring method and anticipated accuracy of obtained results.
Material mechanical disintegrating for measurements Applied disintegrating method should be selected appropriately to tested material. Substances that are hard and brittle (crisp) can be disintegrated by cutting. Grinding such substances may cause their heating and thus humidity vaporization, resulting in unreliable measurement results. Unless a substance can be prepared for measurement otherwise than grinding, any possible moisture content loss should be calculated.
Use of high-silica sand Ensuring optimum substance drying requires that a sample has the largest possible surface for moisture content evaporation. Test results of moisture content for substance with surface in a form of a shell (e.g. glucose syrup) or doughy (e.g. butter), can be much more reliable if a sample is mixed with a dried high-silica sand (improvement of measurement accuracy and repeatability). While using mixture, disposable weighing pan with extended brim must be applied (greater volume of a sample).
Grease in a form of paste or melting substances Such substance requires testing with use of a filter made of glass fibre, which considerably increases active evaporation surface by separating the substance between the fibre. Initial filter drying is necessary only in case of measurements which require very high accuracy.
© PCE Instruments 62

Liquid substances It refers to liquid substances, which by creation of drops on their surface, caused by surface tension, may render difficulties in drying process. In such cases, it is proved to use a glass fibre filter to shorten measurement time. The filter causes separating tested liquid around the fibres, and increasing active evaporating surface. Initial filter drying is necessary only in case of measurements which require very high accuracy.
Substances with structure of leather or temperature sensitive In case of such substances it is proved to use a glass fibre filter. While testing, a substance is placed on a drying pan, and sample surface is covered with a filter, which protects the sample from direct heat radiation. In such case, the sample is heated by convection (which is milder than radiation).
Substances containing sugar The surface of such substances often may caramelize during testing procedure. Therefore, it is recommended to use thin layer of a sample, and moderate drying temperature.
Sample distribution on a pan:
Loose materials Dried in their natural state, i.e. in their natural form or disintegrated. Sample disintegration causes smaller dispersion between the following measurements. Sample mass should not be too high, and the sample should be evenly spread on whole surface of the drying pan.
Liquid substances Semi-fluid substances are dried in their natural form. Large amount of grease (fat) occurring in some of substances makes moisture content determination difficult. In such case it is recommended to use additional components, which increase sample’s active surface and aid moisture content releasing process from a sample. Such components are high silica sand, blotting paper or filter. Before drying a tested substance, initially dry the additional component, so that its humidity is close to zero.
Solid objects Depending on solid object’s structure (dense or loose), moisture content determining process may take short or long time. The size of solid’s surface determines the speed of drying process, and measurement reliability. Thus, the surface of a solid object should be as large as possible. Since solid objects release moisture through their outer surface, sample thickness is another important factor.
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15 Selection of Drying Parameters
15.1 Selecting Optimum Mass for a Sample Sample mass influences the accuracy of measurement result and measurement time. Higher mass of a sample, causes higher amount of water (moisture content) which needs to evaporate, and therefore measurement time is also longer. Obtaining short measurement time is feasible in case of small sample mass, but sample mass cannot be too small, as it may negatively influence required measurement accuracy.

15.2 Influence of Sample Weight on Measurement Result Repeatability
Sample mass considerably influences repeatability of measurement results obtained on a moisture analyzer. Relation between sample mass and repeatability is presented in a table below.

Sample weight ~2g ~10 g

Repeatability ±0.05% ±0.01%

The above data refers to a model, uniform sample, containing no moisture due to the evaporation process and showing no signs of decomposition (e.g. wet high-silica sand).

