mihm-vogt HT-S 2 High Temperature Sintering Furnaces Instruction Manual

September 29, 2024
mihm-vogt

HT-S 2 High Temperature Sintering Furnaces

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Specifications:

  • Manufacturer: MIHM-VOGT GmbH & Co. KG
  • Model: Sintering Furnaces
  • Location: 76297 Stutensee

Product Information:

1. General Information:

The supplemental information provided here is to assist in the
maintenance and smooth operation of MIHM-VOGT sintering furnaces.
It is important to strictly follow the operating instructions.

2. Heating Chambers:

2.1. Manual Cleaning of the Heating Chambers:

The heating chambers or sintering plating should be cleaned
using a soft brush. Avoid using compressed air for cleaning.

2.2. Cleaning the Heating Chambers by Means of a Cleaning

Firing:

Chemical residues can be reduced by running a cleaning program
multiple times. Specific programs can be accessed based on the
device type and serial number.

2.3. Cleaning Cycle of the Heating Chambers:

Cleaning cycles should be performed weekly or monthly depending
on the usage to maintain the heating chambers.

3. Heating Elements:

3.1. Checking MoSi Heating Elements:

Visual inspection of MoSi heating elements is necessary before
each sintering process to ensure they are intact and free from
chemical contamination.

3.2. Regeneration Firing of MoSi Heating Elements:

Regeneration firing can be done following specific instructions
based on the device’s serial number to maintain the heating
elements.

FAQ:

Q: How often should I clean the heating chambers?

A: The heating chambers should be cleaned weekly or monthly,
depending on your usage.

Q: What should I avoid when cleaning the heating chambers?

A: Do not use compressed air for cleaning; instead, use a soft
brush.

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Maintenance of MIHM-VOGT Sintering Furnaces
MIHM-VOGT GmbH & Co. KG, 76297 Stutensee

Contents

1. General information

3

2. Heating chambers

3

2.1. Manual cleaning of the heating chambers

3

2.2. Cleaning the heating chambers by means of a cleaning firing

4

2.3. Cleaning cycle of the heating chambers

4

3. Heating elements

5

3.1. Checking MoSi heating elements

5

3.2. Regeneration firing of MoSi heating elements

6

3.3. Regeneration cycle of MoSi heating elements

7

3.4. Checking SiC heating elements

7

4. Installing sintering furnaces

8

4.1. Dust prevention

8

4.2. Acidic ambient air

9

5. Pre-drying of zirconium oxide

9

6. Additional maintenance tasks

9

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Service and maintenance of MIHM-VOGT sintering furnaces

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1. General information
The following information presents supplemental information to the operating instructions for MIHM-VOGT sintering furnaces. The contents of the operating instructions must be strictly observed. This supplemental information is intended to help ensure the smooth operation of MIHM-VOGT sintering furnaces.
2. Heating chambers
The heating chambers of MIHM-VOGT sintering furnaces are comprised of two high-quality insulating layers. The following information is intended to help ensure that MIHM-VOGT sintering furnaces have a long service life. A visual inspection of the heating chambers should be performed prior to each sintering process. Foreign particles and accumulations of dirt can affect the sintering results. Dust and foreign particles must be removed by means of manual cleaning, while chemical contamination (e.g. as a result of colouring liquids) can be eliminated by a cleaning firing.
2.1. Manual cleaning of the heating chambers
The heating chambers or sintering plating (see Fig. 1 or Fig. 2) must be cleaned using a soft brush. Under no circumstances should compressed air be used to clean the heating chambers!

Fig. 1

Fig. 2

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Service and maintenance of MIHM-VOGT sintering furnaces

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2.2. Cleaning the heating chambers by means of a cleaning firing
Chemical residues, for example from zirconium oxide, can be reduced using a cleaning program. If necessary, the cleaning program should be run multiple times. In the case of devices with a 6-digit serial number, the cleaning program can be accessed as follows:

Type of device:

Program

TABEO-1/M/ZIRKON-100

C

TABEO-1/S/ZIRKON-100

C

TABEO-2/M/ZIRKON-120

C

TABEO-2/S/ZIRKON-120

C

HTS-2/M/ZIRKON-120

32

HT-2/M/ZIRKON-120

32

Tab. 1

In the case of devices with a 5-digit serial number, the cleaning program can be programmed as follows:

Heating rate Temperature Holding time

°C/min.

°C

min.

TLevel 4

25

a

bLevel 3

25

.

Level 2

25

2

Level 1

25

300

0

1500

120

0

0

0

0

Tab. 2 2.3. Cleaning cycle of the heating chambers

The wear of materials in the heating chambers of MIHM-VOGT sintering furnaces depends substantially on the individual use. The cleaning cycles described below should therefore simply serve as a suggestion.

Service and maintenance of MIHM-VOGT sintering furnaces

V1.0

What?
Cleaning the heating chamber with a brush
Cleaning the heating chamber using a cleaning program
Tab. 3

When? weekly monthly

3. Heating elements
Mihm-Vogt sintering furnaces are equipped either with MoSi heating elements (Fig. 3) or with SiC heating elements (Fig. 4). Furnaces equipped with MoSi heating elements can be heated to 1650 °C; furnaces with SiC heating elements can be heated to a maximum of 1550 °C.

