HANNA instruments HI9813-51 Portable pH EC TDS Temperature Meters Instruction Manual

HI9813-51 Portable pH EC TDS Temperature Meters
Instruction Manual

HI9813-51 & HI9813-61 Portable
pH / EC / TDS / Temperature Meters

Dear Customer,
Thank you for choosing a Hanna Instruments® product. Please read this instruction manual carefully before using this instrument. This manual will provide you with the necessary information for the correct use of this instrument, as well as a precise idea of its versatility. If you need additional technical information, do not hesitate to e‑mail us at tech@hannainst.com or view our contact list at www.hannainst.com.
All rights are reserved.
Reproduction in whole or in part is prohibited without the written consent of the copyright owner, Hanna Instruments Inc., Woonsocket, Rhode Island, 02895, USA.

PRELIMINARY EXAMINATION

Remove the instrument and accessories from the packaging and examine them carefully. For further assistance, please contact your local Hanna Instruments ® office or email us at tech@hannain.com. Each instrument is delivered in a rugged carrying case and supplied with:

• HI1285-51 pH / EC / TDS / Temperature combination probe with DIN connector with 1 m (3.3’) cable (HI9813-51)
• HI1285-61 pH / EC / TDS / Temperature combination probe with CAL Check™ and DIN connector with 1 m (3.3’) cable (HI9813-61)
• pH 7.01 buffer solution (1 sachet)
• 1413 μS/cm conductivity solution (1 sachet)
• 1500 ppm TDS calibration solution (1 sachet)
• General purpose cleaning solution for Agriculture (2 sachets)
• Calibration check solution (2 sachets) (HI9813-61)
• 100 mL plastic beaker (1 pc.)
• 9V Alkaline battery (1 pc.)
• Instrument quality certificate
• Instruction manual

Note: Save all packing material until you are sure that the instrument works correctly. Any damaged or defective item must be returned in its original packing material with the supplied accessories.

GENERAL DESCRIPTION

HI9813-51 and HI9813-61 are portable, water-resistant meters, designed for measuring pH, EC / TDS, and temperature when paired with their respective probes, i.e. HI9813-51 with HI1285-51 and HI9813-61 with HI1285-61. The meters are easy to use, with dedicated keys for measurement modes that are clearly displayed on the LCD, and knobs for 1-point calibration of pH and EC. On- screen tutorial messages guide the user through calibration and measurement.
Main Features

• 3-in-1 combination probe with pH, EC /T DS, and temperature sensors
• CAL Check™ (HI9813-61 only)
• Best for hydroponics, greenhouses, farming, and groundwater app.

Probe features
The polypropylene (PP) body houses three sensors:
pre-amplified pH electrode: Cloth junction, Polymer-gel electrolyte, Low temperature (LT) glass-sensing bulb
amperometric EC/TDS sensor: Two stainless-steel prongs for determination of conductivity and total dissolved solids
NTC Thermistor (built-in): Ensures that readings are compensated for temperature variations

FUNCTIONAL DESCRIPTION & LCD DISPLAY

HI9813-51

HI9813-61

7. ppm (mg/L) key – TDS selection

 SPECIFICATIONS

Mete
pH

EC

TDS

actual EC readings (based on 442 curves for natural water)

Temperature

HI1285-61 for HI9813-61
Battery life| Approximately 150 hours of continuous use
Auto shut-off| After 8 minutes of non-use
Battery type| 1 x 9V Alkaline
Environment| 0 to 50 °C (32 to 122 °F); 100% RH
Dimensions| 145 x 80 x 36 mm (5.7 x 3.1 x 1.4 “)
Weight| 230 g (8.1 oz.)

• The range may be limited by the probe’s limits.

Probe

EC: 0 to 6 mS/cm
Temperature: 0 to 50°C (32 to 122°F)
Tip Shape| Spheric, Ø 8.0 mm (0.31”)
Glass Type| LT (low temperature)
Temperature Sensor| Yes
Amplifier| Yes
Body Material| Polypropylene
Dimensions| Length: 186 mm (7.32”)
Shaft length: 95 mm (3.74”)
Shaft diameter: 16 mm (0.62”)
Cable| 1 m (3.3’) with an 8-pin DIN connector
Plug| HI1285-51: DIN
HI1285-61: DIN with CAL Check™

GENERAL OPERATIONS

5.1. BATTERY REPLACEMENT
To replace the batteries, follow the next steps:

• Turn OFF the instrument.
• Remove the three screws on the back of the instrument to open the battery compartment.
• Remove the old battery.
• Insert one new 9 V Alkaline battery in the battery compartment while paying attention to the correct polarity.
• Close the battery compartment using the three screws.

Note: If the battery percentage indicator is empty, the battery level is too low and the battery needs to be replaced.

5.2. CONNECTING THE ELECTRODE
Align the DIN connector’s 8 pins with the socket and push in the plug.
5.3. TURNING THE METER ON
Turn the instrument on by pressing the On/Off key.

