SKC Chek-Mate Air Sampling Calibrator User Guide

October 30, 2023
SKC

SKC Chek-Mate Air Sampling Calibrator User Guide

SKC Chek-Mate Air Sampling Calibrator

Personal sampling pumps are essential equipment for sampling airborne contaminants. However, determining airborne concentrations requires accurate knowledge of the volume of air sampled. Constancy of flow rate and equipment reliability are two important factors that affect air volume.

Some sample pumps feature a built-in rotameter, which is not a precision instrument and can provide only an approximation of pump flow rate. Other pumps have an electronic flow sensor built in, which can provide a more accurate flow rate. No matter how accurately the pump displays the flow rate, the flow rate through the sampling train should be measured with an electronic calibrator or a precision rotameter before and after sampling. The performance of any such calibrator should be traceable to a primary standard; periodic calibration by an accredited laboratory is recommended. Some electronic calibrators, such as CalChek®, provide advanced calibration options. The CalChek feature of the SKC chek-mate® Calibrator with CalChek (medium and high flow models) provides direct communication with CalChek-ready sample pumps such as the SKC AirChek TOUCH and Leland Legacy for automatic calibration. This Sample Setup Guide describes Calibrating a Pump Using a chek-mate Calibrator. For calibration with a film flowmeter (non-electronic), refer to Publication 1163.

Required Equipment

  1. An air sampling pump capable of sampling at the recommended flow rate with the sampling medium in line, such as:

    • SKC Pocket Pump TOUCH

    • SKC AirChek® Series (low flow applications require the All-in-One Low Flow
      Single/Adjustable Holder Cat. No. 224-27 or Constant Pressure Controller Cat. No. 224-26CPC and the Cat. No. 224-26 Series Adjustable Multiple-tube Low Flow Holder)

    • SKC AirLite (low flow applications require the All-in-One Low Flow Single/Adjustable Holder Cat. No. 224-27 or Constant Pressure Controller Cat. No. 224-26 Series Adjustable Multiple-tube Low Flow Holder)

    • SKC Leland Legacy®

    • SKC QuickTake® 30

  2. SKC chek-mate Calibrator, such as:

    • Low Flow chek-mate Calibrator Cat.
      Nos. 375-00205N, 375-00205, and 375-00205S

    • Medium Flow chek-mate Calibrator with CalChek Cat.
      Nos. 375-0550N, 375-0550, and 375-0550S

    • High Flow chek-mate Calibrator with CalChek Cat.
      Nos. 375-50300N, 375-50300, and 375-50300S

  3. Sampling medium as specified in the method*

  4. Any additional equipment specified in the method*

  5. CalChek Communication Cable Cat. No. 375-200 for CalChek calibration, for use with chek-mate Calibrator with CalChek and AirChek TOUCH and Leland Legacy Sample Pumps

  6. Pulsation Dampener Cat. No. 375-150, required for calibration of high flow pumps and CalChek automatic calibration (High Flow chek-mate Calibrator with CalChek used with Leland Legacy Sample Pump)

  • Refer to the method and to the related Sample Setup Guide for preparing a sampling train: Pre-filter and Tube Publication 1164, Impingers Publication 1165, Filters and Cyclones Publication 1166, Air Sample Bags Publication 1167, Single Sorbent Sample

Introduction
This Sample Setup Guide provides general information about calibrating an air sampling pump using the chek-mate Calibrator. For details about the operation of a particular calibrator or sample pump, refer to the individual operating instructions.

1. Setting Up the Electronic Calibrator

Turn on the chek-mate Calibrator by pressing the on/off button (Figure 1).

SKC Chek-Mate Air Sampling Calibrator - Fig. 1

2. Setting Up the Calibration Train

Manual Calibration (Figure 2)
Allow the pump to equilibrate from one temperature to another and to run for 5 minutes before calibrating. Prepare an appropriate train as specified in the method. Ensure that the pump is in the appropriate mode (high or low flow for the desired flow rate) and that any necessary flow accessories, such as a constant pressure controller (CPC) and low flow tube holder or All-in-One, are in place. Use flexible tubing to connect the calibrator outlet or suction port to the inlet of a representative sample medium. Note : When using the High Flow chek-mate Calibrator, Pulsation Dampener Cat. No. 375-150 is required in line. See calibrator and pump operating instructions.