The results uncertainty cannot be avoided, this is due to sample nature and moisture analyzer repeatability. In practice, it means that obtained measurement result may exceed repeatability values provided above.
© PCE Instruments 64

15.3 Drying Temperature Drying temperature has the largest impact on drying time. Temperature value depends on type of dried substance. Too low drying temperature causes too low moisture content evaporation (underdried sample), and consequently unnecessary extending of measurement time. Too high drying temperature causes burning of dried sample (sample overheating, chemical decomposition). Drying temperature of traditional method (using a furnace) is specified in applicable industry or company standards. Unless standards apply, then temperature should be adjusted by tests.
On selecting drying temperature value, proceed as follows: – Determine moisture content in a sample – Determine temperature of substance chemical decomposition by tests – Compare result obtained on a moisture analyzer with the one of traditional method
When drying a sample with high moisture content, it is possible to shorten measurement time by selecting quick or step drying mode. In such case, the majority of moisture content is released drying temperature higher than set. Only after some time, the temperature is lowered to the set value, and maintained until completing drying process.
15.4 Selecting Drying Profile The software of moisture analyzer enables selecting one of four drying profiles:
– Standard – Quick – Mild – Step
STANDARD profile Standard profile is the most frequently used of all drying profiles. It enables accurate determining of moisture content in a dried sample.
MILD profile Mild profile is used in case of drying substances that are sensitive to rapid heat emitted by filaments operating at full power in the initial stage of drying process. This profile prevents from decomposing of substances sensitive to heat by mild temperature increase in set amount of time (time interval has to be selected by tests). Mild profile is recommended to drying samples of leather structure.
© PCE Instruments 65

FAST profile Fast profile is recommended to drying samples that moisture content varies from 5%, and 15%. In the initial stage of Fast profile, heating takes place at full power of the filaments, causing heating the drying chamber to increased temperature (maximum temperature value is higher by 30% from set drying temperature). Overheating compensates heat loss during evaporation of large moisture content in the test’s initial stage.
STEP profile Enables determining up to three steps with random drying temperature. Step profile is recommended for drying substances with moisture content over 15%. Temperature and heating time in each step have to be adjusted by tests.
15.5 Drying Time Drying time is set by selecting one of available finish mode criteria. This means that a moisture analyzer must meet pre-set criterion (one of the requirements: mass over time, time) to automatically finish the drying process. Finish of drying process can be triggered by amount of time, independently on loss in mass. This criterion is used for substances that may decompose during drying process, and their mass does not reach constant value. The second criterion is loss in mass (less than 1 mg) in defined amount of time.
Automatic finish mode (Auto switch off mode) The operator can choose between various types of finish modes:
– Automatic 1 (change 1mg/10s) – Automatic 2 (change 1mg/25s) – Automatic 3 (change 1mg/60s) – Automatic 4 (change 1mg/90s) – Automatic 5 (change 1mg/120s)
Time-defined finish mode – drying process finish takes place on elapsing a set amount of time, independently on measurement result (maximum drying time 99 hours 59 minutes).
Manual finish mode – the operator ends drying process manually by pressing START/STOP soft key on moisture analyzer’s display.
© PCE Instruments 66