5.4. SENSOR PREPARATION & CONDITIONING

1. Remove the protective cap
2. If the protective cap does not contain any liquid, pour the HI70300 Storage solution into the cap.
3. Place it back on the sensor and soak it for at least 30 min. before use.
4. Rinse with tap water prior to Calibration or Measurement.

CALIBRATION

6.1. pH
For high accuracy, frequent calibrations are recommended. Additionally, the pH range should be recalibrated:

• Whenever the electrode is replaced.
• At least once a month.
• After testing aggressive chemicals.
• If HI9813-61 does not pass the CAL Check test

Preparation
Recommended pH calibration standard buffers: pH 4.01, 6.86 (NIST), 7.01, 9.18 (NIST), 10.01. Use pH 7.01 (HI7007) for neutral samples, pH 4.01(HI7004) for acidic samples, and pH 10.01 (HI7010) for alkaline samples.
Procedure

1. Connect the probe and turn the meter on.
2. Press the pH key to select the pH measurement mode.
3. Remove the protective cap and rinse the probe.
4. Pour buffer solution into a clean beaker.
5. Immerse the tip of the probe 4 cm (1 1/2”) in the selected buffer and wait a few minutes for the measurement to stabilize.
6. Press the temperature key (°C) to measure buffer solution temperature. Take note of the displayed value.
7. Rotate the calibration knob to adjust the pH value to match the written buffer solution temperature. The pH calibration is now complete. (see pH VALUES AT VARIOUS TEMPERATURES section).

Notes: If, when rotating the knob, the required value cannot be reached, the probe requires cleaning (see the PROBE MAINTENANCE section). If the issue still persists, the probe requires replacement.

6.2. EC / TDS
Preparation
Recommended EC calibration points: 1.41 mS/cm (1413 μS/cm) using HI70031 EC calibration solution, or 1500 ppm using HI70442 TDS calibration solution. Calibrate the probe frequently for improved accuracy. Additionally, calibration should be performed:

• Whenever the probe is replaced
• Always use fresh calibration solutions and perform electrode maintenance prior to calibration (see PROBE MAINTENANCE section).

Procedure

1. Pour calibration solution into clean beakers sufficient to cover the sensing portion of the probe (4 cm / 1 1/2”). If possible, use plastic beakers to minimize any EMC  interferences. For accurate calibration and to minimize cross-contamination, use two beakers, one for rinsing the probe and one for calibration.
2.  Raise and lower the probe in the standard to ensure the entire cell area is filled with the standard.
3. Shake any bubbles off the two electrodes (prongs).
4. Center probe in beaker away from beaker walls.
5. Press the mS/cm (or ppm) key to select EC or TDS measurement mode.
6. Rotate the EC/TDS calibration knob until the reading is displayed at 25 °C.

EC/TDS Conversion Factor
HI9813-51 and HI9813-61 have a variable TDS conversion factor, automatically adjusted from 0.56 to 0.78 based on actual EC readings (based on the 442 curves for natural water).

MEASUREMENT

7.1. pH

• Immerse the probe tip 4 cm (1 1/2”) into the sample.

• Press pH key to select pH measurement mode.

• Stir briefly and wait a few minutes for the measurement to stabilize. The measured pH value is displayed on the screen.
  

• If measurements are taken in different samples successively, rinse the probe thoroughly to minimize cross-contamination. After rinsing with water, rinse the probe with some of the samples to be measured next.

7.2. EC / TDS

• Immerse the probe tip 4 cm (1 1/2”) into the sample.  If possible, use plastic beakers to minimize any EMC interferences.

• Tap the probe lightly on the bottom of the beaker to remove any air bubbles trapped inside.

• Press the mS/cm or ppm key to select EC or TDS measurement mode.

• Wait a few minutes. The displayed measured value (in mS/cm or ppm)is temperature compensated automatically.  teens from DY9812V3 received from M

7.3. TEMPERATURE

• Immerse the tip of the probe 4 cm (1 1/2”) into the sample.
• Press the °C (Temperature) key.
• Stir briefly and wait a few minutes for the measurement to stabilize. The real value is displayed on the LCD.

7.4. WARNINGS
pH & EC / TDS

• If the measured value is outside the parameter limit of the instrument, the maximum or minimum value is displayed blinking.
• If a broken / wrong probe has been connected, “— — —” is displayed.

Temperature

• If the probe is not connected, or if a broken / wrong probe has been connected, “— — —” is displayed.

pH VALUES AT VARIOUS TEMPERATURES

For instance, if the buffer temperature is 25 °C, the display should show pH 4.0 or 7.0, or 10.0. If the buffer temperature is 10 °C, the display should show pH 4.0 or 7.0 or 10.1.

PROBE MAINTENANCE

Periodic Maintenance
Proper care and maintenance is essential for accurate readings. Cleaning, calibrating, and appropriate storage extend the life of the probe.

