SHIKAI 54000 CBD Double Strength Cream Instructions

: June 4, 2024
: SHIKAI

Table of Contents

SAFETY ANALYSIS – SUMMARY
Cannabinoid Analysis
Pesticide Analysis
Residual Solvents Analysis
Heavy Metals Analysis
Microbiology Analysis
Potency 20 – LOQ (0.01)
Heavy Metals
Mycotoxins
Pesticides FL V4
Residual Solvents – FL (CBD)
Moisture
Pathogenic Microbiology – SE (MicroArray)
Listeria Monocytogenes
Microbiology (qPCR)
References
Read User Manual Online (PDF format)
Download This Manual (PDF format)

SHIKAI Products PO Box 2866 Santa Rosa, Ca 95405
800-448-0298 707-544-0298 fax: 707-544-0266
info@shikai.com www.shikai.com

CBD Topical Product Guarantee

Product Name	CBD Double Strength Cream
Product Category	Topicals/Cosmetics (Not for consumption)

Instructions for
use/Preparation| Apply a small amount to the affected area. Use as needed throughout the day. Store in a cool dry place. Do not take it internally. Cannabidiol uses while pregnant or breastfeeding may be harmful.
CBD Source| CBD is sourced from hemp grown by federally authorized state pilot programs (e.g. Kentucky, Oregon, or Colorado’s R&D program) or approved
hemp program.
NOTE: This product is not intended to diagnose, treat, cure or prevent any disease
WARNING: The safety of this product has not been determined.
Batch Information|
Batch ID Number| 21251
Batch Size| 400 lbs
Units Produced per SKU| Item 54000 (2 oz): 2880 units
Manufacture date| 9/8/2021
Expiration date| 09/08/2023

SHIKAI 54000 CBD Double Strength Cream - sambol 1
Date: 09/08/2021
Hemp Quality Assurance Testing
CERTIFICATE OF ANALYSIS

SAMPLE NAME: CBD Double Strength Cream 21251_#19
Infused, Hemp Infused

CULTIVATOR / MANUFACTURER	DISTRIBUTOR / TESTED FOR
Business Name:	Business Name: Shikai Products
License Number:	License Number:
Address:	Address:

SAMPLE DETAIL
Batch Number: 21251
Sample ID: 210910N048
Date Collected: 09/10/2021
Date Received: 09/10/2021
Batch Size:
Sample Size:
Unit Mass:
Serving Size:

https://client.sclabs.com/verify/210910N048/

CANNABINOID ANALYSIS – SUMMARY

Total THC: Not Detected
Total CBD: 9.609 mg/g
Sum of Cannabinoids: 9.630 mg/g
Total Cannabinoids: 9.630 mg/g| Total THC/CBD is calculated using the following formulas to take into
account the loss of a carboxyl group during the decarboxylation step:
Total THC = ∆9THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))
Sum of Cannabinoids = ∆9THC + THCa + CBD + CBDa + CBG + CBGa +
THCV + THCVa + CBC + CBCa + CBDV + CBDVa + ∆8THC + CBL + CBN
Total Cannabinoids = (∆9THC+0.877THCa) + (CBD+0.877CBDa) +
(CBG+0.877CBGa) + (THCV+0.877THCVa) + (CBC+0.877CBCa) +
(CBDV+0.877CBDVa) + ∆8THC + CBL + CBN
---|---

SAFETY ANALYSIS – SUMMARY

Pesticides: ND
Microbiology (PCR): ND| Residual Solvents: ND
Microbiology (Plating): ND| Heavy Metals: ND
---|---|---

For quality assurance purposes. Not a Pre-Harvest Hemp Lab Test Report. These results relate only to the sample included in this report. This report shall not be reproduced, except in full, without the written approval of the laboratory.
Sample Certification: The action Limits used in this report are a compilation of guidance from state regulatory agencies in all states. Action limits for required tests are either state-specific or the lower of any conflicting state regulations based upon the panel requested.
Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS – Results within limits/specifications, FAIL – Results exceed limits/specifications.
References: limit of detection (LOD), the limit of quantification (LOQ), not detected (ND), not tested (NT), too numerous to count >250 CFU/plate (TNTC), colony-forming unit (CFU)

