HANNA HALO2 Wireless Refillable pH Tester for Wine Instruction Manual

June 4, 2024
HANNA

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HANNA HALO2 Wireless Refillable pH Tester for Wine

HANNA-HALO2-Wireless-Refillable-pH-Tester-for-Wine-
PRODUCT

Dear Customer

Thank you for choosing a Hanna Instruments product. Please read this instruction manual carefully before using this instrument. This manual will provide you with the necessary information for the correct use of this instrument, as well as a precise idea of its versatility. If you need additional technical information, do not hesitate to e‑mail us at tech@hannainst.com or view our contact list at www.hannainst.com

PRELIMINARY EXAMINATION

Remove the tester and accessories from the packaging and examine them carefully. For further assistance, please contact your local Hanna Instruments office or email us at tech@hannainst.com

Each HI9810332 is supplied with a starter kit consisting of

  • pH 3.00 buffer solution, 20 mL sachet (2 pcs.)
  • pH 7.01 buffer solution, 20 mL sachet (2 pcs.)
  • Cleaning solution for wine deposits, 20 mL sachet (1 pc.)
  • Cleaning solution for wine stains, 20 mL sachet (1 pc.)
  • Electrode storage solution, 13 mL dropper bottle (1 pc.)
  • Electrolyte refill solution, 30 mL
  • Pipette
  • 3V Lithium battery – CR2032
  • Instrument quality certificate and Instruction manual

Note: Save all packing material until you are sure that the tester works correctly. Any damaged or defective item must be returned in its original packing material with the supplied accessories.

SPECIFICATIONS

HANNA-HALO2-Wireless-Refillable-pH-Tester-for-Wine-
FIG-1

  • Available with Hanna Lab App
  • Measuring outside the recommended operating temperature range may damage the gel electrolyte and void the product warranty.

Note: The tester can display measurements from –2.00 to 16.00 pH. Measurements outside of the pH range will flash. In this case assess the integrity of the tester and the type of measured sample.

GENERAL DESCRIPTION & INTENDED USE

  • HI9810332 is a professional wireless pH tester, part of the Hanna Instruments HALO2 family.
  • The integrated Bluetooth module allows the tester to be connected to a compatible smart device with the Hanna Lab App.
  • The tester has a compact, waterproof casing, and automatic pH calibration at up to three points, or four points when used with the Hanna Lab App.
  • Automatically compensated temperature readings are displayed on a large LCD.
  • Accurate and easy to use, the tester is designed to measure the pH at each step of the winemaking process from pre‑fermentation and fermentation to post‑fermentation and bottling.

Operating Modes

The HI9810332 can be used as a stand‑alone pH tester or connected to the Hanna Lab App. The Hanna Lab App turns a compatible smart device into a full- featured pH meter. Features include electrode condition, GLP with time-stamp, live readings, mV resolution, manual temperature compensation, stability criteria, calibration reminder, pH (mV) and temperature alarms, tester ID, and data sharing.

Probe Features

The HI9810332 features a non-porous glass body that is easy to clean. Specialized low-temperature (LT) pH glass ensures fast stabilization and accurate results at lower temperatures. The domed tip allows a large surface area to be in contact with the wine sample. The double junction design presents a silver-free electrolyte solution interacting with the sample, making the electrode less susceptible to clogging and guaranteeing a fast response and stable reading. A built-in temperature sensor at the tip of the pH electrode allows for rapid determination of the sample temperature and a high-accuracy temperature reading. Polyethylene (PE) movable sleeve with Clogging Prevention System (CPS™). The sleeve is part of the outer ground glass junction. The PE material repels solids and prevents clogging. Additionally, the sleeve can be moved and the ground glass surface cleaned, resulting in faster response times and stable readings.

FUNCTIONAL DESCRIPTION & LCD DISPLAY

Front & Back view

HANNA-HALO2-Wireless-Refillable-pH-Tester-for-Wine-
FIG-2

LCD display

  1. Calibration indicator
  2. Stability indicator
  3. Battery percentage indicator
  4. Battery icon
  5. Bluetooth icon
  6. Temperature compensation
  7. Second LCD line
  8. Temperature unit
  9. First LCD line
  10. Measurement unit

GENERAL OPERATIONS

Turning the Tester On & Off

  • Turn the tester face down. Rotate the battery cover on the back of the tester counterclockwise and set it aside. Remove the battery insulation film.
  • Press the ON/OFF button to turn the tester on or off. The initialization screen displays all LCD segments, followed by the battery percentage. The tester enters measurement mode. Before the tester turns off, “OFF PWR” is displayed briefly.
  • Press and hold the ON/OFF button to turn the tester off when connected to Bluetooth.