• Inspect connector for corrosion and replace probe if necessary.
• Inspect probe and cable for cracks or points of broken insulation. If any are present, replace the probe.
• After use rinse the probe with tap water and dry it.
• Monthly, a more thorough cleaning is advised. Clean the EC sensor with a non-abrasive, mild detergent.

Cleaning & Conditioning
pH portion

• Remove the protective cap.
• If the bulb and/or junction are dry, soak the electrode in the HI70300 Storage solution for at least 30 minutes. To ensure a quick response time, the glass bulb and the junction should be kept moist and not allowed to dry.
• Rinse the sensor in flowing water then clean by soaking it for 1 minute in HI7073 Protein cleaning solution or HI7077 Oil and fat cleaning solution. After cleaning, soak the sensor in HI70300 Storage solution for 30 minutes before calibrating.

EC portion

• After every series of measurements, rinse the probe with tap water.
•  If a more thorough cleaning is required clean the sensor with a soft brush to loosen any debris.
• Use a mild detergent to remove oily coatings.
• Flush with purified water after cleaning.

Notes: Recalibrate the meter after cleaning. If, after cleaning, the meter still can not be calibrated, replace the probe. For field applications, have a spare probe ready. When maintenance does not correct the issue, change the probe and recalibrate the meter.

Storage

• Store the sensor with a few drops of HI70300 Storage solution or pH 4.01 buffer in the protective cap. Tap water may also be used for a very short period (a few days).
• Never use distilled or deionized water to store pH sensors.

CAL Check™ & Cleaning (HI9813-61)
To check the meter’s calibration status:

1. Rinse the probe with water

2. Immerse the tip of the probe 4 cm (1 1/2”) into the HI50021 calibration check solution.
   Note: A reading around pH 4.01 indicates that the probe is broken and requires replacement.

3. Press the Check key. “Probe is OK” is displayed if the meter is calibrated. “Clean Probe and Calibrate” indicates that cleaning is required.

To clean the probe:

1. Immerse the tip of the probe 4 cm (1 1/2”) into a HI700661 cleaning solution and soak for 5 minutes.
2.  Rinse with tap water.
3. Immerse the tip of the probe in the HI50021 calibration check solution.
4. Press the Check key. “Probe is OK” is displayed if the meter does not require calibration. “Clean Probe and Calibrate” indicates that the meter requires calibration. Follow pH Calibration steps.

ACCESSORIES

Probes

HI1285-51| Combination, amplified pH / EC / TDS/temperature probe with built- in temperature sensor, 8-pin DIN connector, and 1 m (3.3’) cable
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HI1285-61| Combination, amplified pH / EC / TDS / temperature probe with built-in temperature sensor, with CAL Check™ feature,8-pin DIN connector, and 1 m (3.3’) cable

pH Buffer Solutions

Conductivity & TDS Calibration Solutions

Other Solutions

Other Accessories

CERTIFICATION

All Hanna® instruments conform to the CE European Directives.

Disposal of Electrical & Electronic Equipment. The product should not be treated as household waste. Instead, hand it over to the appropriate collection point for the recycling of electrical and electronic equipment which will conserve natural resources. Disposal of waste batteries. This product contains batteries, do not dispose of them with other household waste. Hand them over to the appropriate collection point for recycling. Ensuring proper product and battery disposal prevents potential negative consequences for the environment and human health, which may be caused by inappropriate handling. For more information, contact your city, your local household waste disposal service, or the
place of purchase.

RECOMMENDATIONS FOR USERS

Before using these products, make sure they are entirely suitable for your specific application and the environment in which they are used. Any variation introduced by the user to the supplied equipment may degrade the instruments’ EMC performance. For your and the instrument’s safety do not use or store the instrument in hazardous environments.

WARRANTY

HI9813-51 and HI9813-61 are warranted for two years against defects in workmanship and materials when used for their intended purpose and maintained according to instructions. Probes are guaranteed for six months. This warranty is limited to repair or replacement free of charge. Damage due to accidents, misuse, tampering, or lack of prescribed maintenance is not covered. If service is required, contact your local Hanna Instruments office. If under warranty, report the model number, date of purchase, serial
number (engraved on the bottom of the meter), and the nature of the problem. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna ® Instruments, first obtain a Returned Goods Authorization (RGA) number from the Technical Service department and then send it with shipping costs prepaid. When shipping any instrument, make sure it is properly packed for complete protection.
Hanna ®Instruments  reserves the right to modify the design, construction, or appearance of its products without advance notice.

World Headquarters
Hanna Instruments Inc.
Highland Industrial Park
584 Park East Drive
Woonsocket, RI 02895 USA
www.hannainst.com
MAN9813-61
Printed in ROMANIA

References

• pH Meters, Photometers, Titrators, Controllers - Hanna Instruments

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