GASTEC 7LAN Phosphine Detector Tube Instruction Manual

No.7LAN
Instructions for
Phosphine Detector Tube

FOR SAFE OPERATION :

Carefully read this manual and the instruction manual of your Gastec Gas Sampling Pump.
WARNING :

1. Use only Gastec detector tubes in a Gastec pump .
2.  Do not interchange or use non-Gastec parts or components in Gastec’s detector tube and pump system .
3. Using non-Gastec parts or components in Gastec’s detector tube and pump system or using a non-Gastec detector tube with a Gastec pump or using a Gastec detector tube with a non­ Gastec pump may damage your detector tube and pump system , or may cause serious injuries, or death to the end-user. It will also void all warranties, and guarantees regarding performance and data accuracy.

CAUTION : If you do not observe the following precautions, you may
suffer injuries or damage the product.

1. When breaking the tube ends, keep away from eyes.
2. Do not touch the broken glass tubes, broken pieces and reagent with bare hand(s) .
3. The sampling time represents the time necessary to draw the air sample through the tube.The tube must be positioned in the desired sampling area for the entire sampling time or until the flow finish indicator indicates the end of the sampling.

NOTES : For maintaining performance and reliability of the test results, observe the following.

1. Use Gastec Gas Sampling Pump together with Gastec Detector Tubes only for the purposes specified in the instruction manual of the detector tube.
2. Use this tube within the temperature range of 0- 40’C (32- 104’F).
3. Use this tube within the relative humidity range of O – 90%.
4. This tube may be interfered with by the coexisting gases. Please refer to the table “INTERFERENCES” below.
5. The shelf life and storage condition of the tube are marked on the label of the tube box.
6. If this tube is exposed under the direct sunlight, the original colour and discoloration may become pale, and inaccurate result may be given.

APPLICATION OF THE TUBE :

Use this tube for detecting Phosphine in the air or in industrial areas and for determining the environmental atmospheric condition .

SPECIFICATION :

(Because of Gastec’s commitment to continued improvement, specifications are subject to change without notice.)

Measuring Range| 0.04 — 0.06 ppm| 0.06 — 0.1 ppm| 0.1 — 2.0 ppm| 2.0 — 3.8 ppm| 3.8 — 8.4 ppm
---|---|---|---|---|---
Number of Pump Strokes| 4| 3| 2| 1| 1/2
Correction Factor| 0.4| 0.6| 1| 1.9| 4.2
Sampling Time| 1.5 minutes per pump stroke| 45 seconds
Detecting Limit| 0.015 ppm (n = 4)
Colour Change| Yellow →’ Pink
Reaction Principle| Phosphine reacts with the reagent to form intermediate material
which stains indicator pink.

Coefficient of Variance : 10% (for 0.1 to 2.0 ppm)
Shelf Life : Please refer to the validity date printed on the tube box.
Store the tubes in a dark and cool place.
CORRECTION FOR TEMPERATURE, HUMIDITY AND PRESSURE :
Temperature : No correction is required between 0 – 40’C (32- 104°F).
Humidity : No correction is required between O – 90% R.H.
Pressure : To correct for pressure, use the formula below
Tube Reading* (ppm) x 1013 (hPa)
Atmospheric Pressure (hPa)

• This value is after other correction(s), if any, are applied.

MEASUREMENT PROCEDURE:

1. For checking the leakage of the pump, insert a freshly sealed detector tube into pump.
   Follow instructions provided with the pump operating manual.

2. Break tips off a fresh detector tube with the tube tip breaker in the pump.

3. Insert the tube into the pump inlet with arrow ( ) on the tube pointing toward the pump.

4. Make certain the pump handle is all the way in. Align the guide marks on the pump body with the guide marks on the handle.

5. Pull the handle all the way out until it locks at one pump stroke (100 ml). Wait 1.5 minutes and confirm the completion of the sampling. Repeat the above sampling procedure one more time.

6. For smaller measurements less than 0.1 ppm, repeat the above sampling procedure 1 or 2 more times until the stain reaches the first calibration mark. For measurements higher than 2.0 ppm, prepare a fresh tube and perform one or a half pump stroke.

7. Read the concentration level at the interface where the stained reagent meets the unstained reagent.

8. If necessary , multiply the readings by the correction factors of pump strokes and atmospheric pressure .

INTERFERENCES :

Substance| Concentration| Interference| Changes colour by itself to
---|---|---|---
Arsine| ⪴.05 ppm| +| Pink (⪴0.03ppm)
Diborane| 10 times| No| No discolouration (90 ppm)
Hydrogen Chloride| ⪳2000 ppm| No| No discolouration (⪳2000 ppm)
Hydrogen Sulphide| ⪳1 ppm| No| No discolouration (⪳1 ppm)
Monosilane| ⪴1 ppm| +| No discolouration (⪳3 ppm)
Ammonia| 93 ppm| No| No discolouration (188 ppm)
Carbon Dioxide| 10%| No| No discolouration

This table of interference gases primarily expresses the interference of each coexisting gas in the concentration range that is equivalent to the target gas concentration. Therefore, the test result may show positive results due to other substances not listed in the table. If more information is needed, please contact us or our distributors in your territory.

DANGEROUS AND HAZARDOUS PROPERTIES :
Threshold Limit Value-Time Weighted Average by ACGIH (2023): 0.05 ppm
Threshold Limit Value-Ceiling by ACGIH (2023): 0.15 ppm

INSTRUCTIONS ON DISPOSAL :
The reagent of the tube does not use toxic substances. When disposing the tube regardless of whether it has been used or not, follow the rules and regulations of your local government.

WARRANTY:

If you have any ques tions regarding gas detection and the qual ity of the tubes, please feel free to contact your Gastec representatives.

Manufacturer : Gastec Corporation
8-8-6 Fukayanaka, Ayase-City, Kanagawa 252-1195, Japan
https://www.gastec.co.jp/
Telephone +81-467-79-3910 Facsimile +81-467-79-3979
IM007LANE1
Pr inted in Japan
24C1Z

References

• GASTEC CORPORATION | For all types of gas and vapour

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