SHIKAI 54000 CBD Double Strength Cream - sambol 2

Cannabinoid Analysis

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).
Method: QSP 1157 – Analysis of Cannabinoids by HPLC-DAD

TOTAL THC: Not Detected
Total THC (∆9THC+0.877THCa)
TOTAL CBD: 9.609 mg/g
Total CBD (CBD+0.877CBDa)
TOTAL CANNABINOIDS: 9.630 mg/g
Total Cannabinoids (Total THC) + (Total CBD) + (Total CBG) + (Total THCV) + (Total CBC) + (Total CBDV) + ∆8THC + CBL + CBN

TOTAL CBG: ND
Total CBG (CBG+0.877CBGa)
TOTAL THCV: ND
Total THCV (THCV+0.877THCVa)
TOTAL CBC: ND
*Total CBC (CBC+0.877CBCa)
TOTAL CBDV: 0.021 mg/g*
Total CBDV (CBDV+0.877CBDVa)

CANNABINOID TEST RESULTS – 09/12/2021

COMPOUND| LOD/LOQ
(mg/g)| MEASUREMENT
UNCERTAINTY (mg/g)| RESULT
(mg/g)| RESULT
(%)
---|---|---|---|---
CBD| 0.004 / 0.011| ±0.4603| 10.| 0.9609
CBDV| 0.002 / 0.012| ±0.0011| 0.021| 0.0021
A9THC| 0.002 / 0.014| N/A| ND| ND
A8THC| 0.01 / 0.02| N/A| ND| ND
THCa| 0.001 / 0.005| N/A| ND| ND
THCV| 0.002 / 0.012| N/A| ND| ND
THCVa| 0.002 / 0.019| N/A| ND| ND
CBDa| 0.001 /0.026| N/A| ND| ND
CBDVa| 0.001 / 0.018| N/A| ND| ND
CBG| 0.002 / 0.006| N/A| ND| ND
CBGa| 0.002 / 0.007| N/A| ND| ND
CBL| 0.003 / 0.010| N/A| ND| ND
CBN| 0.001 /0.007| N/A| ND| ND
CBC| 0.003 / 0.010| N/A| ND| ND
ND
CBCa| 0.001 / 0.015| N/A| ND
SUM OF CANNABINOIDS| | | 9.630 mg/g| 0.963%

Pesticide Analysis

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).
*GC-MS utilized where indicated.
Method: QSP 1212 – Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 – Analysis of Pesticides by GC-MS

PESTICIDE TEST RESULTS – 09/11/2021 ND

COMPOUND| LOD/LOQ
(nig)| ACTION LIMIT
(nig)| MEASUREMENT
UNCERTAINTY (pg/g)| RESULT
(PS/g)
---|---|---|---|---
Abamectin| 0.03 / 0.10| 0.3| N/A| ND
Azoxystrobin| 0.01 /0.04| 40| N/A| ND
Bifenazate| 0.01 / 0.02| 5| N/A| ND
Bifenthrin| 0.01 / 0.02| 0.5| N/A| ND
Boscalid| 0.02 / 0.06| 10| N/A| ND
Chlorpyrifos| 0.02 / 0.06| LOD| N/A| ND
Cypermethrin| 0.1 /0.3| 1| N/A| ND
Etoxazole| 0.010 / 0.028| 2.| N/A| ND
Hexythiazox| 0.01 / 0.04| 2| N/A| ND
Imidacloprid| 0.01 /0.04| 3| N/A| ND
Malathion| 0.02 / 0.05| 5| N/A| ND
Myclobutanil| 0.03 / 0.1| 9| N/A| ND
Permethrin| 0.03 / 0.09| 20| N/A| ND
Piperonylbutoxide| 0.003 / 0.009| 8| N/A| ND
Propiconazole| 0.01 / 0.03| 20| N/A| ND
Spiromesifen| 0.02 / 0.05| 12| N/A| ND
Tebuconazole| 0.02 / 0.07| 2| N/A| ND
Trifloxystrobin| 0.01 /0.03| 30| N/A| ND

