AQUALABO PF-CAP-C-00141 Optod Numerical Sensor User Manual

AQUALABO PF-CAP-C-00141 Optod Numerical Sensor

General
In order to maintain and ensure the good working order of the OPTOD Plastic sensor, users must comply with the safety precautions and warnings featured in this manual.

Assembly and activation:

• Assembly, electrical connection, activation, operation and maintenance of the measuring system must only be carried out by specialist personnel authorized by the user of the facilities.
• Trained personnel must be familiar with and comply with the instructions in this manual.
• Make sure the power supply complies with the specifications before connecting the device.
• A clearly-labeled power switch must be installed near the device.
• Check all connections before turning the power on.
• Do not attempt to use damaged equipment: it may represent a hazard and should be labeled as faulty.
• Repairs must only be carried out by the manufacturer or by AQUALABO’s after-sales service department.

Marking on the body of the sensor:
The marking on the body of the sensor indicates the serial number of the sensor (for traceability) and the LOGO CE.

X : version

YYYYY : number

3| CE mark

Characteristics

Technical characteristics.
The technical characteristics can be modified without advance notice.

Measures

Measure principle| Optical measure by luminescence

Measure ranges

| 0,00 to 20,00 mg/L

0,00 to 20,00 ppm

0-200%

Resolution| 0,01

Accuracy

| +/- 0,1mg/L

+/- 0,1 ppm

+/- 1 % (+/-5% if EMI Perturbations are more than 10V/m)

The sensor must be fully immerged to ensure maximum precision

Limit of detection| 0.7 %
Limit of quantification| 2.2 %
Repeatability (100% Sat)| 0.2 %
Linearity| >0.99
Response time| 0-> 100 %; T90< 40s

100 -> 0%; T90< 65 s

Frequency of recommended measure| >5 s
Water Flow| no movement required for measurement
Temperature compensation| Via NTC
Temperature| 0.00-50.00 °C

Accuracy: +/- 0.5 °C

Stocking temperature| – 10°C to + 60°C
Sensor

Dimensions| Standard version: Diameter: 27 mm ; length : 143 mm

Longer version: Diameter: 27 mm ; length : 166 mm

Weight| 300 g (sensor + cable 3 m)

Wetted material

| Black POMC, PVC

Cable: polyurethane jacket Steam gland: Polyamide

Patch with active material (black) – DO DISK : Optical isolation silicon

DO disk

| No cross-sensitivity with:

pH 1 – 14; CO2, H2S, SO2

Cross-sensitivity to Organic solvents, such as acetone, toluene, chloroform or methylene chloride

Chlorine gas

Maximum pressure| 5 bars
IP classification| IP68
Connection| 9 armoured connectors, polyurethane jacket, bare-wire
Sensor cable| Standard: 3, 7 and 15 m (other length on request).

100 m Max.

CE compliance.
Pursuant to the article 11 of the directive 89 / 336 / EEC relative to the electromagnetic compatibility.
We declare that the digital sensor of the range DIGISENS sensor OPTOD was tested and declared in compliance with the European standards:

Standard tests: NF EN IEC 61326-1: 2021-06
NF EN IEC 61326-1 (2021-06)
Electrical equipment for measurement, control and laboratory use – EMC requirements –
Part 1: General requirements.
2.2. NORMATIVE REFERENCES [1] NF EN 55011: 2016-06 +/A1 : 2017-06 +/A2 : 2021-04
Industrial, scientific and medical equipment – Radio-frequency disturbance characteristics – Limits and methods of measurement.
Immunity: Radiated immunity EN 61000-4-3 Industrial environment – Criteria A
ESD (Electrostatic discharge) EN 61000-4-2 Industrial environment – Criteria B
RF Common mode EN 61000-4-6 Industrial environment – Criteria A
Surge EN 61000-4-5 Industrial environment – Criteria B
Fast Transients EN 61000-4-4 Industrial environment – Criteria B
Disturbance: EN 55011B
Radiated emissions – EN 55011 Group 1 – Class A
Conducted emissions – EN 55011 Group 1 – Class A

Description.