Battery Replacement

  1. Turn off the tester. Turn the tester face down and rotate the battery cover counterclockwise.
  2. Set the battery cover aside. Press the metallic pin to push the old battery out.
  3. Place the new battery with a positive (+) sign facing out.
  4. Reset the date and time in setup, or connect to the Hanna Lab App to update it automatically.
  5. Align the mark on the cover with the open lock icon ( ) on the case. Rotate the cover clockwise until the mark on the cover aligns with the closed lock icon ( ).

Note: Only use specified battery type. Dispose of old batteries in accordance with local regulations.

SETUP

The Setup button is located inside the battery compartment. After the Setup configuration, replace the cover.

Setup Menu Navigation

  • Press the Setup button to enter Setup mode and navigate menu items.
  • To exit Setup mode, press the Setup button after the “SEt TIME” option is displayed.
  • Press the ON/OFF button to configure menu item options.

Temperature Unit

Option: °Cor°F

  • Press the ON/OFF button to select desired temperature unit.

Auto-Off Interval

HANNA-HALO2-Wireless-Refillable-pH-Tester-for-Wine-
FIG-9

  • Option: 8, 60 min., or “—-” (disabled)
  • Press the ON/OFF button to select the desired interval.
  • To save battery life, after the selected auto-off interval has elapsed, the tester will automatically turn off.
Calibration Points
  • Option: 2P or 3P
  • Press the ON/OFF button to select between up to two- or up to three-point calibration.

Buffer Set

  • Option: 7.01 pH (Hanna) or 6.86 pH (NIST)
  • Press the ON/OFF button to select the calibration buffer set (Hanna or NIST).

pH Resolution

  • Option: 0.01 pH or 0.1 pH
  • Press the ON/OFF button to select resolution.

Bluetooth Wireless Mode

  • Option: On, PAlr, or OFF
  • Press the ON/OFF button to select the Bluetooth option of staff-up.

Bluetooth Pairing

  • Option: dEL PAIr
  • Press the ON/OFF button to delete the saved paired device.

Date & Time

  • Option: Set TIME
  • Press the ON/OFF button to set the date and time.
  • Option: YEAR, MO, DAY, HOUR, and MIN
  • Use the Setup button to select the option and press the ON/OFF button to change the selected option.

BLUETOOTH

With “PAIr BLU” or “On BLU” selected in Setup, the Bluetooth icon (&) will blink for up to 45 seconds, indicating the tester is in discoverable mode. Once connected, the icon will stop blinking. If not connected, the icon is not displayed.

  • Select “On BLU”, to enable Bluetooth without bonding.
  • Select “PAIr BLU”, to enable Bluetooth with bonding. A 6-digit bonding pin is displayed the first time the tester and smart device are paired. Once the devices are paired, the bonding pin is not required when reconnected.
  • Select “OFF BLU”, to disable Bluetooth.
  • Select “dEL PAIR”, to delete all paired devices. If PAIr BLU is enabled, a bonding pin will need to be re-entered.

HANNA LAB APPLICATION

  • The Hanna Lab App is available on the App Store® and on Google Play.1
  • Consult the Help section of the application for information on calibration, measurement, data logging, and sharing.
  • When the tester is in discoverable mode, it will appear in the list of “Available Devices”.
  • Within the application, tap “Connect” to pair the tester with the device. All readings are transmitted directly to the application.

Tag a Measurement

  • Once connected to the application, the ON/OFF button can be pressed to tag the current reading.
  • Press the ON/OFF button from measurement mode. The display shows “SEt TAG”, followed by “- TAG”.
  • The reading on the application will flash green and the note icon ( ) will be displayed. Tap the note icon ( ) to add an annotation.

CALIBRATION

Preparation & Guidelines

  1. Unscrew the top collar to vent the cap before removing the probe from the plastic storage tube. Save the cap for probe storage.
  2. Rinse off any storage solution or salts that may be on the body.
  3. Verify there is solution inside the pH bulb by shaking the probe down to restore continuity as the solution may have moved up the stem during shipping.
  4. For best results, use a rinse beaker and a separate calibration beaker for each buffer. Discard rinsing buffers after use.