Residual Solvents Analysis

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC- MS).
Method: QSP 1204 – Analysis of Residual Solvents by GC-MS

RESIDUAL SOLVENTS TEST RESULTS – 09/12/2021 ND

COMPOUND| LOD/LOQ
(P9/9)| ACTION LIMIT
(P9/9)| MEASUREMENT
UNCERTAINTY (pg/g)| RESULT
(P9/9)
---|---|---|---|---
Propane| 10 / 20| 5000| N/A| ND
Butane| 10 / 50| 5000| N/A| ND
Pentane| 20 / 50| 5000| N/A| ND
Hexane| 2 / 5| 290| N/A| ND
Heptane| 20 / 60| 5000| N/A| ND
Benzene| 0.03 / 0.09| 1| N/A| ND
Toluene| 7 / 21| 890| N/A| ND
Total Xylenes| 50/ 160| 2170| N/A| ND
Methanol| 50 / 200| 3000| N/A| ND
Ethanol| 20 / 50| 5000| N/A| ND
Isopropyl Alcohol| 10 / 40| 5000| N/A| ND
Acetone| 20 / 50| 5000| N/A| ND
Ethyl ether| 20 / 50| 5000| N/A| ND
Ethylene Oxide| 0.3 / 0.8| 1| N/A| ND
Ethyl acetate| 20 / 60| 5000| N/A| ND
Chloroform| 0.1 / 0.2| 1| N/A| ND
Methylene chloride| 0.3 / 0.9| 1| N/A| ND
Trichloroethylene| 0.1 / 0.3| 1| N/A| ND
1,2-Dichloroethane| 0.05 / 0.1| 1| N/A| ND
Acetonitrile| 2 / 7| 410| N/A| ND

Heavy Metals Analysis

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).
Method: QSP 1160 – Analysis of Heavy Metals by ICP-MS

HEAVY METALS TEST RESULTS – 09/11/2021 ND

COMPOUND| LOD/LOQ
(μg/g)| ACTION LIMIT
(μg/g)| MEASUREMENT
UNCERTAINTY (μg/g)| RESULT
(μg/g)
---|---|---|---|---
Arsenic| 0.02 / 0.1| 0.42| N/A| ND
Cadmium| 0.02 / 0.05| 0.27| N/A| ND
Lead| 0.04 / 0.1| 0.5| N/A| ND
Mercury| 0.002 / 0.01| 0.4| N/A| ND

Microbiology Analysis

PCR AND PLATING
Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.
Method: QSP 1221 – Analysis of Microbiological Contaminants

Analysis conducted by 3M™ Petrifilm™ and plate counts of microbiological contaminants.
Method: QSP 6794 – Plating with 3M™ Petrifilm™

MICROBIOLOGY TEST RESULTS (PCR) – 09/14/2021 ND

COMPOUND	ACTION LIMIT (cfu/g)	RESULT (cfu/g)
Shiga toxin-producing Escherichia coli	Not Detected in 1g	ND
Salmonella spp.	Not Detected in 1g	ND
Bile-Tolerant Gram-Negative Bacteria	100	ND
Staphylococcus aureus	Not Detected in 1g	ND

MICROBIOLOGY TEST RESULTS (PLATING) – 09/14/2021 ND

COMPOUND	ACTION LIMIT (cfu/g)	RESULT (cfu/g)
Total Aerobic Bacteria	100	ND
Total Yeast and Mold	10	ND

logo2

721 Cortaro Dr.
Sun City Center, FL 33573
www.acslabcannabis.com
License No. 800025015
FL License # CMTL-0003
CLIA No. 10D1094068

Certicate of Analysis
Compliance Test

CBD Isolate Sample Matrix: CBD/HEMP Edibles (Ingestion)

https://portal.acslabcannabis.com/qr-coa- view?salt=QUFCTTMwN18yMTAwNjRDQ18wNjI4MjAyMV82MGRhMmZmYWVlMDNl