Product overview
The OPTOD dissolved oxygen sensor applies the luminescence-based optical measurement technology and measures reliably and accurately without requiring calibration. With no consumables or maintenance required, the OPTOD sensor gives an immediate return on the investment. The only intervention required is to replace the DO disk every two years. Since it does not consume oxygen, the OPTOD sensor can be used in all media; even when there is a very weak flow of water.

The OPTOD sensor offers the following advantages:

• Low operating costs due to reduced maintenance work (no electrolyte changes)
• Greater calibration intervals due to low drift behaviour
• No polarization voltage required
• High measuring accuracy, even for low concentrations
• Rapid response times
• No minimum inflow (no oxygen consumption);

The sensor features excellent interference immunity thanks to the integrated preamplifier and digital signal processing. The measured value for dissolved oxygen is automatically compensated with the temperature, air pressure, and salinity (salt content), and transferred without interference to the connected display unit and controller via a digital interface. The membrane cap is easy to replace, meaning the sensor is very easy to maintain. The current calibration data is saved directly in the sensor electronics. As a result, the system’s Plug and Play function is enabled without recalibration. The sensor also includes a log book containing the last ten successful calibrations in the form of a ring buffer.

Applications
The compact and robust plastic sensor is particularly well suited to the following typical areas of application:

• Monitoring of surface waters, coastal waters, aquariums,
• Fish farming: closed containment, offshore,
• Fish farming, aquaculture,

**Construction and dimensions.

**

1. Protective strainer (2 versions: standard and longer)
2. DODISK on plastic support
3. DODISK Gasket
4. Gasket
5. Sensor’s body with electronic part
6. Cable gland
7. Securely connected connection cable

Communication.

Modbus RTU registers.
The link protocol must correspond to MODBUS RTU. See document:

• Modbus_over_serial_line_V1_02.pdf

• Modbus_Application_Protocol_V1_1a.pdf

• Modbus memory for PONSEL digital Sensors:
  SENSOR_TramesCom_xxx_UK.xls (refer to www.aqualabo.fr)
  The Modbus memory plane is identical for each parameter of the Sensors.
  The Modbus protocol for the Sensors allows you to measure the parameter (+ temperature) of the Sensor and to calibrate the parameter (+ temperature). Furthermore, there are certain numbers of functions such as:

• Select the averaging value

• Read the Sensor description

•  Return to default coefficients

• Modify the Sensor address

• Information on measures conducted (Out Of Specification measures, measures in progress, etc.).

• Date and name of the operator who performed the calibration

• etc.
  To have more information on the open PONSEL’s Modbus protocol please consult the last version of the following documents:

• the pdf file: Modbus_SpecificationsVxxx-EN

• the excel file: Digital sensor Frame_XXX_UK

SDI12 frame.
A list of SDI12 registers is available for network communication. Refer to www.aqualabo.fr for more information.

Compensation
Influences on the measurement.
The oxygen measurement is dependent on parameters:

• The temperature of the measurement medium
• The air pressure (atmospheric pressure)
• The salinity of the measurement medium
  The degree of solubility of oxygen in water is dependent on the temperature, the salinity, and
  the air pressure. This dependency is stored in the sensor’s measurement electronics in the
  form of functions. The sensor can therefore determine the oxygen concentration of the measurement medium, in order to digitally transmit the influencing factors above, in compensated form, to the transmitter/controller.

Temperature compensation.
The temperature compensation is automatic and managed directly by the sensor via the integrated sensor of temperature (NTC).

Atmospheric pressure.
With the most frequently used calibration method – end value calibration of the sensor in water
vapor-saturated air – the air pressure must be taken into account.
For this purpose, the air pressure can, for example, be transmitted to the sensor by the way of your terminal, where it is saved.
By default, the value of the atmospheric used for the compensation is 1013 hPa.

Salinity.
The value for the salinity of the measurement medium could be transmitted to the sensor by the way of your terminal.
By default, the value of the salinity used for the compensation is 0 g/Kg.

Sampling rate
Optical oxygen sensors do not carry out any continuous measurements. To extend the operating life of the optical membrane, the measurement interval can be set to a value superior to 10 seconds.