Procedure

  • For most applications, it is recommended to start with pH 7.01 buffer (or pH 6.86).
  • To restore factory defaults, press and hold the ON/OFF button. “CAL CLR” is displayed.

Note: It is recommended to calibrate the electrode with buffers at the temperature it will be used at.

Stand-Alone Tester (Up to Three-Point Calibration)

  1. Rinse the electrode tip with purified water and blot dry. Then rinse with the buffer being used for calibration.
  2. Press and hold the ON/OFF button until “CAL MODE” is displayed.
  3. When “7.01 USE” or “6.86 USE” is displayed with the “CAL” tag blinking, place the tip of the electrode in the correct buffer.
  4. When the buffer has been recognized, “REC“ is displayed.
  5. “WAIT” is displayed with the stability indicator ( ) blinking until the reading is stable.
  6. Wait until the measurement is stored and the stability indicator disappears.
  7. To save a one-point calibration and return to measurement mode, press the ON/OFF button. “CAL SAVE” is displayed briefly.

With 2P option selected

  1. Place the tip of the electrode in the second buffer rinse beaker, then in the second calibration buffer. Wait until the measurement is stored and the stability indicator disappears.
  2. After the second point has been stored, “CAL SAVE” is displayed briefly and the tester will return to measurement mode automatically.

With 3P option selected

  1. Place the tip of the electrode in the second buffer rinse beaker, then in the second calibration buffer. Wait until the measurement is stored and the stability indicator disappears.
  2. Place the tip of the electrode in the third buffer rinse beaker, then in the third calibration buffer. Wait until the measurement is stored and the stability indicator disappears.
  3. After the third point has been stored, “CAL SAVE” is displayed briefly and the tester will return to measurement mode automatically.

With Hanna Lab App (Up to Four-Point Calibration)

  • Connect the tester to the Hanna Lab App and follow the calibration procedure.
  • See the App Help section for the calibration procedure.

CARE & MAINTENANCE

  • Never immerse the tester over the maximum immersion level.
  • Fresh buffers should be used for each calibration. Once the sachets are opened the buffer value can change over time.
  • If the electrode is slow or sluggish, soak it in the cleaning solution for 20 minutes. Rinse with water and hydrate the electrode in storage solution for a minimum of 30 minutes before calibrating.
  • If measurements are taken successively, rinse the probe thoroughly in distilled or deionized water to eliminate cross‑contamination between measurements.

Refilling the Electrode

  • If the filling solution (electrolyte) is more than 1 cm (½”) below the fill hole, add HI7082 3.5M KCl electrolyte fill solution for double junction electrodes.
  • Unscrew the fill hole cover during measurements so the liquid reference junction maintains an outward flow of electrolyte.
  • The reference junction may be cleaned by lifting the PTFE sleeve. Refill sensor with fresh HI7082 after replacing sleeve.

Storage

To ensure a quick response, the glass tip and junction should be kept hydrated.

  1. When not in use, add a few drops of storage solution to the storage cap. If a storage solution is not available, pH 3.00 or pH 7.01 buffer can be used.
  2. Note: Do not store the electrode in distilled or deionized water.
  3. Place the probe tip into the cap and gently tighten the collar.

WARNING & ERROR MESSAGES

HANNA-HALO2-Wireless-Refillable-pH-Tester-for-Wine-
FIG-29

ABBREVIATIONS

  • ATC: Automatic Temperature Compensation
  • GLP: Good Laboratory Practice
  • MTC: Manual Temperature Compensation
  • NIST: National Institute of Standards and Technology

ACCESSORIES

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FIG-31

RECOMMENDATIONS FOR USERS

Before using this product, make sure it is entirely suitable for your specific application and for the environment in which it is used. Any variation introduced by the user to the supplied equipment may degrade the tester’s performance. For your and the tester’s safety do not use or store it in hazardous environments.

WARRANTY

HI9810332 is warranted for a period of one year against defects in workmanship and materials when used for its intended purpose and maintained according to instructions. This warranty is limited to repair or replacement free of charge. Damage due to accidents, misuse, tampering, or lack of prescribed maintenance is not covered. If service is required, contact your local Hanna Instruments office. If under warranty, report the model number, date of purchase, serial number, and the nature of the problem. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the tester is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization (RGA) number from the Technical Service department and then send it with shipping costs prepaid. When shipping any product, make sure it is shipped back in compliance with shipping regulations, thoroughly cleaned and free of any chemicals, and properly packaged for complete protection.