GENCANNA ACQUISITION CORP.
4274 COLBY ROAD
WINCHESTER, KY 40391
Batch # 210064CC
Batch Date: 2021-06-14
Extracted From: Industrial Hemp

Sampling Method: MSP 7.3.1 Test Reg
State: Florida

Order # G
EN210614-010045
Order Date: 2021-06-14
Sample # AABM307

Sampling Date: 2021-06-17
Lab Batch Date: 2021-06-17
Completion Date: 2021-06-28
Initial Gross Weight: 35.734 g

SHIKAI 54000 CBD Double Strength Cream - fig 2

Potency 20 – LOQ (0.01)

Specimen Weight: 58.810 mg

Analyte
CBD
CBDV
THCV
Exo-THC
THCVA
THCA-A
CBC
Delta-9 THC
CBCA
Delta-8 THC
Delta-10 THC
CBT
CBNA
CBN
CBL
CBGA
CBG
CBDVA
CBDA
Delta-8 THCV| LOD
(%)
0.000054
0.000065
0.000007
0.0002
0.000047
0.000032
0.000018
0.000013
0.000107
0.000026
0.000003
0.0002
0.000095
0.000014
0.000035
0.00008
0.000248
0.000014
0.00001
0.0002| LOQ
(%)
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.0
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01| Result
(mg/g)
997.70
1.71
0.28| (%)
99.77
0.17
0.03
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
---|---|---|---|---

Potency Summary

Total THC
None Detected| Total CBD
99.770%
---|---
Total CBG
None Detected| Total CBN
None Detected
Other Cannabinoids
0.199%| Total Cannabinoids
99.969%

Heavy Metals

Specimen Weight: 248.000 mg
Dilution Factor: 2.000
Passed
(ICP-MS)

Analyte	LOQ (ppb)	Action Level (ppb)	Result (ppb)
Arsenic (As)	100	1500	<LOQ
Lead (Pb)	100	500	<LOQ
Cadmium (Cd)	100	500	<LOQ
Mercury (Hg)	100	3000	<LOQ

Mycotoxins

Specimen Weight: 163.900 mg
Dilution Factor: 9.152
Passed
(LCMS)

Analyte	LOQ (ppb)	Action Level (ppb)	Result (ppb)
Aatoxin B1	6	20	<LOQ
Aatoxin G1	6	20	<LOQ
Ochratoxin A	12	20	<LOQ
Aatoxin B2	6	20	<LOQ
Aatoxin G2	6	20	<LOQ

Pesticides FL V4

Specimen Weight: 163.900 mg
Dilution Factor: 9.152
Passed
(LCMS/GCMS)

Analyte	LOQ (ppb)	Action Level (ppb)	Result (ppb)

Abamectin
Acequinocyl
Aldicarb
Bifenazate
Boscalid
Carbaryl
Chlorantraniliprole
Chlorfenapyr
Chlorpyrifos
Coumaphos
Cypermethrin
Diazinon
Dimethoate
Ethoprophos
Etoxazole
Fenoxycarb
Fipronil
Fludioxonil
Imazalil
Kresoxim Methyl
Metalaxyl
Methomyl
Mevinphos
Naled
Paclobutrazol
Permethrin
Piperonylbutoxide
Propiconazole
Pyrethrins
Spinetoram
Spiromesifen
Spiroxamine
Thiacloprid
Trioxystrobin
Acephate
Acetamiprid
Azoxystrobin
Bifenthrin
Captan
Carbofuran
Chlordane
Chlormequat Chloride
Clofentezine
Cyuthrin
Daminozide
Dichlorvos
Dimethomorph
Etofenprox
Fenhexamid
Fenpyroximate
Flonicamid
Hexythiazox
Imidacloprid
Malathion
Methiocarb
methyl-Parathion
Myclobutanil
Oxamyl
Pentachloronitrobenzene
Phosmet
Prallethrin
Propoxur
Pyridaben
Spinosad
Spirotetramat
Tebuconazole
Thiamethoxam| 28.23
48
30
30
10
10
10
30
30
48
30
30
30
30
30
30
30
48
30
30
10
30
10
30
30
30
30
30
30
10
30
30
30
30
30
30
10
30
30
10
10
10
30
30
30
30
48
30
10
30
30
30
30
30
30
10
30
30
10
30
30
30
30
30
30
30
30| 300
2000
100
3000
3000
500
3000
100
100
100
1000
200
100
100
1500
100
100
3000
100
1000
3000
100
100
500
100
1000
3000
1000
1000
3000
3000
100
100
3000
3000
3000
3000
500
3000
100
100
3000
500
1000
100
100
3000
100
3000
2000
2000
2000
3000
2000
100
100
3000
500
200
200
400
100
3000
3000
3000
1000
1000| <LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ

Residual Solvents – FL (CBD)

Specimen Weight: 105.700 mg
Dilution Factor: 1.000
Passed
(GCMS)

Analyte	LOQ (ppm)	Action Level (ppm)	Result (ppm)

1,1-Dichloroethene
Acetone
Benzene
Chloroform
Ethyl Acetate
Ethylene Oxide
Hexane
Methanol
Pentane
Toluene
Trichloroethylene
1,2-Dichloroethane
Acetonitrile
Butanes
Ethanol
Ethyl Ether
Heptane
Isopropyl alcohol
Methylene chloride
Propane
Total Xylenes| 0.16
2.08
0.02
0.04
1.11
0.1
1.17
0.69
2.08
2.92
0.49
0.04
1.17
2.5
2.78
1.39
1.39
1.39
2.43
5.83
2.92| 8
5000
2
60
5000
5
290
3000
5000
890
80
5
410
2000
5000
5000
5000
500
600
2100
2170| <LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
<LOQ
Passed
<LOQ
<LOQ
<LOQ
<LOQ

Moisture

Specimen Weight: N/A Dilution Factor: 1.000
Tested
(Moisture Meter)

Analyte	Action Level (%)	Result (%)
Moisture		0.71

Pathogenic Microbiology – SE (MicroArray)

Specimen Weight: 1039.190 mg
Dilution Factor: 1.000
Passed
(Micro Array)

Analyte	Result (cfu/g)
Salmonella	Absence in 1g
STEC E. Coli	Absence in 1g

Listeria Monocytogenes

Specimen Weight: 996.500 mg
Dilution Factor: 1.000
Passed
(qPCR)

Analyte	Action Level (cfu/g)	Result
Listeria Monocytogenes	1	Absence in 1g

Microbiology (qPCR)

Specimen Weight: 253.730 mg
Dilution Factor: 1.000
Passed
(qPCR)

Analyte	Result
Total Aerobic Count	Passed
Total Enterobacteriaceae	Passed
Total Coliform	Passed
Total Yeast/Mold	Passed

SHIKAI 54000 CBD Double Strength Cream - sambol 11

Definitions and Abbreviations used in this report: Total CBD = CBD + (CBD-A 0.877), Total THC = THCA-A 0.877 + Delta 9 THC, CBG Total = (CBGA 0.877)

CBG, CBN Total = (CBNA 0.877) + CBN, *Other Cannabinoids Total = CBC + CBDV
THCV + THCV-A, Total Detected Cannabinoids = CBD Total + CBG Total + CBN
Total + THC Total + CBC + CBDV + THCV + THCV-A, Analyte Details above show the Dry Weight Concentrations unless specified as 12% moisture concentration.
(mg/ml) = Milligrams per Milliliter, LOQ = Limit of Quantitation, LOD = Limit of Detection, Dilution = Dilution Factor (ppb) = Parts per Billion, (%) = Percent, (cfu/g) =
Colony Forming Unit per Gram (cfu/g) = Colony Forming Unit per Gram, , LOD = Limit of Detection, (µg/g) = Microgram per Gram (ppm) = Parts per Million, (ppm) =
(µg/g), (aw) = aw (area ratio) = Area Ratio, (mg/Kg) = Milligram per Kilogram , *Measurement of Uncertainty = +/- 5%
This report shall not be reproduced, without written approval, from ACS Laboratory. The results of this report relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Accredited by a third-party accrediting body as a competent testing laboratory pursuant to ISO/IEC 17025 of the International Organization for Standardization.