Fig. 3

Fig. 4

3.1. Checking MoSi heating elements
A visual inspection of the heating elements should be performed prior to each sintering process. MoSi heating elements are protected against outgassing by a glaze-like oxide layer. However, chemical contamination (e.g. by colouring liquids) can destroy the protective oxide layer on the heating elements, and spalling may occur on the surface (Fig. 5).

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Service and maintenance of MIHM-VOGT sintering furnaces

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3.2. Regeneration firing of MoSi heating elements
A regeneration firing can be used to attempt to restore the protective oxide layer on the MoSi heating elements. The furnace must be empty when it is heated during the regeneration firing ­ i.e. without sintering support structures or sintering aids. The protective coating on the heating elements must be examined after the firing. If the surface does not have a glaze-like coating (see Fig. 6), the regeneration firing must be repeated.

Page 6

Fig. 5

Fig. 6

In the case of devices with a 6-digit serial number, the regeneration firing can be accessed as follows:

Type of device: TABEO-1/M/ZIRKON-100 TABEO-2/M/ZIRKON-120 HTS-2/M/ZIRKON-120 HT-2/M/ZIRKON-120
Tab. 4

Program E E 33 33

Service and maintenance of MIHM-VOGT sintering furnaces

V1.0

In the case of devices with a 5-digit serial number, the regeneration firing can be programmed as follows:

Serial number is lower than 50703:

Heating rate Temperature Holding time

°C/min.

°C

min.

Level 4

25

300

0

Level 3

25

1550

120

Level 2

25

1550

180

Level 1

25

Tab. 5

1550

180

3.3. Regeneration cycle of MoSi heating elements
Wear in MoSi heating elements in MIHM-VOGT sintering furnaces depends substantially on the individual use. The cycles described below should therefore simply serve as a suggestion.

What?

When?

Checking the heating elements

monthly

Regeneration of the heating elements with the aid of regeneration programs
Tab. 6

monthly

3.4. Checking SiC heating elements
A visual inspection of the heating elements should be performed prior to each sintering process. Unlike MoSi heating elements, SiC heating elements do not have an oxide layer. In particular in the case of the first sintering processes, blistering may occur on the surface of these heating elements. This blistering is not critical and can be ignored.

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Service and maintenance of MIHM-VOGT sintering furnaces

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When SiC heating elements approach the end of their service life, there is a significant reduction in their heating capacity. As a rule, SiC heating elements can only be replaced as a complete set.
4. Installing sintering furnaces
When installing MIHM-VOGT sintering furnaces, the conditions in the operating manual must be observed. The following presents supplementary information.
4.1. Dust prevention
Excessive dust exposure can damage the sintering furnaces and thus substantially shorten the service life of the device. Dust must therefore be avoided as much as possible (for examples if an excessive load, see Fig. 7 and Fig. 8). Excessive dust exposure may be caused by zirconium oxide milling machines with insufficient extraction. If zirconium oxide milling machines are set up in the immediate vicinity of sintering furnaces, care should be taken to ensure that these devices have adequate extraction. Otherwise, zirconium oxide sintering furnaces should be set up in separate rooms that are not exposed to dust.

Fig. 7

Fig. 8

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Service and maintenance of MIHM-VOGT sintering furnaces

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4.2. Acidic ambient air
Acidic ambient air can cause damage, especially to the electronic components in a sintering furnace (for examples, see Fig. 9 and Fig. 10) and therefore should be avoided. Acidic ambient air may arise due to the use of acidic colouring liquids. Such colouring liquids should therefore be used outside of the room in which the sintering furnaces are installed whenever possible. Care should also be taken to ensure that the sintering furnaces are only loaded with well-dried zirconium oxide restorations.

Fig. 9

Fig. 10

5. Pre-drying of zirconium oxide
Moisture can damage MIHM-VOGT sintering furnaces. It can be introduced into the furnace, for example, by colouring liquids or even by wet-grinding milling machines, for example. It is therefore recommended that restorations undergoing sintering are dried in an external furnace.
6. Additional maintenance tasks
The need to carry out maintenance work largely depends on the individual frequency of use of the furnace. The intervals shown below are therefore to be considered as approximate values only.

V1.0

Service and maintenance of MIHM-VOGT sintering furnaces

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What?

When?

Cleaning the housing

as needed

Cleaning the heating chamber with a brush

weekly

Cleaning the heating chamber using a cleaning program

monthly

Inspecting the surface of the heating element and performing a regeneration firing

monthly

Checking the temperature Tab. 7

annually

How?
with a dry cloth
See the instructions above
See the instructions above
See the instructions above
using a MIHM-VOGT test kit

MIHM-VOGT GmbH & Co. KG Friedrich-List-Str. 8
76297 Stutensee-Blankenloch 07244-70871-0www.MIHM-VOGT.de

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Service and maintenance of MIHM-VOGT sintering furnaces

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