Installation.

Sensor installation option
For the installation of the sensors in condition of immersion or in-pipe insertion, we advise to use accessories adapted and proposed by AQUALABO.

Accessories for immersion installation.
In immersion condition, it is necessary to maintain the sensor by the body and not to leave the sensor suspended by the cable at the risk of damaging the sensor AQUALABO proposes a range or pole (short and long version) in order to install the sensor in open basins. It can be positioned a considerable distance from the basin edge with the bracket suspended on a chain, for example. Please note the following when planning your set-up:

• The fitting must be easily accessible to allow the sensor or the fitting itself to be maintained and cleaned regularly
• Do not allow the fitting (and thus also the sensor) to swing against and hit the basin edge
• When working with systems involving pressure and/or temperature, ensure that the fitting and sensor meet all relevant requirements
• The system designer must check that the materials in the fitting and sensor are suitable for the measurement (chemical compatibility, for instance)
  Material| PVC
  ---|---
  Admissible temperature| 0 to 60 °C
  Pressure max.| 5 bars

Short pole

The short pole is available in 2 versions:
version with elbowed shutter. The nozzle of support is included in the offer.

PF-ACC-C-00486

| 90° ELBOW SHORT PERCH FOR PLASTIC OPTOD

SENSOR (1495 mm, ELBOWED SHUTTER)

---|---

version with shutter for mounting with chain, nozzle of support is included in the offer.

PF-ACC-C-00487

| 90° ELBOW SHORT PERCH FOR PLASTIC OPTOD

SENSOR (1550 mm, RING SHUTTER)

---|---

Long pole

The long poles are available in elbow version, for installations in the aeration basin, and straight, for applications in open channel. Every pole is equipped with an elbowed shutter and with waterproofness joints. The lower part includes a nozzle which is adapted to the sensor what assures its mechanical support.

Elbowed pole with elbowed shutter

PF-ACC-C-00484

| 90° ELBOW LONG PERCH FOR         PLASTIC         OPTOD

SENSOR (2955 mm, ELBOWED SHUTTER)

---|---

Straight long pole with an elbowed shutter

PF-ACC-C-00485

| STRAIGHT LONG PERCH FOR PLASTIC OPTOD SENSOR (2745 mm, ELBOWED

SHUTTER)

---|---

Mounting accessories for pole.
The elements of fixation for the poles are flexible and specially studied to adapt themselves to the different configurations of assembly.

– Pole kit fixation

NC-ACC-C-00009

| POLE FIXATION KIT FOR

NUMERICAL SENSOR (ON LOW WALL)

---|---

NC-ACC-C-00010

| POLE FIXATION KIT FOR

NUMERICAL SENSOR (ON LIFE LINE)

NC-ACC-C-00011

| POLE FIXATION KIT FOR

NUMERICAL SENSOR (ON VERTICAL AXIS)

PF-ACC-C-00272

| VERTICAL AXIS FOR NUMERICAL SENSOR POLE

(TO BE FIXED ON SOIL)

Accessories kit for assembly of poles with chain.

SHORT POLE FIXATION KIT FOR NUMERICAL SENSOR (ON LIFE LINE)

NC-ACC-C-00014| SHORT POLE FIXATION KIT FOR NUMERICAL SENSOR (ON VERTICAL AXIS)

Insertion in a pole.
The sensor is mounted on the relevant fitting as described below, using a sensor holder, which can be used both for the short and long pole:

1. Remove the protective cap on the sensor and insert the sensor (2) into the nozzle (1) as far as the stop..
2. Insert the sensor cable into the fitting pipe (6) and completely feed through.
3. Screw the sensor holder with the union nut (5) onto the fitting pipe (6) and tighten until handtight.

 Electrical connections.

The sensor could deliver within version bare wire on 3, 7, 15 m or on other length (up to 100 m).