Defined finish mode – user defined criterion. The operator determines the limit value for loss of mass and time in which the loss of mass must not exceed a pre-set value. As the moisture analyzer reaches the set criterion it automatically finishes the measurement (drying process). – User defined 1 (m ­ change of mass and t ­ change of time must be given, the former in mg, the later amounts to 120 s. maximally) – User defined 2 (set moisture content change ratio %M over time 60s)
15.6 Drying Profile Analysis For the first case, the drying profile is an asymptote. Moisture content value remains constant even after long drying time. Using this drying profile makes determination of humidity easy. The measurement result is always referred to constant value of asymptote. The result corresponds easily and it is not difficult to select a proper criterion of finish mode. For the second case the drying process is quick at the beginning, next it stabilizes. Moisture content value is never constant. Drying process profile may proceed as follows: The sample undergoes thermal decomposition, wherein evaporation takes place and as a result the product weigh decreases. Evaporation of grease, oil, plastic or other volatile materials may take much more time than in case of water. Difficult to evaporate materials drop weight. Result obtained using this mode may be optimistic:
– Lower temperature may slower material reaction. – Selection of appropriate criterion may let the user recognize end of analysis, within
described drying step. – Constant drying often assures good drying results. – Maintaining start sample weight permanently (+10%….+20%).
16 Drying
DRYING mode has been designed to enable determination of moisture content of a given sample. The moisture content value is obtained via evaporation of moisture from sample placed inside of the drying chamber. The result is calculated automatically (and displayed) in real time, the calculation is made on the basis of sample mass at the beginning, in the course, and at the end of the process.
Procedure for activation of Drying mode: – Select mode, the home screen is displayed automatically, wherein the top bar of the screen features pictogram.
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Info field provides the following information: – Product – Drying program – Drying profile and drying temperature value – Finish mode – Printout parameters – Info field displaying (in the course of drying) time and drying temperature values – Info field displaying chamber status – Buttons: parameters, user, drying program, open/close cover, drying mode settings, start, databases
16.1 Mode Related Settings The supplementary settings enable you to adjust the working mode to your needs and requirements. Drying profile Parameter enabling you to select respective drying profile and set drying temperature. Finish mode Parameter enabling you to select respective finish mode and set its parameters. Printout parameters Parameter enabling you to set the drying process unit for both the display and the printout, and measurement result printout interval during drying.
Prognosis Parameter enabling to turn on/off result prognosis function.
Close the cover and turn the moisture analyzer off Parameter enabling you to activate/deactivate auto opening/closing of the drying chamber’s lid upon switching the moisture analyzer off by pressing button.
For means of operation of the remaining functions read point 8.11 WEIGHING Mode Settings.
16.2 Drying ­ Quick Access Key Each working mode features automatically displayed set of default keys. The set can be modified by assigning out-of- list quick access keys to the on-screen buttons. Such operation requires particular permissions level. List of quick access keys it to be found in section 7.6 of this user manual.
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17 Drying Process Performed by Means of Quick Menu
Default display configuration in drying mode. Current drying parameters are displayed in a form of pictograms in the middle of the information field. Willing to perform the procedure in accordance with other parameters, enter the settings and modify the respective parameters values. Enter drying process menu, set the following parameters:
– Drying process mode and drying process parameters, – Drying process finish mode and finish mode parameters – Unit for a displayed and printed result – Interval for measurement printout, wherein the measurements are printed during the
drying process 17.1 Drying Process Profile and Drying Parameters
Enter drying parameters settings and select mode type. Upon selection fields enabling setting profile parameters are displayed. Parameters depend on selected mode.
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Drying process mode parameter takes the following values:
– STANDARD drying profile For standard profile set drying temperature in which a sample is to be tested.
– FAST drying profile For quick profile, set both, heating time in a temperature higher than the preset one and temperature for which a sample is to be tested.
Specific feature of this drying profile is fast increase of drying temperature in short period of time. When compared to the preset temperature, the drying temperature rises 30% within 180 seconds and it is maintained at this level for a specified amount of time, next it drops to temperature value preset in drying profile parameters.
CAUTION! For Fast profile set the drying temperature and heating time 30% higher than set temperature. Heating time is measured since reaching the set temperature.
– MILD drying profile For mild profile, set length of time within which moisture analyzer is to reach specified temperature and temperature for which a sample is to be tested.
– STEP drying profile For step profile, set heating time in temperature number one, first step temperature, heating time in temperature number two, second step temperature and temperature in which a sample is to be tested.
CAUTION! For Step profile, set step temperature ,,1″ and ,,2″ and temperature of drying, set also time heating time in particular indirect temperatures (1 and 2). Time for heating in particular steps is counted from the moment of reaching a preset temperature for a particular step.
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17.2 Automatic Finish Mode
Automatic finish mode (Auto switch off mode) takes the following values: Automatic 1 – auto switch-off (mass change of 1mg / within time length of 10s) Automatic 2 – auto switch-off (mass change of 1mg / within time length of 25s) Automatic 3 – auto switch-off (mass change of 1mg / within time length of 60s) Automatic 4 – auto switch-off (mass change of 1mg / within time length of 90s) Automatic 5 – auto switch-off (mass change of 1mg / within time length of 120s) Manual Manual switch-off (on pressing Start/Stop button, maximum drying time is 99 hours and 59 minutes, when drying takes this long or longer the drying process is finished automatically) Time-defined time-defined switch-off (maximum drying time is 99 hours 59 minutes) Defined 1 defined switch-off (change of mass comprised within the balance range, set with moisture analyzer readability, time interval ranging from 1 to 120s) Defined 2 defined switch- off (change in humidity set with moisture analyzer readability, time interval ranging from 1 to 60s).
17.3 Unit of Displayed and Printed Measurement
g – mass change, measurement result is mass change recorded during drying process, %M – percent loss of weight, displays weight change recorded during drying process expressed in percent, %D – part of dry mass obtained during drying process, expressed in percent, measurement result is part of mass that is remaining on a drying pan after humidity content evaporation,
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%R – humid / dry ratio obtained as a result of drying process, expressed in percent, measurement result is part of mass that evaporated from the dried sample during drying process 17.4 Printout interval
The time interval between printouts in seconds ranging from 0 to 120.
18 Drying Process Performed with Use of Drying Modes Database
Moisture analyzer can record up to 200 drying modes that may be freely configured, recorded and used. Procedure ­ selecting a mode:
– Insert the mode to moisture analyzer’s memory (read section 13 Databases) – Select inserted mode prior drying process. Drying parameters update to parameters
saved in selected drying mode.
Or: Insert data related to product/sample that is to be dried. Set the inserted mode as drying mode (read section 13 Databases). Select inserted product as a current one prior drying process. Drying parameters update to parameters saved in the drying mode that is assigned to a selected product.
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19 Drying Process