Use a second length of tubing to connect the sample medium outlet to the pump inlet. Use the shortest length possible to avoid kinks and bends.

SKC Chek-Mate Air Sampling Calibrator - Fig. 2

Jarless calibration method (chek-mate Calibrator only): If a sampler does not have a calibration adapter, attach the sampler/medium to the chek-mate inlet using the shortest length of tubing possible and the sample pump to the chek- mate outlet (suction port). See Figure 3. Note: If using the High Flow chek- mate Calibrator, place Pulsation Dampener Cat. No. 375-150 in line between calibrator and pump. Proceed with calibration per the instructions in Step 2 and pump operating instructions.

SKC Chek-Mate Air Sampling Calibrator - Fig. 3

If Using CalChek Feature ­ AirChek TOUCH and Leland Legacy Sample Pumps (Figures 4 and 5)
Allow the pump to run 5 minutes to stabilize. Prepare an appropriate train as specified in the method. Use flexible tubing to connect the calibrator outlet or suction port to the inlet of a representative sample medium (see Note below). Use a second length of tubing to connect the sample medium outlet to the pump inlet. Use the shortest length possible to avoid kinks and bends.

Note : CalChek single-point calibration is performed with a sample medium in line but also requires Pulsation Dampener Cat. No. 375-150 in line with the High Flow chek-mate Calibrator and Leland Legacy Pump.

AirChek TOUCH pump : CalChek calibration is performed with the pump installed on a Standard Charging Cradle or Charging e-Cradle that must be plugged into a standard wall outlet (100-240 V). Prepare the cradle by inserting the connector end of the power supply cable into the power port on the side of the cradle, and then inserting the wall cube end into a standard wall outlet (100-240 V). Align the contacts on the bottom edge of the pump with the contacts in the cradle and insert the pump in the cradle. Insert one end of the CalChek Communication Cable in the CalChek interface socket on the side of the chek-mate Calibrator with CalChek and the other end in the CalChek port on the back of the cradle.

Leland Legacy pump : Insert one end of the CalChek Communication Cable in the CalChek interface socket on the side of the chek-mate Calibrator with CalChek and the other end in the data port on top of the pump.

SKC Chek-Mate Air Sampling Calibrator - Fig. 4

SKC Chek-Mate Air Sampling Calibrator - Fig. 5

3. Calibrating the Flow Rate

Manual Calibration
Ensure that the pump has run for 5 minutes before calibrating. Following operating instructions for the calibrator, adjust the flow rate on the pump until the appropriate flow rate is displayed. Take a minimum of three readings to verify flow. Do not adjust the flow any further. Record flow rate as the pre-sample flow rate.

If Using CalChek Feature ­ AirChek TOUCH and Leland Legacy Sample Pumps
Ensure that the pump has run for 5 minutes before calibrating. Set the pump to CalChek single-point calibration (see pump operating instructions).

The calibrator will automatically calibrate the pump at a set flow.

4. Setting Up the Sampling Train

When ready to begin sampling, remove the calibrator (and pulsation dampener if used) and representative sampling medium from the calibration train. If CalChek was used, remove the CalChek Communication Cable. Set these items aside to verify flow after sampling. Place a new unexposed sampling medium of the same type into the train.

5. Sampling

Attach the sampling medium to a worker’s clothing in the breathing zone and the pump to the worker’s belt. Run the pump and note sampling start time.

6. After Sampling

At the end of the sampling period, turn off the pump and note sampling end time. Remove the sampling medium and seal it. Refer to the sampling medium operating instructions for details. Record pertinent sampling information.

7. Verifying Flow

Reinstate the representative sampling medium and the calibrator (and pulsation dampener if used) in the sampling train. If using an AirChek TOUCH or Leland Legacy with CalChek, reinstall the CalChek Communication Cable (see “If Using CalChek Feature” in Step 2). Take three flow readings as outlined in Step 3 and record this value as the post-sample flow rate. Do not adjust pump flow rate. Compare the pre- and post-sample flow rates. Note in sampling documentation if the values differ by more than ± 5%. Report sample time and other relevant data to the laboratory.

8. Transporting Samples

Send the sealed sampling medium, blanks, and pertinent sampling information to a laboratory for analysis. Consult sampling medium operating instructions for details.

Copyright 1997 – 2022

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SKC Inc.
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714-992-2780

Publication 1366 Rev 221108

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