Communication – Power supply

Signal interface

| Modbus 1 RS-485 or SDI-12 2,3

1,2 The sensor responds in Modbus / SDI12 including during Standby

3 The use and connexion of SDI12 bus may increase the standby power consumption* up to 100uA depending the level of the line (high or low). The consumption is not increased if the SDI12 line is disconnected or released to 0V

(Modbus RTU only)

Sensor power-supply (RS485 and SDI12)

| 5 V 1,2 to 12 3,4 V DC (warm-up time 100 ms)

1 Absolute minimum 4.5V with 1m of cable, boot and precision not guaranteed under 5V

2 Minimum voltage subjected to cable length-related losses

3 13V Absolute maximum with a more than 2 mA continuous over consumption

4 Small over consumption between 12V and 12.5V

Typical Consumption at 5V (RS485) Recommended for ultra- low power (1 measure uses less than 18 uWh)

Subject to modifications in case of internal parts

evolution

| Automatic standby less than 22 μA* (110 μW) Maximum peak current: RS485 55 mA (2 ms)

Maximum current during the measurement: 19.5 mA (97.5 mW) Average current during the measurement: 13 mA (65 mW)

Average current RS485 (1 meas. / seconde): 3 mA (15 mW)

Typical Consumption at 12V (RS485)

Never exceed 12.0V for low power (1 measure uses less than 43 uWh)

Subject to modifications in case of internal parts

evolution

| Automatic standby less than 25 μA* (300 μW) Maximum peak current: 80 mA (2.5 ms)

Maximum current during the measurement: 20.5 mA (246 mW) Average current during the measurement: 14 mA (168 mW)

Average current RS485 (1 meas. / seconde): 3.2 mA (38.4 mW)

Typical Consumption at 12.5V (RS485)

Not recommended for low power

Subject to modifications in case of internal parts evolution

| Automatic standby less than typical 35 μA* (438 μW) max 1 mA Maximum peak current: 85 mA (3 ms)

Maximum current during the measurement: 21 mA (262.5 mW) Average current during the measurement: 18 mA (225 mW)

Average current RS485 (1 meas. / seconde): 3.2 mA (40 mW)

Typical Consumption at 12V (SDI12)

Never exceed 12.0V for low power

Subject to modifications in case of internal parts evolution

| Automatic standby less than 25 μA* (300 μW) Maximum peak current: 85 mA (3 ms)

Maximum current during the measurement: 27 mA (324 mW)

Average current during the measurement: 18 mA (216 mW) Average current

(1 meas. / seconde): 6 mA (72 mW)

Wiring diagram

Cable length up to 15m| Cable lenght 15 to 100 meters Red

Purple

Yellow           Power supply

Orange          V+ pink

2 – Blue          SDI-12

3 – Black          Power supply V- 4 – Green        B ” RS-485 ”

5 – White        A ” RS-485 ”

6 –               Cable shield Green/yellow with Power

supply V-

 | 1- Red| Power supply V+|
2 – Blue| SDI-12
3 – Black| Power supply V-
4 – Green| B ” RS-485 “
5 – White| A ” RS-485 “
6 –

Green/yellow

| Cable shield with Power supply V-

Note:
Never exceed a voltage of 10VDC (absolute maximum rating) on communication lines RS485, A or B, under penalty of irreversible destruction of the transceiver component RS 485.
SDI-12: respect the voltage value described in the associated standard (nominal: 5 VDC)
Always connect ground + shield first.

Start-up and maintenance.

Initial startup
Once the sensor is connected to your terminal, the sensor is settled in its accessory of assembly and the parameterization has been carried out on the display unit, the sensor is ready for initial start-up.

Note:
For measurement, you must eliminate bubbles trapped under the membrane.
Presence of chlorine will distort the measure (overestimation of dissolved oxygen level).
During the introduction of the sensor in the measurement environment, wait for sensor’s temperature stabilization before measure processing.
To optimize a sustainable functioning of your probe, w e recommend you to respect a frequency of measure superior to 10 seconds. .

Started:
Remove the black cap of protection (by holding the sensor head downward and by unscrewing the hood towards the right).
The sensor is delivered dry and the DODISK must be rehydrated so that the measures are optimized.
After dry storage, rehydrate the membrane for a 12 hours period (one night) in clear water.