Drying process settings are displayed in the information field above the buttons.
Press Start button in order to run the drying process. If the drying chamber’s lid is closed, it gets opened automatically Prompts and messages are displayed making moisture analyzer operation easier. Follow the prompts to correctly prepare the sample and to perform the process of humidity content determination for a tested sample.
Program prompts you to prepare a weighing pan. A respective pictogram on drying chamber status is displayed.

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Place the disposable weighing pan in a pan handle and deposit it on a bracket. The display shows disposable pan weight. It is recommended to close the drying chamber in order to provide stable ambient conditions while taring, to do it press pictogram (to be found at the bottom of the screen).
Press key to zero the weighing pan weight.
Indication equals ZERO, drying chamber’s lid gets opened automatically, subsequent prompt is displayed and the pictogram on drying chamber status changes.
Deposit sample on a weighing pan. Sample weight shall be selected on the basis of prior experience and tested material characteristics.
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On sample preparation and result

stabilization press

key to confirm

sample preparation completion.

Drying chamber’s lid gets closed

automatically, the drying process starts.

You can close the drying chamber by

pressing

pictogram (to be found at

the bottom of the screen), this also triggers

the drying process start.

Information on the drying process is

displayed, moisture analyzer proceeds to

carrying it out accordingly to set

parameters.

Required

mass

measurements and calculations of tested

sample moisture content are performed,

wherein the calculations are a result of

mass change. On process start, printout

header is sent to a selected interface

(accordingly to set printout options ­

parameter group DRYING PROCESS

REPORT/HEADER).

In course of a drying process current

weight results and information on the

process is displayed (test duration, drying

chamber temperature, etc.).

In course of a drying process (accordingly

to set printout options ­ parameter group

DRYING

PROCESS

REPORT/MEASUREMENT)

measurements are sent to a selected

communication port in a preset time

intervals (INTERVAL).

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key allows you to swap between displayed result type during the process.
Upon drying process completion, summary of the test is displayed, final moisture content result is held, drying chamber’s lid gets opened automatically. Printout footer is sent to a selected interface (accordingly to set printout options ­ parameter group DRYING PROCESS REPORT/FOOTER).

Drying process may be aborted at any time. In order to abort the process, press

key and

confirm completion by pressing key. Manual auto switch-off mode is an exception to the rule ­ for moisture analyzer working in this

mode, the drying process ends upon pressing

key, there is no need to confirm completion

by pressing key.

Report on drying is printed again by pressing key located in the bottom bar of the display. Report is also automatically saved in moisture analyzer’s memory in the drying reports database.

In order to return to the main screen of drying process settings press

key located in the

bottom bar of the display. Moisture analyzer returns to its initial state, completed process

summary is blanked. The moisture analyzer is ready to perform another test.