CERTIFICATION

All Hanna Instruments conform to the CE European Directives. Disposal of Electrical and Electronic Equipment. The product should not be treated as household waste. Instead, hand it over to the appropriate collection point for the recycling of electrical and electronic equipment, which will conserve natural resources. Disposal of waste batteries. This product contains batteries, do not dispose of them with other household waste. Hand them over to the appropriate collection point for recycling. Ensuring proper product and battery disposal prevents potential negative consequences for the environment and human health. For more information, contact your city, your local household waste disposal service, or the place of purchase.

Regulatory Notices for stand-alone, Bluetooth, low-energy modules

All modules have identical operations. All references to US FCC Rules and Canadian RSS standards on device classification and operation, listed here under BMD-300 Module, apply to all models noted here. Remove the battery cover to check the installed module.

BMD-300 Module

United States (FCC) FCC ID: 2AA9B04

This device complies with FCC Rules, Part 15, Subpart C “Intentional Radiators” and Subpart B, Chapter §15.105. This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant to part 15 of the FCC Rules. These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment. This equipment generates, uses, and can radiate radio frequency energy and, if not installed and used in accordance with the instruction manual, may cause harmful interference to radio communications. Operation of this equipment in a residential area is likely to cause harmful interference in which case, users are required to correct the interference at their own expense.

Canada (ISED) IC: 12208A-04

This device complies with Industry Canada license exempt RSS standard(s). Operation is subject to the following two conditions: (1) this device may not cause interference, and (2) this device must accept any interference, including interference that may cause undesired operation of the device. Le présent appareil est conforme aux CNR d’Industrie Canada applicables aux appareils radio exempts de licence. L’exploitation est autorisée aux deux conditions suivantes: (1) l’appareil ne doit pas produire de brouillage, et (2) l’utilisateur de l’appareil doit accepter tout brouillage radioélectrique subi, même si le brouillage est susceptible d’en compromettre le fonctionnement.

Australia / New Zealand (RCM) BMD-300 complies with the AS/NZS 4268:2017.
Japan (MIC)

| South Korea (KCC)  R-CRM-Rgd-BMD-300
Brazil (ANATEL): Contains ANATEL-approved module # 00820-21-05903.| Mexico (IFETEL): Este equipo contiene el módulo con IFT #: NYCE/CT/0146/17/TS.

BMD-350 Module

United States (FCC) FCC ID: 2AA9B05| Canada (ISED) IC: 12208A-05
Japan (MIC) | Australia / New Zealand (RCM) BMD-350 complies with the AS/NZS 4268:2017
Eurasia (EAC)          EAЭC N RU Д-US.HA27.B.00650/18| Brazil (ANATEL) Contains ANATEL-approved module # 00857-21-05903
China (SRRC) CMIIT ID: 2018DJ7255| Mexico (IFETEL) Este equipo contiene el módulo con IFT #: RCPRIBM18-1491

ANNA-B112 Module

United States (FCC) FCC ID: XPYANNAB1| Canada (ISED) IC: 8595A-ANNAB1
Contains Transmitter Module

Taiwan (NCC)  CCAI18LP2200T2

| South Korea (KCC)  R-C-ULX-ANNA-B112
South Africa (ICASA) ICASA TA-2019/1203 Approved| China (SRRC) CMIIT ID: 2021DJ6698
Australia / New Zealand (ACMA) ANNA-B1 complies with AS/NZS 4268:2012 standard
Japan (MIC)

The module complies with the Japanese Technical Regulation Conformity Certification of Specified Japan (MIC) Radio Equipment (ordinance of MPT N°. 37, 1981), Article 2, Paragraph 1, Item 19 “2.4 GHz band wide band low power data communication system”.

Brazil (ANATEL) This equipment operates on a secondary basis and, consequently, must accept harmful interference, including from stations of the same kind, and may not cause harmful interference to systems operating on a primary basis.

App Store is a trademark of Apple, Inc.
Google Play and the Google Play logo are trademarks of Google LLC.

Hanna Instruments reserves the right to modify the design, construction, or appearance of its products without advance notice.

World Headquarters

  • Hanna Instruments Inc.
  • ADDRESS: Highland Industrial Park 584 Park East Drive Woonsocket, RI 02895 USA
  • www.hannainst.com

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