Calibration
The sensor is calibrated to specification at the factory. The manufacturer does not recommend calibration unless periodically required by regulatory agencies. If calibration is required, let the sensor come to equilibrium with the process before calibration. Do not calibrate the sensor at setup.
After the membrane cap is replaced, calibration should be carried out.
It is also advisable to regularly clean the sensor (see the chapter maintenance: 5.3);

Calibration in 2 points.
With two-point calibration, the zero point (0% – offset) and slope (100 %) of the sensor are calibrated. This calibration method offers the greatest possible level of accuracy and is particularly recommended for measurements of small oxygen concentrations.
It is carried out as follows:

Offset calibration:

• The sensor beforehand cleaned (to see chapter maintenance 5.3) is immersed in a water-sulfite solution (sulphite concentration < 2 %) in order to determine the zero point (0 % saturation). Mix the solution with the sensor so that the saturation in oxygen decreases more quickly (The oxygen fixed to the DODISK) must be consumed),
  CAUTION! Damage to the sensor membrane due to chemicals.
  A damaged membrane can lead to incorrect measurement results.
  The sensor membrane must not be in contact with the sulphite solution for longer than one hour.

• Washing (with clear water) and drying the sensor,
  Slope calibration:

• Sensor slope is determined by positioning in the oxygen-saturated environment (100 % saturation.
  The slope of the sensor is calibrated beyond the defined state of 100 % oxygen saturation. This state can in principle be achieved in two ways:

• By positioning the sensor in water vapor-saturated air (for example, directly over a water
  surface).

• By positioning the sensor in air-saturated water (air is directed through water until the water
  is saturated with it). The illustration below is a representation of the conditions in air-saturated water.

• The sensor must be kept dry during the calibration process. Drops of water adhering to the sensor membrane could distort the measurement result.

•  The air pressure and temperature must remain constant during the calibration.

Calibration in 1 point.
The calibration in 1 point consists in propping up a 100% point: please consult the above chapter (slope calibration).

Maintenance

The maintenance schedule shows minimum intervals for regular maintenance tasks. Perform
maintenance tasks more frequently for applications that cause electrode fouling.
Note: Do not disassemble the probe for maintenance or cleaning.

• The sensor must always be kept clean, particularly in the area around the optical membrane. The presence of a biofilm on the membrane cap can lead to measuring errors.
• A dirty membrane should be cleaned with warm, soapy w ater. A soft sponge should be used for cleaning (not an abrasive scouring sponge).
• If the sensor is put out of operation, it should be rinsed prior to being stored, and the protective cap should be fitted with the protective case and a moist absorbent surface (like cotton).

Cleaning.
Rinse meticulously the sensor and the membrane with clear water.
If deposits like biofilm or mud persist, wipe the membrane gently with a sweet cloth or an absorbent paper.
Attention: For the Titanium version clean the body of the sensor by means of acetone (do not use methylated spirit, ethanol or methanol).

Change of the DODISK.
The average life time of the DODISK is of 2 years.
In case of deterioration of the DODISK or of difficulty on the processes of calibration, the DODISK will be to change.

• Open the black pouch and take out the active tablet (DODISK on white plastic holder) and the seal.

• Hold the sensor vertically in the air.
  Unscrew the strainer to access the used DODISK. Remove the gasket and the used DODISK.

• Hold the sensor vertically.
  Check the groove for foreign matter. Position the 16 x 1 O-ring in the groove.

• Hold the sensor vertically.
  Position the DO-Disk and its holder, head-centered, with the black surface of the DO-Disk visible.

• Hold the sensor vertically.
  Screw the strainer to the stop, the DO-Disk holder will center with the tapping.

Storage.
With the aim of keeping the active pastille operational quickly, keep the membrane hydrated with the protective case and a moist absorbent surface (like cotton wool). After dry storage, rehydrate the membrane for a 12 hours period.

AQUALABO After-Sales Service
AQUALABO
115 Rue Michel MARION
56850 CAUDAN – France
Tel.: +33 (0)4 11 71 97 41

References

• Aqualabo - World leader in water monitoring and analysis
• Aqualabo - World leader in water monitoring and analysis

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