An example of drying report:

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19.1 End Result Prognosis This option enables estimating end result before drying process is completed. Based on characteristics of current drying curve, created online, moisture analyzer estimates the end result of drying process. It is an approximate result characterized with small error (about +/- 10% of the end result for most of the products and +/- 20% for products that require drying process to be longer such as: plastics, gels and materials containing more than 30% of water). This option is useful for users who need faster estimation of the drying process end result. The time of the prognosis process ranges between 15% and 40% of the standard drying time.
CAUTION: Do not open the weighing chamber during drying process while using prognosis option. It may distract the process and the calculations would be incorrect. Prognosis is finished when the drying chamber is opened and a suitable message is displayed.
Prior drying process using prognosis option, set the following parameters.
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1. Enable prognosis option in accordance with the following instructions:
2. In accordance with description in point 8.6.2., place the label with displayed prognosis on the home screen.
3. If the prognosis is to be printed with the measurement, enable its printing in the following settings: PRINTOUTS/REPORT FROM DRYING PROCESS/MEASUREMENT/PROGNOSIS.
4. On setting the above parameters you can start drying process by following the above description. On starting the drying process an additional button is displayed in the bottom part of
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the display. On pressing this button, a window with prognosis is displayed. In the initial stage of the drying process there is no result of prognosis yet and the status is displayed in the prognosis window.
5. When the intersection of the drying curve is found, the end result can be estimated. When calculated, it is displayed in the prognosis label.

6. If the result of prognosis meets your expectations, you can abort the drying process before its

completion. To do that, return to home screen and press

button.

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7. On drying process completion a footer of drying report containing status, end result and estimated result are printed. The estimated result is a result that would be achieved on reaching the criteria set by the user for a given process. An exemplary report from drying process containing prognosis result:
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20 Communication
COMMUNICATION menu is comprised within Parameters menu. It is accessed by pressing key. The balance can communicate with a peripheral device, wherein the communication is established via the following ports:
– COM 1 (RS232), – USB 1 type A, – USB 2 type B, – Ethernet, – Wi-Fi.
The ports can be configured using parameter group. To enter this submenu,
press key, next press “Communication” key.

20.1 RS-232 Port Settings Procedure:
– Select communication port . Set appropriate values.
The RS 232 ports enable the following setting of transmission parameters: – Baud rate – 2400, 4800, 9600, 19200, 38400, 57600, 115200 bit/s – Parity – None, Even, Odd

20.2 Ethernet Port Settings Procedure:

Select < –

Ethernet> communication port, next set appropriate values: DHCP – Yes ­ No IP Address – 192.168.0.2 Subnet mask – 255.255.255.0 Default gate – 192.168.0.1

CAUTION! The above presented settings serve information purposes only. Transmission parameters should be selected in accordance with the settings of customer’s local network.

Return to weighing mode and restart the device.

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20.3 Wi-Fi Port Settings
CAUTION! 1. Make sure that transmission parameters are accordant for your local network settings, 2. For correct communication via Wi-Fi, set port parameter for computer to value: <PERIPHERALS/COMPUTER/PORT/WIFI>, next set the parameters as described below.
Balance equipped with Wi-Fi module features a respective pictogram at the home screen in the top right-hand corner:

Pictogram for Wi-Fi network connection status:

No. Pictogram Overview

Balance connected, very strong signal

Balance connected, strong signal

Balance connected, poor signal

Balance connected, very poor signal

No connection (too poor signal or inaccessible selected network or

invalid connection parameters ­ password, IP, etc.)

Exemplary settings for Wi-Fi port:

CAUTION! The above presented settings serve information purposes only. Make sure that your transmission parameters are accordant for your local network settings.
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Procedure: – Select communication port
Enter parameter and set DHCP parameter value:
With DHCP set to NO value, enter manually: , , parameters. With DHCP set to YES value, the balance software automatically reads and displays data assigned by Wi-Fi router by means of which the balance is to be connected, Enter parameter and start network searching procedure. Upon completion, list of detected networks is displayed along with information on signal strength and channel number.
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Select network of your choice. Password window is displayed, enter the password using an on-screen keyboard.

window is displayed, connection procedure starts automatically.

Press

button to go one level up, parameter features sign

informing on the fact that the balance tries to connect the network,

For successfully established connection status turns to

status, respective pictogram is displayed (see pictogram overview above)

If it takes too long to establish connection it may be concluded that connection parameters are

References

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